Application of molecularly imprinted polymers to determine B 1 , B 2 , and B 3 fumonisins in cereal products

The aim of this study was to develop an analytical method for qualitative and quantitative determination of the B 1 , B 2, and B 3 fumonisins in cereal products. A LC coupled to an IT‐ MS was used as the analytical instrument. The AFFINIMIP F umo ZON M olecularly I mprinted P olymer SPE cartridges (...

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Veröffentlicht in:Journal of separation science 2013-02, Vol.36 (3), p.578-584
Hauptverfasser: Bryła, Marcin, Jędrzejczak, Renata, Roszko, Marek, Szymczyk, Krystyna, Obiedziński, Mieczysław W., Sękul, Janusz, Rzepkowska, Małgorzata
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Sprache:eng
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Zusammenfassung:The aim of this study was to develop an analytical method for qualitative and quantitative determination of the B 1 , B 2, and B 3 fumonisins in cereal products. A LC coupled to an IT‐ MS was used as the analytical instrument. The AFFINIMIP F umo ZON M olecularly I mprinted P olymer SPE cartridges (Polyintell) were used to isolate fumonisins from the analyzed samples and the clean‐up step. Statistical parameters evaluated in some validation experiments were as follows: mean recovery 95–106%, precision
ISSN:1615-9306
1615-9314
DOI:10.1002/jssc.201200753