Syntheses with stable isotopes: Sodium cyanide‐ 13 C

Sodium cyanide‐ 13 C has been prepared in 65–70% overall yield from carbon‐ 13 C monoxide in a three‐step synthesis proceeding through isopropyl formate‐ 13 C and formamide‐ 13 C as intermediates. Several. methods for the dehydration of formamide have been investigated.

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Veröffentlicht in:Journal of labelled compounds 1975-01, Vol.11 (3), p.307-312
Hauptverfasser: Whaley, Thomas W., Ott, Donald G.
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container_title Journal of labelled compounds
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creator Whaley, Thomas W.
Ott, Donald G.
description Sodium cyanide‐ 13 C has been prepared in 65–70% overall yield from carbon‐ 13 C monoxide in a three‐step synthesis proceeding through isopropyl formate‐ 13 C and formamide‐ 13 C as intermediates. Several. methods for the dehydration of formamide have been investigated.
doi_str_mv 10.1002/jlcr.2590110302
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title Syntheses with stable isotopes: Sodium cyanide‐ 13 C
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