Syntheses with stable isotopes: Sodium cyanide‐ 13 C

Syntheses with stable isotopes: Sodium cyanide‐ 13 C

Sodium cyanide‐ 13 C has been prepared in 65–70% overall yield from carbon‐ 13 C monoxide in a three‐step synthesis proceeding through isopropyl formate‐ 13 C and formamide‐ 13 C as intermediates. Several. methods for the dehydration of formamide have been investigated.

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Veröffentlicht in:Journal of labelled compounds 1975-01, Vol.11 (3), p.307-312
Hauptverfasser: Whaley, Thomas W., Ott, Donald G.
Format: Artikel
Sprache:eng
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Zusammenfassung:Sodium cyanide‐ 13 C has been prepared in 65–70% overall yield from carbon‐ 13 C monoxide in a three‐step synthesis proceeding through isopropyl formate‐ 13 C and formamide‐ 13 C as intermediates. Several. methods for the dehydration of formamide have been investigated.
ISSN:0022-2135
DOI:10.1002/jlcr.2590110302