Synthesis of tritium labelled catechol

The preparation of tritium labelled catechol by catalytic reduction of tetrabromocatechol is described. Recrystallization of catechol (U‐3H) after silica gel column purification gave 68% yield of the desired product with 98% purity as assayed by high performance liquid chromatography.

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Bibliographische Detailangaben
Veröffentlicht in:	Journal of labelled compounds & radiopharmaceuticals 1982-01, Vol.19 (1), p.35-38
Hauptverfasser:	Hwang, K. K., Bhooshan, B., Kouri, R. E., Henry, C. J.
Format:	Artikel
Sprache:	eng
Schlagworte:	Catechol (U-3H) High performance liquid chromatography Hydrogeneration apparatus Instant thin-layer chromatography-silica gel Tetrabromocatechol Tritium gas
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Beschreibung
Zusammenfassung:	The preparation of tritium labelled catechol by catalytic reduction of tetrabromocatechol is described. Recrystallization of catechol (U‐3H) after silica gel column purification gave 68% yield of the desired product with 98% purity as assayed by high performance liquid chromatography.
ISSN:	0362-4803 1099-1344
DOI:	10.1002/jlcr.2580190106