N,N,N′,N′-Tetraalkylaminoazoxybenzene Derivatives; Convenient Synthesis and Mechanistic Study

N,N,N′,N′‐tetraalkyaminoazoxybenzene derivatives were conveniently prepared by the coupling of N,N‐dialkylnitrosoaniline in the presence of acetone and KOH. The reaction mechanism was proposed and investigated, and the structure of compound 3b was also confirmed by single crystal X‐ray diffractometr...

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Veröffentlicht in:Journal of the Chinese Chemical Society (Taipei) 2007-12, Vol.54 (6), p.1639-1643
Hauptverfasser: Lai, Long-Li, Chang, Yi-Ging, Hsu, Hui-Chu, Hsu, Shun-Ju, Luo, Dao-Wen
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Sprache:eng
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Zusammenfassung:N,N,N′,N′‐tetraalkyaminoazoxybenzene derivatives were conveniently prepared by the coupling of N,N‐dialkylnitrosoaniline in the presence of acetone and KOH. The reaction mechanism was proposed and investigated, and the structure of compound 3b was also confirmed by single crystal X‐ray diffractometry.
ISSN:0009-4536
2192-6549
DOI:10.1002/jccs.200700231