Convenient synthesis of symmetrical diketosulfides from enolizable ketones using [hydroxy(tosyloxy)iodo]benzene and na 2 S ⋅ 9H 2 O
An efficient method for the preparation of symmetrical diketosulfides of the type ArCOCH 2 SCH 2 COAr has been developed from the reaction of [hydroxy(tosyloxy)iodo]benzene with various acetophenones, followed by treatment with Na 2 S ⋅ 9H 2 O. © 2009 Wiley Periodicals, Inc. Heteroatom Chem 20:172–1...
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| Veröffentlicht in: | Heteroatom chemistry 2009-01, Vol.20 (3), p.172-176 |
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| Hauptverfasser: | , , , |
| Format: | Artikel |
| Sprache: | eng |
| Online-Zugang: | Volltext |
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| Zusammenfassung: | An efficient method for the preparation of symmetrical diketosulfides of the type ArCOCH
2
SCH
2
COAr has been developed from the reaction of [hydroxy(tosyloxy)iodo]benzene with various acetophenones, followed by treatment with Na
2
S ⋅ 9H
2
O. © 2009 Wiley Periodicals, Inc. Heteroatom Chem 20:172–176, 2009; Published online in Wiley InterScience (
www.interscience.wiley.com
). DOI 10.1002/hc.20524 |
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| ISSN: | 1042-7163 1098-1071 |
| DOI: | 10.1002/hc.20524 |