Development of wall material for the microencapsulation of natural vanilla extract by spray drying
Background and objectives The aim of this study was to develop a wall material using rice starch (Oryza sativa) to optimize the microencapsulation of vanilla extract by spray drying. Native starch rice was hydrolyzed, succinated, extruded, and characterized. Findings The peak viscosity of modified s...
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| Veröffentlicht in: | Cereal chemistry 2020-05, Vol.97 (3), p.555-565 |
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| creator | Ocampo‐Salinas, Israel Oswaldo Gómez‐Aldapa, Carlos Alberto Castro‐Rosas, Javier Vargas‐León, Enaim Aída Guzmán‐Ortiz, Fabiola Araceli Calcáneo‐Martínez, Netzahualcoyol Falfán‐Cortés, Reyna Nallely |
| description | Background and objectives
The aim of this study was to develop a wall material using rice starch (Oryza sativa) to optimize the microencapsulation of vanilla extract by spray drying. Native starch rice was hydrolyzed, succinated, extruded, and characterized.
Findings
The peak viscosity of modified starches was reduced from 3,875 cP to |
| doi_str_mv | 10.1002/cche.10269 |
| format | Article |
| fullrecord | <record><control><sourceid>wiley_cross</sourceid><recordid>TN_cdi_crossref_primary_10_1002_cche_10269</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>CCHE10269</sourcerecordid><originalsourceid>FETCH-LOGICAL-c2739-1ef766e0412e5c934539f3b1523298482b55eb8a58f3ed679afd51117af931933</originalsourceid><addsrcrecordid>eNp9kMtOwzAQRS0EEqWw4Qu8RgrYnjiJlygUilSJDayjSTqmRs5DTtqSvyclrFnNjHTm6uowdivFvRRCPVTVjqZNJeaMLaSJIYIEsnO2EEKYSIBWl-yq77-mE2QKC1Y-0YF829XUDLy1_Ije8xoHCg49t23gw4547arQUlNh1-89Dq5tTmyDwz5M1AEb5z1y-h4CVgMvR953AUe-DaNrPq_ZhUXf083fXLKP59V7vo42by-v-eMmqlQKJpJk0yQhEUtFujIQazAWSqkVKJPFmSq1pjJDnVmgbZIatFstpUzRGpAGYMnu5typa98HskUXXI1hLKQoTnaKk53i184Eyxk-Ok_jP2SR5-vV_PMDGv1oVQ</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype></control><display><type>article</type><title>Development of wall material for the microencapsulation of natural vanilla extract by spray drying</title><source>Access via Wiley Online Library</source><creator>Ocampo‐Salinas, Israel Oswaldo ; Gómez‐Aldapa, Carlos Alberto ; Castro‐Rosas, Javier ; Vargas‐León, Enaim Aída ; Guzmán‐Ortiz, Fabiola Araceli ; Calcáneo‐Martínez, Netzahualcoyol ; Falfán‐Cortés, Reyna Nallely</creator><creatorcontrib>Ocampo‐Salinas, Israel Oswaldo ; Gómez‐Aldapa, Carlos Alberto ; Castro‐Rosas, Javier ; Vargas‐León, Enaim Aída ; Guzmán‐Ortiz, Fabiola Araceli ; Calcáneo‐Martínez, Netzahualcoyol ; Falfán‐Cortés, Reyna Nallely</creatorcontrib><description>Background and objectives
The aim of this study was to develop a wall material using rice starch (Oryza sativa) to optimize the microencapsulation of vanilla extract by spray drying. Native starch rice was hydrolyzed, succinated, extruded, and characterized.
Findings
The peak viscosity of modified starches was reduced from 3,875 cP to <100 cP by effect of the modification step. Native starch was gelatinized by extrusion according to gelatinization enthalpy (∆H J/g). Natural vanilla extract was encapsulated, and the most optimal conditions for the drying process were air inlet temperature of 125°C, 14.0% of total solids, and 86.2% of encapsulation efficiency. The scanning electron microscopy evidenced the formation of microcapsules; however, the confocal laser scanning microscopy showed no interaction between the wall material and the vanilla extract. This could be related to the zeta potential values of the vanilla extract and the wall material.
Conclusions
Modified rice starch is a potential wall material for the encapsulation of different bioactive compounds in the food sector.
Significance and novelty
Chemical and physical modifications such as hydrolysis, succinylation, and extrusion in native rice starch offer adequate properties to achieve 86.2% encapsulation efficiency of natural vanilla extract using spray drying.</description><identifier>ISSN: 0009-0352</identifier><identifier>EISSN: 1943-3638</identifier><identifier>DOI: 10.1002/cche.10269</identifier><language>eng</language><subject>microencapsulation ; modified starch ; rice ; spray drying ; vanilla</subject><ispartof>Cereal chemistry, 2020-05, Vol.97 (3), p.555-565</ispartof><rights>2020 Cereals & Grains Association</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c2739-1ef766e0412e5c934539f3b1523298482b55eb8a58f3ed679afd51117af931933</citedby><cites>FETCH-LOGICAL-c2739-1ef766e0412e5c934539f3b1523298482b55eb8a58f3ed679afd51117af931933</cites><orcidid>0000-0002-5507-4889 ; 0000-0002-7823-8954 ; 0000-0003-1333-3624 ; 0000-0003-3440-5981 ; 0000-0003-2767-9896 ; 0000-0002-4723-3093 ; 0000-0002-6568-8454</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Fcche.10269$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Fcche.10269$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,780,784,1417,27924,27925,45574,45575</link.rule.ids></links><search><creatorcontrib>Ocampo‐Salinas, Israel Oswaldo</creatorcontrib><creatorcontrib>Gómez‐Aldapa, Carlos Alberto</creatorcontrib><creatorcontrib>Castro‐Rosas, Javier</creatorcontrib><creatorcontrib>Vargas‐León, Enaim Aída</creatorcontrib><creatorcontrib>Guzmán‐Ortiz, Fabiola Araceli</creatorcontrib><creatorcontrib>Calcáneo‐Martínez, Netzahualcoyol</creatorcontrib><creatorcontrib>Falfán‐Cortés, Reyna Nallely</creatorcontrib><title>Development of wall material for the microencapsulation of natural vanilla extract by spray drying</title><title>Cereal chemistry</title><description>Background and objectives
The aim of this study was to develop a wall material using rice starch (Oryza sativa) to optimize the microencapsulation of vanilla extract by spray drying. Native starch rice was hydrolyzed, succinated, extruded, and characterized.
Findings
The peak viscosity of modified starches was reduced from 3,875 cP to <100 cP by effect of the modification step. Native starch was gelatinized by extrusion according to gelatinization enthalpy (∆H J/g). Natural vanilla extract was encapsulated, and the most optimal conditions for the drying process were air inlet temperature of 125°C, 14.0% of total solids, and 86.2% of encapsulation efficiency. The scanning electron microscopy evidenced the formation of microcapsules; however, the confocal laser scanning microscopy showed no interaction between the wall material and the vanilla extract. This could be related to the zeta potential values of the vanilla extract and the wall material.
Conclusions
Modified rice starch is a potential wall material for the encapsulation of different bioactive compounds in the food sector.
Significance and novelty
Chemical and physical modifications such as hydrolysis, succinylation, and extrusion in native rice starch offer adequate properties to achieve 86.2% encapsulation efficiency of natural vanilla extract using spray drying.</description><subject>microencapsulation</subject><subject>modified starch</subject><subject>rice</subject><subject>spray drying</subject><subject>vanilla</subject><issn>0009-0352</issn><issn>1943-3638</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><recordid>eNp9kMtOwzAQRS0EEqWw4Qu8RgrYnjiJlygUilSJDayjSTqmRs5DTtqSvyclrFnNjHTm6uowdivFvRRCPVTVjqZNJeaMLaSJIYIEsnO2EEKYSIBWl-yq77-mE2QKC1Y-0YF829XUDLy1_Ije8xoHCg49t23gw4547arQUlNh1-89Dq5tTmyDwz5M1AEb5z1y-h4CVgMvR953AUe-DaNrPq_ZhUXf083fXLKP59V7vo42by-v-eMmqlQKJpJk0yQhEUtFujIQazAWSqkVKJPFmSq1pjJDnVmgbZIatFstpUzRGpAGYMnu5typa98HskUXXI1hLKQoTnaKk53i184Eyxk-Ok_jP2SR5-vV_PMDGv1oVQ</recordid><startdate>202005</startdate><enddate>202005</enddate><creator>Ocampo‐Salinas, Israel Oswaldo</creator><creator>Gómez‐Aldapa, Carlos Alberto</creator><creator>Castro‐Rosas, Javier</creator><creator>Vargas‐León, Enaim Aída</creator><creator>Guzmán‐Ortiz, Fabiola Araceli</creator><creator>Calcáneo‐Martínez, Netzahualcoyol</creator><creator>Falfán‐Cortés, Reyna Nallely</creator><scope>AAYXX</scope><scope>CITATION</scope><orcidid>https://orcid.org/0000-0002-5507-4889</orcidid><orcidid>https://orcid.org/0000-0002-7823-8954</orcidid><orcidid>https://orcid.org/0000-0003-1333-3624</orcidid><orcidid>https://orcid.org/0000-0003-3440-5981</orcidid><orcidid>https://orcid.org/0000-0003-2767-9896</orcidid><orcidid>https://orcid.org/0000-0002-4723-3093</orcidid><orcidid>https://orcid.org/0000-0002-6568-8454</orcidid></search><sort><creationdate>202005</creationdate><title>Development of wall material for the microencapsulation of natural vanilla extract by spray drying</title><author>Ocampo‐Salinas, Israel Oswaldo ; Gómez‐Aldapa, Carlos Alberto ; Castro‐Rosas, Javier ; Vargas‐León, Enaim Aída ; Guzmán‐Ortiz, Fabiola Araceli ; Calcáneo‐Martínez, Netzahualcoyol ; Falfán‐Cortés, Reyna Nallely</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c2739-1ef766e0412e5c934539f3b1523298482b55eb8a58f3ed679afd51117af931933</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>microencapsulation</topic><topic>modified starch</topic><topic>rice</topic><topic>spray drying</topic><topic>vanilla</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Ocampo‐Salinas, Israel Oswaldo</creatorcontrib><creatorcontrib>Gómez‐Aldapa, Carlos Alberto</creatorcontrib><creatorcontrib>Castro‐Rosas, Javier</creatorcontrib><creatorcontrib>Vargas‐León, Enaim Aída</creatorcontrib><creatorcontrib>Guzmán‐Ortiz, Fabiola Araceli</creatorcontrib><creatorcontrib>Calcáneo‐Martínez, Netzahualcoyol</creatorcontrib><creatorcontrib>Falfán‐Cortés, Reyna Nallely</creatorcontrib><collection>CrossRef</collection><jtitle>Cereal chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Ocampo‐Salinas, Israel Oswaldo</au><au>Gómez‐Aldapa, Carlos Alberto</au><au>Castro‐Rosas, Javier</au><au>Vargas‐León, Enaim Aída</au><au>Guzmán‐Ortiz, Fabiola Araceli</au><au>Calcáneo‐Martínez, Netzahualcoyol</au><au>Falfán‐Cortés, Reyna Nallely</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Development of wall material for the microencapsulation of natural vanilla extract by spray drying</atitle><jtitle>Cereal chemistry</jtitle><date>2020-05</date><risdate>2020</risdate><volume>97</volume><issue>3</issue><spage>555</spage><epage>565</epage><pages>555-565</pages><issn>0009-0352</issn><eissn>1943-3638</eissn><abstract>Background and objectives
The aim of this study was to develop a wall material using rice starch (Oryza sativa) to optimize the microencapsulation of vanilla extract by spray drying. Native starch rice was hydrolyzed, succinated, extruded, and characterized.
Findings
The peak viscosity of modified starches was reduced from 3,875 cP to <100 cP by effect of the modification step. Native starch was gelatinized by extrusion according to gelatinization enthalpy (∆H J/g). Natural vanilla extract was encapsulated, and the most optimal conditions for the drying process were air inlet temperature of 125°C, 14.0% of total solids, and 86.2% of encapsulation efficiency. The scanning electron microscopy evidenced the formation of microcapsules; however, the confocal laser scanning microscopy showed no interaction between the wall material and the vanilla extract. This could be related to the zeta potential values of the vanilla extract and the wall material.
Conclusions
Modified rice starch is a potential wall material for the encapsulation of different bioactive compounds in the food sector.
Significance and novelty
Chemical and physical modifications such as hydrolysis, succinylation, and extrusion in native rice starch offer adequate properties to achieve 86.2% encapsulation efficiency of natural vanilla extract using spray drying.</abstract><doi>10.1002/cche.10269</doi><tpages>11</tpages><orcidid>https://orcid.org/0000-0002-5507-4889</orcidid><orcidid>https://orcid.org/0000-0002-7823-8954</orcidid><orcidid>https://orcid.org/0000-0003-1333-3624</orcidid><orcidid>https://orcid.org/0000-0003-3440-5981</orcidid><orcidid>https://orcid.org/0000-0003-2767-9896</orcidid><orcidid>https://orcid.org/0000-0002-4723-3093</orcidid><orcidid>https://orcid.org/0000-0002-6568-8454</orcidid></addata></record> |
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| subjects | microencapsulation modified starch rice spray drying vanilla |
| title | Development of wall material for the microencapsulation of natural vanilla extract by spray drying |
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