The use of sodium tetraethylborate in the derivatization of octyltin compounds
Octyltin trichloride (OctSnCl3) and dioctyltin dichloride (Oct2SnCl2) have been reacted with sodium tetraethylborate (NaBEt4) to yield the volatile tetraalkyltin derivatives OctSnEt3 and Oct2SnEt2. Single and mixed solutions of the octyltin chlorides have been derivatized, separated and quantified u...
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Veröffentlicht in: | Applied organometallic chemistry 1994, Vol.8 (1), p.1-3 |
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description | Octyltin trichloride (OctSnCl3) and dioctyltin dichloride (Oct2SnCl2) have been reacted with sodium tetraethylborate (NaBEt4) to yield the volatile tetraalkyltin derivatives OctSnEt3 and Oct2SnEt2. Single and mixed solutions of the octyltin chlorides have been derivatized, separated and quantified using interfaced GC AA and GC MS methodology. |
doi_str_mv | 10.1002/aoc.590080102 |
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Single and mixed solutions of the octyltin chlorides have been derivatized, separated and quantified using interfaced GC AA and GC MS methodology.</description><identifier>ISSN: 0268-2605</identifier><identifier>EISSN: 1099-0739</identifier><identifier>DOI: 10.1002/aoc.590080102</identifier><identifier>CODEN: AOCHEX</identifier><language>eng</language><publisher>West Sussex: John Wiley & Sons, Ltd</publisher><subject>analysis ; Analytical chemistry ; Chemistry ; Chromatographic methods and physical methods associated with chromatography ; derivatization ; Exact sciences and technology ; Gas chromatographic methods ; GC AA ; GC MS ; Octyltin ; sodium tetrathylborate</subject><ispartof>Applied organometallic chemistry, 1994, Vol.8 (1), p.1-3</ispartof><rights>Copyright © 1994 John Wiley & Sons, Ltd.</rights><rights>1994 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c3522-51bb2e65cf3d29fa0673491c7c5b8c8987d156771cd2cd820ae1e102a552cf443</citedby><cites>FETCH-LOGICAL-c3522-51bb2e65cf3d29fa0673491c7c5b8c8987d156771cd2cd820ae1e102a552cf443</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Faoc.590080102$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Faoc.590080102$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,776,780,1411,4010,27902,27903,27904,45552,45553</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=3948103$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Craig, Peter J.</creatorcontrib><creatorcontrib>Mennie, Darren</creatorcontrib><title>The use of sodium tetraethylborate in the derivatization of octyltin compounds</title><title>Applied organometallic chemistry</title><addtitle>Appl. Organometal. Chem</addtitle><description>Octyltin trichloride (OctSnCl3) and dioctyltin dichloride (Oct2SnCl2) have been reacted with sodium tetraethylborate (NaBEt4) to yield the volatile tetraalkyltin derivatives OctSnEt3 and Oct2SnEt2. Single and mixed solutions of the octyltin chlorides have been derivatized, separated and quantified using interfaced GC AA and GC MS methodology.</description><subject>analysis</subject><subject>Analytical chemistry</subject><subject>Chemistry</subject><subject>Chromatographic methods and physical methods associated with chromatography</subject><subject>derivatization</subject><subject>Exact sciences and technology</subject><subject>Gas chromatographic methods</subject><subject>GC AA</subject><subject>GC MS</subject><subject>Octyltin</subject><subject>sodium tetrathylborate</subject><issn>0268-2605</issn><issn>1099-0739</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1994</creationdate><recordtype>article</recordtype><recordid>eNp9kDFPwzAQhS0EEqUwsmdgTTnbcRyPVQUFUbUDRUgsluM4qiGNK9sFwq8nVauKieF0w33v7t5D6BrDCAOQW-X0iAmAAjCQEzTAIEQKnIpTNACSFynJgZ2jixDeAUDkOBug-XJlkm0wiauT4Cq7XSfRRK9MXHVN6byKJrFtEnuqMt5-qmh_-nLtTuB07JrYj7Vbb9y2rcIlOqtVE8zVoQ_Ry_3dcvKQzhbTx8l4lmrKCEkZLkticqZrWhFRK8g5zQTWXLOy0IUoeIVZzjnWFdFVQUAZbHpTijGi6yyjQ5Tu92rvQvCmlhtv18p3EoPchSH7MOQxjJ6_2fMbFbRqaq9abcNRREVWYKA9xvfYl21M9_9OOV5M_h44PGRDNN9HpfIfsvfGmXydTyUH-rTM4Vm-0V_4rn7S</recordid><startdate>1994</startdate><enddate>1994</enddate><creator>Craig, Peter J.</creator><creator>Mennie, Darren</creator><general>John Wiley & Sons, Ltd</general><general>Wiley</general><scope>BSCLL</scope><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>1994</creationdate><title>The use of sodium tetraethylborate in the derivatization of octyltin compounds</title><author>Craig, Peter J. ; Mennie, Darren</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c3522-51bb2e65cf3d29fa0673491c7c5b8c8987d156771cd2cd820ae1e102a552cf443</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1994</creationdate><topic>analysis</topic><topic>Analytical chemistry</topic><topic>Chemistry</topic><topic>Chromatographic methods and physical methods associated with chromatography</topic><topic>derivatization</topic><topic>Exact sciences and technology</topic><topic>Gas chromatographic methods</topic><topic>GC AA</topic><topic>GC MS</topic><topic>Octyltin</topic><topic>sodium tetrathylborate</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Craig, Peter J.</creatorcontrib><creatorcontrib>Mennie, Darren</creatorcontrib><collection>Istex</collection><collection>Pascal-Francis</collection><collection>CrossRef</collection><jtitle>Applied organometallic chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Craig, Peter J.</au><au>Mennie, Darren</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>The use of sodium tetraethylborate in the derivatization of octyltin compounds</atitle><jtitle>Applied organometallic chemistry</jtitle><addtitle>Appl. Organometal. Chem</addtitle><date>1994</date><risdate>1994</risdate><volume>8</volume><issue>1</issue><spage>1</spage><epage>3</epage><pages>1-3</pages><issn>0268-2605</issn><eissn>1099-0739</eissn><coden>AOCHEX</coden><abstract>Octyltin trichloride (OctSnCl3) and dioctyltin dichloride (Oct2SnCl2) have been reacted with sodium tetraethylborate (NaBEt4) to yield the volatile tetraalkyltin derivatives OctSnEt3 and Oct2SnEt2. Single and mixed solutions of the octyltin chlorides have been derivatized, separated and quantified using interfaced GC AA and GC MS methodology.</abstract><cop>West Sussex</cop><pub>John Wiley & Sons, Ltd</pub><doi>10.1002/aoc.590080102</doi><tpages>3</tpages></addata></record> |
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subjects | analysis Analytical chemistry Chemistry Chromatographic methods and physical methods associated with chromatography derivatization Exact sciences and technology Gas chromatographic methods GC AA GC MS Octyltin sodium tetrathylborate |
title | The use of sodium tetraethylborate in the derivatization of octyltin compounds |
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