The use of sodium tetraethylborate in the derivatization of octyltin compounds

Octyltin trichloride (OctSnCl3) and dioctyltin dichloride (Oct2SnCl2) have been reacted with sodium tetraethylborate (NaBEt4) to yield the volatile tetraalkyltin derivatives OctSnEt3 and Oct2SnEt2. Single and mixed solutions of the octyltin chlorides have been derivatized, separated and quantified u...

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Veröffentlicht in:	Applied organometallic chemistry 1994, Vol.8 (1), p.1-3
Hauptverfasser:	Craig, Peter J., Mennie, Darren
Format:	Artikel
Sprache:	eng
Schlagworte:	analysis Analytical chemistry Chemistry Chromatographic methods and physical methods associated with chromatography derivatization Exact sciences and technology Gas chromatographic methods GC AA GC MS Octyltin sodium tetrathylborate
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Beschreibung
Zusammenfassung:	Octyltin trichloride (OctSnCl3) and dioctyltin dichloride (Oct2SnCl2) have been reacted with sodium tetraethylborate (NaBEt4) to yield the volatile tetraalkyltin derivatives OctSnEt3 and Oct2SnEt2. Single and mixed solutions of the octyltin chlorides have been derivatized, separated and quantified using interfaced GC AA and GC MS methodology.
ISSN:	0268-2605 1099-0739
DOI:	10.1002/aoc.590080102