First total synthesis of a naturally occurring nucleoside disulfide： 9-（5＇-Deoxy-51-thio-β-D-xylofuranosyl）adenine disulfide

First total synthesis of a naturally occurring nucleoside disulfide： 9-（5＇-Deoxy-51-thio-β-D-xylofuranosyl）adenine disulfide

A naturally occurring nucleoside disulfide, 9-（51-deoxy-5t-thio-β-D-xylofuranosyl）adenine disulfide, was first synthesized from o-xylose over 7 steps in 20% overall yield. The key step involved Vorbri.iggen glycosylation of silylated N6-benzoyladenine with xylose diacetate moiety.

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Veröffentlicht in:中国化学快报：英文版 2012, Vol.23 (9), p.996-998
1. Verfasser: Hai Xin Ding Ling Cui Da Ru Chun Yang Ban Peng Cao Qi Sun Qiang Xiao
Format: Artikel
Sprache:eng
Schlagworte:
二硫化物
呋喃
总合成
核苷
硫代
糖基化
腺嘌呤
自然
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creator Hai Xin Ding Ling Cui Da Ru Chun Yang Ban Peng Cao Qi Sun Qiang Xiao
description A naturally occurring nucleoside disulfide, 9-（51-deoxy-5t-thio-β-D-xylofuranosyl）adenine disulfide, was first synthesized from o-xylose over 7 steps in 20% overall yield. The key step involved Vorbri.iggen glycosylation of silylated N6-benzoyladenine with xylose diacetate moiety.
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1878-5964
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source ScienceDirect Journals (5 years ago - present); Alma/SFX Local Collection
subjects 二硫化物
呋喃
总合成
核苷
硫代
糖基化
腺嘌呤
自然
title First total synthesis of a naturally occurring nucleoside disulfide： 9-（5＇-Deoxy-51-thio-β-D-xylofuranosyl）adenine disulfide
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