Trace elements concentrations measured in bulk sediment samples collected during the IN2017-V01 voyage of the RV Investigator

Progress Code: completed | Statement: At least 2 standards and a blank were included in every digestion batch, which typically involved 24 samples. Samples were analysed in batches of 10 and bracketed by blanks and a Quality Control (Standard, 100 ppb). | Purpose These data were collected in order t...

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Hauptverfasser: Creac'h, L. and Noble, T, CREAC'H, LAYLA, NOBLE, TARYN L, TOWNSEND, ASHLEY T
Format: Dataset
Sprache:eng
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Zusammenfassung:Progress Code: completed | Statement: At least 2 standards and a blank were included in every digestion batch, which typically involved 24 samples. Samples were analysed in batches of 10 and bracketed by blanks and a Quality Control (Standard, 100 ppb). | Purpose These data were collected in order to determine sediment geochemistry and develop palaeoceanographic reconstructions. | Sediment cores were collected from the East Antarctic margin, aboard the Australian Marine National Facility R/V Investigator from January 14th to March 5th 2017 (IN2017_V01; Armand et al., 2018). This marine geoscience expedition, named the “Sabrina Sea Floor Survey”, focused notably on studying the interactions of the Totten Glacier with the Southern Ocean through multiple glacial cycles. The cores were collected using a multi-corer (MC) and a Kasten corer (KC). The MC were sliced every centimetre, wrapped up in plastic bags, and stored in the fridge. The KC was sub-sampled using an u-channel; and sliced every centimetre once back the home laboratory (IMAS, UTAS, Hobart, Australia). This dataset presents concentrations of major and trace elements measured in bulk multi-cores sediment samples collected during the IN2017_V01 voyage. The data include the sampling date (day/month/year), the latitude and longitude (in decimal degrees), the seafloor depth (in meter), the sediment core ID, the sediment depth (in cm), and the concentrations (in ppm or μg/g) of a suite of elements. This dataset presents concentrations of major and trace elements measured in bulk sediment samples collected during the IN2017_V01 voyage. The data include the sampling date (day/month/year), the latitude and longitude (in decimal degrees), the seafloor depth (in meter), the sediment core ID (KC14), the sediment depth (in cm), and the concentrations (in ppm or μg/g) of a suite of elements. About 200 mg of dried and ground sediment were weighed into a clean Teflon vial and oxidized with a mixture of concentrated HNO3 and 30% H2O2 (1:1). Samples were then digested in open vials using an acid mixture comprising 10 mL HNO3, 4 mL HCl, and 2 mL HF, at 180°C until close to dryness. Digested residues were converted to nitric form before being oxidised with a mixture of 1 mL HNO3 and 1 mL HClO4 at 220°C until fully desiccated. Samples were finally re-dissolved in 4 mL 7.5 M HNO3. A 400 μL aliquot was removed from the 4 mL digest solution and diluted ~2500 times in 2% HNO3 for trace metals analysis by Sector Field Indu