Organometallic chemistry in industry a practical approach
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| 245 | 1 | 0 | |a Organometallic chemistry in industry |b a practical approach |c edited by Thomas J. Colacot, Carin C. C. Johansson Seechurn ; with a foreword by Robert H. Grubbs |
| 264 | 1 | |a Weinheim |b Wiley-VCH |c [2020] | |
| 264 | 4 | |c © 2020 | |
| 300 | |a xix, 315 Seiten |b Illustrationen, Diagramme (teilweise farbig) | ||
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| 650 | 0 | 7 | |a Metallorganische Verbindungen |0 (DE-588)4038906-6 |2 gnd |9 rswk-swf |
| 653 | |a 1654: Hardcover, Softcover / Chemie/Organische Chemie | ||
| 653 | |a CG03: Katalyse u. Chemische Reaktionstechnik | ||
| 653 | |a CH30: Technische u. Industrielle Chemie | ||
| 653 | |a CH86: Organometallchemie | ||
| 653 | |a Catalysis & Chemical Reaction Engineering | ||
| 653 | |a Chemical Engineering | ||
| 653 | |a Chemie | ||
| 653 | |a Chemische Verfahrenstechnik | ||
| 653 | |a Chemistry | ||
| 653 | |a Hardback | ||
| 653 | |a Industrial Chemistry | ||
| 653 | |a Katalyse u. Chemische Reaktionstechnik | ||
| 653 | |a Organometallchemie | ||
| 653 | |a Organometallic Chemistry | ||
| 653 | |a Technische u. Industrielle Chemie | ||
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| 689 | 0 | 0 | |a Metallorganische Verbindungen |0 (DE-588)4038906-6 |D s |
| 689 | 0 | |8 1\p |5 DE-604 | |
| 700 | 1 | |a Colacot, Thomas J. |0 (DE-588)1098434447 |4 edt | |
| 700 | 1 | |a Johansson Seechurn, Carin C.C. |0 (DE-588)1209895951 |4 edt | |
| 700 | 1 | |a Grubbs, Robert H. |d 1942-2021 |0 (DE-588)124993532 |4 wpr | |
| 710 | 2 | |a Wiley-VCH |0 (DE-588)16179388-5 |4 pbl | |
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Datensatz im Suchindex
| _version_ | 1819778139430060032 |
|---|---|
| adam_text | CONTENTS
FOREWORD
XIII
PREFACE
XVII
1
INDUSTRIAL
MILESTONES
IN
ORGANOMETALLIC
CHEMISTRY
1
BEN
M.
GARDNER,
GARIN
C.C.
JOHANSSON
SEECHURN,
AND
THOMAS
J.
COLACOT
1.1
DEFINITION
OF
ORGANOMETALLIC
AND
METAL-ORGANIC
COMPOUNDS
1
1.1.1
APPLICATIONS
AND
KEY
REACTIVITY
1
1.1.1.1
ELECTRONIC
APPLICATIONS
1
1.1.1.2
POLYMERS
2
1.1.1.3
ORGANIC
SYNTHESIS
2
1.2
INDUSTRIAL
PROCESS
CONSIDERATIONS
7
1.3
BRIEF
NOTES
ON
THE
HISTORICAL
DEVELOPMENT
OF
ORGANOMETALLIC
CHEMISTRY
FOR
ORGANIC
SYNTHESIS
APPLICATIONS
PERTAINING
TO
THE
CONTENTS
OF
THIS
BOOK
8
1.3.1
SYNTHESIS
OF
STOICHIOMETRIC
ORGANOMETALLIC
REAGENTS
9
1.3.1.1
CONVENTIONAL
BATCH
SYNTHESIS
9
1.3.1.2
ORGANOMETALLICS
IN
FLOW
10
1.3.2
CROSS-COUPLING
REACTIONS
10
1.3.2.1
C
*
H
BOND
ACTIVATION
12
1.3.2.2
CARBONYLATION
13
1.3.2.3
CATALYSIS
IN
WATER
-
MICELLAR
CATALYSIS
13
1.3.3
HYDROGENATION
REACTIONS
14
1.3.4
OLEFIN
FORMATION
REACTIONS
IS
1.3.4.1
WITTIG
REACTION
IS
1.3.4.2
METATHESIS
REACTIONS
IS
1.3.4.3
DEHYDRATIVE
DECARBONYLATION
16
1.3.4.4
OLEFINS
AS
STARTING
MATERIALS
16
1.3.5
POLY-OR
OLIGOMERIZATION
PROCESSES
17
1.3.6
PHOTOREDOX
CATALYSIS
FOR
ORGANIC
SYNTHESIS
17
1.4
CONCLUSION
AND
OUTLOOK
17
BIOGRAPHY
18
REFERENCES
19
VI
CONTENTS
2
DESIGN,
DEVELOPMENT,
AND
EXECUTION
OF
A
CONTINUOUS-FLOW-ENABLED
API
MANUFACTURING
ROUTE
23
ALISON
C
BREWER,
PHILIP
C.
HOFFMAN,
TIMOTHY
D.
WHITE,
YU
LU,
LAURA
MCKEE,
MOUSSA
BOUKERCHE,
MICHAEL
E.
KOBIERSKI,
NESSA
MULLANE,
MARK
PIETZ,
CHARLES
A.
ALT,
JIM
R.
STOUT,
PAUL
K.
MILENBAUGH,
AND
JOSEPH
R.
MARTINELLI
2.1
CONTINUOUS-FLOW-ENABLED
SYNTHETIC
STRATEGY
25
2.2
DESIGN
AND
SCALE-UP
OF
CHAN-LAM
COUPLING
28
2.2.1
DEVELOPMENT
OF
HOMOGENEOUS
CONDITIONS
31
2.2.2
APPLICATION
OF
A
PLATFORM
TECHNOLOGY
TO
AEROBIC
OXIDATION
32
2.2.3
OPTIMIZATION
OF
REACTION
AND
WORKUP
PARAMETERS
35
2.2.4
SAFETY
CONSIDERATIONS
FOR
AEROBIC
OXIDATION ON
SCALE
37
2.2.5
CONTINUOUS
SCALE-UP
AND
MANUFACTURING
38
2.3
DESIGN
AND
SCALE-UP
OF
A
BUCHWALD-HARTWIG
CROSS-COUPLING
42
2.3.1
INITIAL
SCREENING
43
2.3.2
SYNTHESIS
AND
ISOLATION
OF
PD(DBA)DPEPHOS
PRECATALYST
45
2.3.3
WORKUP
PROCEDURE,
METAL
REMOVAL,
AND
CRYSTALLIZATION
46
2.3.4
SCALE-UP
AND
MANUFACTURING
48
2.4
IMPURITY
CONTROL
48
2.4.1
SOLUBILITY
AND
IMPURITY
SPIKING
STUDIES
50
2.5
CONCLUSIONS
54
BIOGRAPHY
54
REFERENCES
58
3
CONTINUOUS
MANUFACTURING
AS
AN
ENABLING
TECHNOLOGY
FOR
LOW-TEMPERATURE
ORGANOMETALLIC
CHEMISTRY
61
ANDREAS
HAFNER
AND
JOERG
SEDELMEIER
3.1
INTRODUCTION
61
3.2
ORGANO-LI
AND
MG
PROCESSES
IN
FLOW
MODE
62
3.2.1
TECHNOLOGICAL
ADVANTAGES
OF
FLOW
TECHNOLOGY
COMPARED
TO
TRADITIONAL
BATCH
OPERATION
62
3.2.2
TEMPERATURE
PROFILE
OF
CONTINUOUS
FLOW
REACTIONS
64
3.2.3
FLASH
CHEMISTRY:
FUNCTIONAL
GROUP
TOLERANCE
65
3.2.4
FLASH
CHEMISTRY:
SELECTIVITY
66
3.2.5
FLASH
CHEMISTRY:
STOICHIOMETRY
AND
CHEMOSELECTIVITY
67
3.3
CONTINUOUS
FLOW
TECHNOLOGY
69
3.3.1
CLOGGING
AS
A
MAJOR
HURDLE
IN
FLOW
CHEMISTRY
71
3.3.2
START-UP
AND
SHUTDOWN
OPERATION
72
3.3.3
MATERIAL
OF
CONSTRUCTION
72
3.3.4
SAFETY
CONCEPT
AND
EMERGENCY
STRATEGIES
73
3.4
DEVELOPMENT
OF
A
FLOW
PROCESS
73
3.4.1
SCREENING
PHASE:
FEASIBILITY
STUDY
74
3.4.2
PROCESS
DEVELOPMENT
PHASE:
EXTENDED
EVALUATIONS
INCLUDING
TECHNICAL
FEASIBILITY
75
3.5
LITERATURE
EXAMPLES:
FLOW
PROCESSES
ON
MULTI
100
G
SCALE
76
3.5.1
MANUFACTURE
OF
VERUBECESTAT
(MK-8931)
77
3.5.2
MANUFACTURE
OF
EDIVOXETINE
77
3.5.3
SCALE-UP
OF
HIGHLY
REACTIVE
ARYL
LITHIUM
CHEMISTRY
80
CONTENTS
VII
3.5.4
SYNTHESIS
OF
BROMOMETHYLTRIFLUOROBORATES
IN
CONTINUOUS
FLOW
MODE
81
3.5.5
TWO-STEP
SYNTHESIS
TOWARD
BORONIC
ACIDS
82
3.5.6
REACTION
SEQUENCE
TOWARD
A
HIGHLY
SUBSTITUTED
BENZOXAZOLE
BUILDING
BLOCK
84
3.6
CONCLUSION
AND
FUTURE
PROSPECTS
86
BIOGRAPHY
86
REFERENCES
87
4
DEVELOPMENT
OF
A
NICKEL-CATALYZED
ENANTIOSELECTIVE
MIZOROKI-HECK
COUPLING
91
JEAN-NICOLAS
DESROSIERS
AND
CHRIS
H.
SENANAYAKE
4.1
INTRODUCTION
91
4.1.1
NONPRECIOUS
METAL
CATALYSIS
ADVANTAGES
FOR
INDUSTRY
91
4.1.2
MIZOROKI-HECK
COUPLINGS
IN
INDUSTRY
WITH
PALLADIUM
92
4.1.3
EMERGENCE
OF
NICKEL-CATALYZED
MIZOROKI-HECK
COUPLINGS
93
4.1.4
ENANTIOSELECTIVE
NICKEL-CATALYZED
COUPLINGS
94
4.1.5
SYNTHESIS
OF
OXINDOLES
VIA
MIZOROKI-HECK
CYCLIZATIONS
96
4.2
DEVELOPMENT
OF
A
NICKEL-CATALYZED
HECK
CYCLIZATION
TO
GENERATE
OXINDOLES
WITH
QUATERNARY
STEREOGENIC
CENTERS
97
4.2.1
PRECEDENTS
AND
CHALLENGES
97
4.2.2
OPTIMIZATION
OF
REDUCING
AGENT
AND
BASE
97
4.2.3
LIGAND
SCREENING
98
4.2.4
IMPACT
OF
ARYL
ELECTROPHILE
AND
OF
STEREOCHEMISTRY
OF
ALKENE
MOIETY
100
4.2.5
EXPLORATION
OF
THE
SUBSTRATE
SCOPE
102
4.2.6
LIMITATIONS
OF
THE
METHODOLOGY
104
4.2.7
MECHANISTIC
CONSIDERATIONS
104
4.3
DEVELOPMENT
OF
FIRST
ENANTIOSELECTIVE
NICKEL-CATALYZED
HECK
COUPLING
107
4.3.1
LIGAND
SCREENING
107
4.3.2
IMPACT
OF
ALKENE
STEREOCHEMISTRY
107
4.3.3
NEUTRAL
VS
CATIONIC
PATHWAYS
108
4.3.4
NICKEL
PRECATALYST
COMPLEX
SYNTHESIS
109
4.3.5
EXPLORATION
OF
THE
SUBSTRATE
SCOPE
110
4.3.6
MECHANISTIC
STUDIES
110
4.4
CONCLUSIONS
113
BIOGRAPHY
114
REFERENCES
115
5
DEVELOPMENT
OF
IRON-CATALYZED
KUMADA
CROSS-COUPLING
FOR
THE
LARGE-SCALE
PRODUCTION
OF
ALISKIREN
INTERMEDIATE
121
SRINIVAS
ACHANTA,
DEBJIT
BASU,
UDAYK.
NEEL
AM,
RAJEEVR.
BUDHDEV,
APURBA
BHATTACHARYA,
AND
RAKESHWAR
BANDICHHOR
5.1
INTRODUCTION
121
5.2
OPTIMIZATION
OF
GRADE
AND
EQUIVALENTS
OF
MG
METAL
123
VII
I
CONTENTS
5.3
5.4
OPTIMIZATION
OF
EQUIVALENTS
OF
1,2-DIBROMOETHANE
123
EFFECT
OF
SOLVENT
CONCENTRATION
ON
PREPARATION
OF
GRIGNARD
REAGENT
AND
KUMADA-CORRIU
COUPLING
124
5.5
EFFECT
OF
ALKYL
CHLORIDE
3
ADDITION
TIME
ON
THE
GRIGNARD
REAGENT
PREPARATION
125
5.6
5.7
5.8
5.9
STABILITY
OF
GRIGNARD
REAGENT
AT
0-5
C
125
IRON-CATALYZED
CROSS-COUPLING REACTION
127
OPTIMIZATION
OF
EQUIVALENTS
OF
NMP
AND
FE(ACAC)
3
129
OPTIMIZATION
OF
EQUIVALENTS
OF
SUBSTRATE
4
AND
ITS
RATE
OF
ADDITION
129
5.10
5.11
5.12
EXECUTION
AT
PILOT
SCALE
AND
SCALE-UP
ISSUES
129
AGITATED
THIN
FILM
EVAPORATOR
(ATFE)
FOR
PURIFICATION
OF
2
131
CONCLUSION
132
ACKNOWLEDGMENTS
133
BIOGRAPHY
133
REFERENCES
135
6
DEVELOPMENT
AND
SCALE-UP
OF
A
PALLADIUM-CATALYZED
INTRAMOLECULAR
DIRECT
ARYLATION
IN
THE
COMMERCIAL
SYNTHESIS
OF
BECLABUVIR
137
COLLIN
CHAN,
ALBERT
J.
DEL
MONTE,
CHAO
HANG,
YI
HSIAO,
AND
ERIC
M.
SIMMONS
6.1
6.2
6.3
6.4
6.4.1
6.4.2
INTRODUCTION
137
KO
AC/DM
AC
PROCESS
141
TMAOAC/DMF
PROCESS
141
TMAOAC/DMAC
PROCESS
149
CYCLIZATION
REACTION
151
MECHANISTIC
UNDERSTANDING
OF
THE
CYCLIZATION
REACTION
AND
IMPURITY
FORMATION
159
6.4.3
6.4.4
6.5
HYDROLYSIS
AND
WORKUP
162
CRYSTALLIZATION
AND
DRYING
164
CONCLUSION
167
BIOGRAPHY
168
REFERENCES
169
7
RUTHENIUM-CATALYZED
C
*
H
ACTIVATED
C
*
C/N/O
BOND
FORMATION
REACTIONS
FOR
THE
PRACTICAL
SYNTHESIS
OF
HETEROCYCLES
AND
PHARMACEUTICAL
AGENTS
171
ANITA
MEHTA,
NARESH
KUMAR,
AND
BISWAJIT
SAHA
7.1
7.2
7.2.1
INTRODUCTION
171
C-H
ACTIVATION
FOLLOWED
BY
C
*
C
BOND
FORMATION
172
C-H
ACTIVATION
FOLLOWED
BY
C
*
C
BOND
FORMATION:
BIARYL/HETEROBIARYL
SYNTHESIS
IN
ORGANIC
SOLVENTS
172
7.2.2
C-H
ACTIVATION
FOLLOWED
BY
C
*
C
BOND
FORMATION:
BIARYL/HETEROBIARYL
SYNTHESIS
IN
GREEN
SOLVENTS
181
7.3
ALKYL/ACYL/ALKENYL
SUBSTITUTION
ON
HETEROCYCLES
185
CONTENTS
IX
7.4
C-H
ACTIVATION
FOLLOWED
BY
C
*
O/N
BOND
FORMATION:
HETEROCYCLE
SYNTHESIS
187
7.4.1
C-H
ACTIVATION
FOLLOWED
BY
C
*
O/N
BOND
FORMATION:
HETEROCYCLE
SYNTHESIS
IN
ORGANIC
SOLVENTS
187
7.4.2
C-H
ACTIVATION
FOLLOWED
BY
C
*
O
AND
C
*
N
BOND
FORMATION:
HETEROCYCLE
SYNTHESIS
IN
GREEN
SOLVENTS
189
7.5
CONCLUSION
196
BIOGRAPHY
197
REFERENCES
198
8
CROSS-COUPLINGS
IN
WATER
-
A
BETTER
WAY
TO
ASSEMBLE
NEW
BONDS
203
THARIQUE
N.
ANSARI,
FABRICS
GALLOU,
AND
SACHIN
HANDA
8.1
8.2
INTRODUCTION
203
TRANSITION
METAL
CATALYSIS
IN
ORGANIC
SOLVENTS
VS
MICELLAR
CATALYSIS
204
8.2.1
8.2.2
MICELLIZATION
20S
SURFACTANT
SOLUTION
-
A
HIGHLY
ORGANIZED
REACTION
MEDIUM
TO
ENHANCE
REACTION
RATE
206
8.2.3
8.2.4
8.2.5
8.2.6
8.2.7
8.2.8
8.2.9
8.3
8.3.1
8.3.2
8.3.3
8.3.4
8.3.5
8.3.6
8.3.7
8.3.8
8.4
REACTION
TEMPERATURE
207
SIZE
OF
MICELLES
207
NATURE
OF
CATALYST
208
INCREASING
THE
EFFICIENCY
IN
MICELLAR
CATALYSIS
209
ORDER
OF
ADDITION
210
PRODUCT
PRECIPITATION OR
EXTRACTION
211
TRACE
METAL
IN
THE
PRODUCT
211
HIGHLY
VALUABLE
REACTIONS
IN
WATER
212
SUZUKI-MIYAURA
COUPLINGS
212
HECK
COUPLINGS
217
NEGISHI
COUPLINGS
219
C-H
ARYLATIONS
221
AMINATIONS
225
BORYLATION
228
ARYLATION
OF
NITRO
COMPOUNDS
228
ADOPTION
OF
MICELLAR
TECHNOLOGY
BY
PHARMACEUTICAL
INDUSTRY
229
CONCLUSIONS
234
BIOGRAPHY
234
REFERENCES
235
9
ASPECTS
OF
HOMOGENEOUS
HYDROGENATION
FROM
INDUSTRIAL
RESEARCH
239
STEPHEN
ROSEBLADE
9.1
9.2
9.3
HOMOGENEOUS
HYDROGENATION:
A
BRIEF
INTRODUCTION
239
CATALYST
SELECTION
BY
EFFECTIVE
SCREENING
APPROACHES
240
CONSIDERATIONS
FOR
REACTION
SCALE-UP
244
X
I
CONTENTS
9.4
9.5
NOTES ON
ADDITIVE
EFFECTS
247
A
NOVEL
APPROACH
TO
ALISKIREN
USING
ASYMMETRIC
HYDROGENATION
AS
A
KEY
STEP
249
9.6
9.7
EFFICIENT
CHEMOSELECTIVE
ALDEHYDE
HYDROGENATION
252
CLOSING
REMARKS/SUMMARY
253
BIOGRAPHY
255
REFERENCES
255
10
LATEST
INDUSTRIAL
USES
OF
OLEFIN
METATHESIS
259
JOHN
H.
PHILLIPS
10.1
10.2
10.2.1
10.2.2
10.3
10.3.1
10.3.2
10.3.3
10.4
10.4.1
10.4.2
10.4.3
10.4.4
10.4.5
10.4.6
10.5
10.5.1
10.5.2
10.5.3
10.5.4
10.6
INTRODUCTION
259
GENERAL
INFORMATION
260
NON-RUTHENIUM
CATALYSTS
260
RUTHENIUM
CATALYSTS
261
INDUSTRIAL
USES
262
RING-CLOSING
METATHESIS
(RCM)
262
CROSS-METATHESIS
(CM)
264
RING-OPENING
METATHESIS
POLYMERIZATION
(ROMP)
268
REACTION
CONSIDERATIONS
270
CATALYST
CHOICE
271
CATALYST
LOADING
273
SOLVENT
273
REACTION
CONCENTRATION
273
OVERALL
HANDLING
274
APPLICATION
GUIDE
AND
AVAILABILITY
274
TROUBLESHOOTING
275
CATALYST
REMOVAL
275
FUNCTIONAL
GROUP
TOLERANCE
276
SUBSTRATE PURITY
276
CATALYST
DECOMPOSITION
-
ISOMERIZATION
277
CONCLUSION
277
BIOGRAPHY
277
REFERENCES
278
11
DEHYDRATIVE
DECARBONYLATION
283
ALEX
JOHN
11.1
11.2
11.3
11.3.1
11.3.2
11.4
11.4.1
11.4.2
11.5
11.6
11.7
INTRODUCTION
283
USE
OF
SACRIFICIAL
ANHYDRIDE
AND
CATALYTIC
MECHANISM
285
RH-
PD-
AND
IR-CATALYSIS
286
EARLY
STUDIES
286
RECENT
STUDIES
289
MILDER
TEMPERATURES
291
PDCL
2
/XANTPHOS/(
F
BU)
4
BIPHENOL
SYSTEM
291
WELL-DEFINED
PD-BIS(PHOSPHINE)
PRECATALYSTS
294
NICKEL
AND
IRON
CATALYSIS
295
ESTER
DECARBONYLATION
297
SYNTHETIC
UTILITY:
A-VINYL
CARBONYL
COMPOUNDS
299
11.8
CONCLUSIONS
AND
FUTURE
PROSPECTS
300
BIOGRAPHY
300
REFERENCES
301
INDEX
305
CONTENTS
XI
|
| any_adam_object | 1 |
| author2 | Colacot, Thomas J. Johansson Seechurn, Carin C.C |
| author2_role | edt edt |
| author2_variant | t j c tj tjc s c c j scc sccj |
| author_GND | (DE-588)1098434447 (DE-588)1209895951 (DE-588)124993532 |
| author_facet | Colacot, Thomas J. Johansson Seechurn, Carin C.C |
| building | Verbundindex |
| bvnumber | BV046622941 |
| classification_rvk | VH 9700 VN 6000 |
| ctrlnum | (OCoLC)1164650361 (DE-599)DNB1193020352 |
| discipline | Chemie / Pharmazie |
| format | Book |
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| genre | (DE-588)4143413-4 Aufsatzsammlung gnd-content |
| genre_facet | Aufsatzsammlung |
| id | DE-604.BV046622941 |
| illustrated | Illustrated |
| indexdate | 2024-12-24T08:09:25Z |
| institution | BVB |
| institution_GND | (DE-588)16179388-5 |
| isbn | 9783527345175 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-032034629 |
| oclc_num | 1164650361 |
| open_access_boolean | |
| owner | DE-29T DE-11 |
| owner_facet | DE-29T DE-11 |
| physical | xix, 315 Seiten Illustrationen, Diagramme (teilweise farbig) |
| publishDate | 2020 |
| publishDateSearch | 2020 |
| publishDateSort | 2020 |
| publisher | Wiley-VCH |
| record_format | marc |
| spellingShingle | Organometallic chemistry in industry a practical approach Metallorganische Verbindungen (DE-588)4038906-6 gnd |
| subject_GND | (DE-588)4038906-6 (DE-588)4143413-4 |
| title | Organometallic chemistry in industry a practical approach |
| title_auth | Organometallic chemistry in industry a practical approach |
| title_exact_search | Organometallic chemistry in industry a practical approach |
| title_full | Organometallic chemistry in industry a practical approach edited by Thomas J. Colacot, Carin C. C. Johansson Seechurn ; with a foreword by Robert H. Grubbs |
| title_fullStr | Organometallic chemistry in industry a practical approach edited by Thomas J. Colacot, Carin C. C. Johansson Seechurn ; with a foreword by Robert H. Grubbs |
| title_full_unstemmed | Organometallic chemistry in industry a practical approach edited by Thomas J. Colacot, Carin C. C. Johansson Seechurn ; with a foreword by Robert H. Grubbs |
| title_short | Organometallic chemistry in industry |
| title_sort | organometallic chemistry in industry a practical approach |
| title_sub | a practical approach |
| topic | Metallorganische Verbindungen (DE-588)4038906-6 gnd |
| topic_facet | Metallorganische Verbindungen Aufsatzsammlung |
| url | http://www.wiley-vch.de/publish/dt/books/ISBN978-3-527-34517-5/ http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=032034629&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=032034629&sequence=000003&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA |
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