Crystal Structure Determination
To solve a crystal structure means to determine the precise spatial arrangements of all of the atoms in a chemical compound in the crystalline state. This knowledge gives a chemist access to a large range of information, induding connectivity, conformation, and accurate bond lengths and angles. In a...
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| 520 | |a To solve a crystal structure means to determine the precise spatial arrangements of all of the atoms in a chemical compound in the crystalline state. This knowledge gives a chemist access to a large range of information, induding connectivity, conformation, and accurate bond lengths and angles. In addition, it implies the stoichiometry, the density, the symmetry and the three dimensional packing of the atoms in the solid. Since interatomic distances are in the region of 100-300 pm or 1-3 A, I microscopy using visible light ( wavelength Je ca. 300-700 nm) is not applicable (Fig. l. l). In 1912, Max von Laue showed that crystals are based on a three dimensional lattice which scatters radiation with a wavelength in the vicinity of interatomic distances, i. e. X -rays with Je = 50-300 pm. The process by wh ich this radiation, without changing its wave length, is converted through interference by the lattice to a vast number of observable "reflections" with characteristic directions in space is called X-ray diffraction. The method by which the directions and the intensities of these reflections are measured, and the ordering of the atoms in the crystal deduced from them, is called X -ray struc ture analysis. The following chapter deals with the lattice properties of crystals, the starting point for the explanation of these interference phenomena. Interatomic distances Crystals . . . . . . . . . | ||
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Datensatz im Suchindex
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| author | Massa, Werner |
| author_facet | Massa, Werner |
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| discipline | Chemie / Pharmazie Physik |
| doi_str_mv | 10.1007/978-3-662-04248-9 |
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| spelling | Massa, Werner Verfasser aut Crystal Structure Determination by Werner Massa Berlin, Heidelberg Springer Berlin Heidelberg 2000 1 Online-Ressource (XI, 206 p) txt rdacontent c rdamedia cr rdacarrier To solve a crystal structure means to determine the precise spatial arrangements of all of the atoms in a chemical compound in the crystalline state. This knowledge gives a chemist access to a large range of information, induding connectivity, conformation, and accurate bond lengths and angles. In addition, it implies the stoichiometry, the density, the symmetry and the three dimensional packing of the atoms in the solid. Since interatomic distances are in the region of 100-300 pm or 1-3 A, I microscopy using visible light ( wavelength Je ca. 300-700 nm) is not applicable (Fig. l. l). In 1912, Max von Laue showed that crystals are based on a three dimensional lattice which scatters radiation with a wavelength in the vicinity of interatomic distances, i. e. X -rays with Je = 50-300 pm. The process by wh ich this radiation, without changing its wave length, is converted through interference by the lattice to a vast number of observable "reflections" with characteristic directions in space is called X-ray diffraction. The method by which the directions and the intensities of these reflections are measured, and the ordering of the atoms in the crystal deduced from them, is called X -ray struc ture analysis. The following chapter deals with the lattice properties of crystals, the starting point for the explanation of these interference phenomena. Interatomic distances Crystals . . . . . . . . . Chemistry Inorganic Chemistry Organic Chemistry Geochemistry Mineralogy Physics, general Inorganic chemistry Organic chemistry Physics Röntgenstrukturanalyse (DE-588)4137203-7 gnd rswk-swf Kristallstrukturanalyse (DE-588)4137204-9 gnd rswk-swf Kristallstruktur (DE-588)4136176-3 gnd rswk-swf 1\p (DE-588)4123623-3 Lehrbuch gnd-content Röntgenstrukturanalyse (DE-588)4137203-7 s 2\p DE-604 Kristallstrukturanalyse (DE-588)4137204-9 s 3\p DE-604 Kristallstruktur (DE-588)4136176-3 s 4\p DE-604 Erscheint auch als Druck-Ausgabe 9783540659709 https://doi.org/10.1007/978-3-662-04248-9 Verlag URL des Erstveröffentlichers Volltext 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 2\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 3\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 4\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Massa, Werner Crystal Structure Determination Chemistry Inorganic Chemistry Organic Chemistry Geochemistry Mineralogy Physics, general Inorganic chemistry Organic chemistry Physics Röntgenstrukturanalyse (DE-588)4137203-7 gnd Kristallstrukturanalyse (DE-588)4137204-9 gnd Kristallstruktur (DE-588)4136176-3 gnd |
| subject_GND | (DE-588)4137203-7 (DE-588)4137204-9 (DE-588)4136176-3 (DE-588)4123623-3 |
| title | Crystal Structure Determination |
| title_auth | Crystal Structure Determination |
| title_exact_search | Crystal Structure Determination |
| title_full | Crystal Structure Determination by Werner Massa |
| title_fullStr | Crystal Structure Determination by Werner Massa |
| title_full_unstemmed | Crystal Structure Determination by Werner Massa |
| title_short | Crystal Structure Determination |
| title_sort | crystal structure determination |
| topic | Chemistry Inorganic Chemistry Organic Chemistry Geochemistry Mineralogy Physics, general Inorganic chemistry Organic chemistry Physics Röntgenstrukturanalyse (DE-588)4137203-7 gnd Kristallstrukturanalyse (DE-588)4137204-9 gnd Kristallstruktur (DE-588)4136176-3 gnd |
| topic_facet | Chemistry Inorganic Chemistry Organic Chemistry Geochemistry Mineralogy Physics, general Inorganic chemistry Organic chemistry Physics Röntgenstrukturanalyse Kristallstrukturanalyse Kristallstruktur Lehrbuch |
| url | https://doi.org/10.1007/978-3-662-04248-9 |
| work_keys_str_mv | AT massawerner crystalstructuredetermination |