Temperature-responsive polymers chemistry, properties, and applications
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| 245 | 1 | 0 | |a Temperature-responsive polymers |b chemistry, properties, and applications |c edited by Vitaliy Khutoryanskiy (University of Reading, UK), Theoni K. Georgiou (Imperial College London, UK) |
| 264 | 1 | |a Hoboken, NJ |b Wiley |c 2018 | |
| 300 | |a xxii, 384 Seiten |b Illustrationen, Diagramme | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 650 | 0 | 7 | |a Thermoresponsive Polymere |0 (DE-588)1118761898 |2 gnd |9 rswk-swf |
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| 700 | 1 | |a Khutoryanskiy, Vitaliy V. |4 edt | |
| 700 | 1 | |a Georgiou, Theoni K. |0 (DE-588)1168598834 |4 edt | |
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Datensatz im Suchindex
| _version_ | 1819703322835156992 |
|---|---|
| adam_text | Contents
About the Editors xiii
List of Contributors xv
Preface xix
Part I Chemistry 1
1 Poly(AMsopropylacrylamide): Physicochemical Properties and
Biomedical Applications 3
Marzieh Najafi, Erik Hebels, Wim E. Hennink, and Tina Vermonden
1.1 Introduction 3
1.2 PNIPAM as Thermosensitive Polymer 4
1.3 Physical Properties of PNIPAM 5
1.3.1 Phase Behavior of PNIPAM in Water/Alcohol Mixtures 5
1.3.2 Effect of Concentration and Molecular Weight of PNIPAM on LCST 5
1.3.3 Effect of Surfactants on LCST 7
1.3.4 Effect of Salts on LCST 7
1.4 Common Methods for Polymerization of NIPAM 8
1.4.1 Free Radical Polymerization 8
1.4.2 Living Radical Polymerization 9
1.4.2.1 ATRP of NIPAM 10
1.4.2.2 RAFT Polymerization of NIPAM 11
1.5 Dual Sensitive Systems 12
1.5.1 pH and Thermosensitive Systems 12
1.5.2 Reduction-Sensitive and Thermosensitive Systems 13
1.5.3 Hybrid-Thermosensitive Materials 13
1.6 Bioconjugation of PNIPAM 15
1.6.1 Protein-PNIPAM Conjugates 16
1.6.2 Peptide-PNIPAM Conjugates 18
1.6.3 Nucleic Acid-PNIPAM Conjugates 21
1.7 Liposome Surface Modification with PNIPAM 21
1.8 Applications of PNIPAM in Cell Culture 22
1.9 Crosslinking Methods for Polymers 23
1.9.1 Crosslinking in PNIPAM-Based Hydrogels 23
1.9.2 Crosslinking of PNIPAM-Based Micelles 26
vi j Contents
1.9.2.1 Shell Crosslinked (SCL) 26
1.9.2.2 Core Crosslinked (CCL) 27
1.10 Conclusion and Outlook of Applications of PNIPAM 27
Acknowledgments 28
References 28
2 Thermoresponsive Multiblock Copolymers: Chemistry, Properties and
Applications 35
Anno P. Constontinou and Theoni K. Georgiou
2.1 Introduction 35
2.2 Chemistry of Thermoresponsive Block-based Copolymers 35
2.3 Architecture, Number of Blocks and Block Sequence 38
2.3.1 Why the Block Structure? 38
2.3.2 Triblock Copolymers 39
2.3.2.1 Micelles 40
23.2.2 Gels 45
23.2.3 Films and Membranes 52
2.3.3 Tetrablock Copolymers 53
2.3.4 Pentablock Copolymers 54
2.3.4.1 Pluronic® Based 54
23.4.2 Non-pluronic Based 56
2.3.5 Multiblockcopolymers 57
2.4 Applications 59
2.5 Conclusions 61
Acknowledgments 61
References 61
3 Star-shaped Poly(2-alky!-2-oxazo!ines): Synthesis and Properties 67
Andrey V. Tenkovtsev, Alina i. Amirova, and Alexander P. Filippov
3.1 Introduction 67
3.2 Synthesis of Star-shaped Poly(2-alkyl-2-oxazolines) 68
3.3 Properties of Star-shaped Poly(2-alkyl-2-oxazolines) 78
3.4 Conclusions 87
References 88
4 Poly(N-vinylcaprolactam): From Polymer Synthesis to Smart
Self-assemblies 93
Fei Liu, Veronika Kozlovskaya, and Eugenia Khariampieva
4.1 Introduction 93
4.2 Synthesis of PVCL Homo- and Copolymers 93
4.2.1 Synthesis of Statistical PVCL Copolymers 95
4.2.2 Synthesis of PVCL Block Copolymers 97
4.2.3 Other PVCL-based Copolymers 99
4.3 Properties of PVCL in Aqueous Solutions 99
4.3.1 Dependence of the LCST of PVCL on Molecular Weight and Polymer
Concentration 99
4.3.2 LCST Dependence on Chemical Composition 100
Contents vii
4.3.3 The Effect of Salt on the PVCL Temperature Response 102
4.3.4 The Effect of Solvent on PVCL Temperature Response 102
4.4 Assembly of PVCL-based Polymers in Solution 102
4.4.1 PVCL Interpolymer Complexes 102
4.4.2 PVCL-based Micelles 103
4.4.3 Self-assembly of PVCL-based Copolymers into Polymersomes 105
4.5 Templated Assemblies of PVCL Polymers 107
4.5.1 Hydrogen-bonded PVCL-based Multilayers 107
4.5.1.1 pH-sensitive Hydrogen-bonded PVCL Multilayers 107
4.5.1.2 Enzymatically Sensitive Hydrogen-bonded PVCL Multilayers 108
4.5.2 Multilayer Hydrogels of PVCL 110
4.6 Outlook and Perspectives 113
Acknowledgment 113
References 114
5 Sodium Alginate Grafted with Poly(A/-isopropylacrylamide) 121
Catalina N. Cheaburu-Yilmaz, Cornelia Vasile, Oana-Nicoleta Ciocoiu, and
Georgios Staikos
5.1 AlginicAcid 121
5.1.1 Monomeric and Polymeric Structure of Alginates 121
5.2 Poly(iV-Isopropylacrylamide) and Thermoresponsive Properties 122
5.3 Synthesis and Characterization of Alginate-grtf/£-PNIPAM
Copolymers 123
5.4 Solution Properties 124
5.4.1 Turbidimetry 124
5.4.2 Fluorescence 124
5.4.3 Rheology 126
5.4.4 Degradability 130
5.4.5 Biocompatibility 131
5.4.5.1 Cytotoxicity 132
5A5.2 Pharmaceutical and Medical Applications 135
5.5 Conclusions and Perspectives 137
References 138
6 Multi-stimuli-responsive Polymers Based on Calix[4]arenes and
Dibenzo-18-crown-6-ethers 145
Szymon Wiktorowicz, Heikki Tenhu, and Vladimir Aseyev
6.1 Introduction 145
6.2 Single-stimuli-responsive Polymers 146
6.2.1 Thermo-responsive Polymers in Polar Media 147
6.2.2 pH-responsive Polymers 148
6.2.3 Photoresponsive Polymers 148
6.2.4 Other Single-stimuli-responsive Polymers 150
6.3 Multi-stimuli-responsive Polymers 150
6.4 Poly(azocalix[4]arene)s and Poly(azodibenzo-18-crown-6-ether)s 151
6.4.1 Calixarenes 151
6.4.2 Crown Ethers 152
viii I Contents
6.4.3 Structural Units of Poly(azocalix[4]arene)s 153
6.4.4 Structural Units of Poly(azodibenzo-18-crown-6-ether)s 154
6.5 Photoisomerization 154
6.6 Host-guest Interactions 156
6.7 Thermo-responsiveness 158
6.7.1 LCST: Tegylated Poly(azocalix[4]arene)s in Water 158
6.7.2 UCST: Tegylated Poly(azocalix[4]arene)s in Alcohols 159
6.7.3 UCST and Photoisomerization of Tegylated Poly(azocalix[4]arene)s 160
6.7.4 UCST and Poly(azodibenzo-18-crown-6-ether)s 161
6.7.5 UCST and Photoisomerization of Poly(azodibenzo-18-crown-6-ether)s 162
6.7.6 UCST in Water-alcohol Mixtures 162
6.8 Solvatochromism and pH Sensitivity 163
6.9 Summary and Outlook 164
Acknowledgments 165
References 165
Part II Characterization of Temperature-responsive Polymers 175
7 Small-Angle X-ray and Neutron Scattering of Temperature-Responsive
Polymers in Solutions 177
Sergey K. Filippov, Martin Hruby, and Petr Stepanek
7.1 Introduction 177
7.2 Temperature-responsive Homopolymers 179
7.3 Hydrophobically Modified Polymers 182
7.4 Cross-Linked Temperature-Sensitive Polymers and Gels 184
7.5 Temperature-Responsive Block Copolymers 185
7.6 Hybrid Nanoparticles 187
171 Gradient Temperature-Responsive Polymers 188
7.8 Multi-responsive Copolymers 189
7.9 Concluding Remarks 191
Acknowledgments 191
References 191
8 Infrared and Raman Spectroscopy of Temperature-Responsive
Polymers 197
Yasushi Maeda
8.1 Introduction 197
8.2 Experimental Methods to Measure IR and Raman Spectra of Aqueous
Solutions 198
8.3 Poly(AAsubstituted acrylamide)s 200
8.3.1 Overall Spectral Change 200
8.3.2 Amide Bands 202
8.3.3 C-H Stretching Bands 204
8.3.4 C-D Stretching Band 206
8.4 Poly(vinyl ether)s 207
8.5 Poly(meth)acrylates 208
Contents
ix
8.6 Effects of Additives on Phase Behavior 210
8.7 Temperature-Responsive Copolymers and Gels 217
References 222
9 Application of NMR Spectroscopy to Study Thermoresponsive
Polymers 225
Jin Spevacek
9.1 Introduction 225
9.2 Coil-Globule Phase Transition and Its Manifestation in NMR Spectra 225
9.3 Temperature Dependences of High-Resolution NMR Spectra:
Phase-Separated Fraction p 227
9.4 Multicomponent Polymer Systems 230
9.5 Effects of Low-Molecular-Weight Additives on Phase Transition 234
9.6 Behavior of Water at the Phase Transition 236
9.7 Conclusion 242
Acknowledgment 242
References 242
10 Polarized Luminescence Studies of Nanosecond Dynamics of
Thermosensitive Polymers in Aqueous Solutions 249
Vladimir D. Pautov, Tatiana N. Nekrasova, Tatiana D. Anan eva, and Ruslan Y. Smyslov
10.1 Introduction 249
10.2 Theoretical Part 250
10.2.1 Polarization of Luminescence 250
10.2.2 The Use of Polarized Luminescence in the Studies of Nanosecond Dynamics
of Macromolecules 253
10.3 Experimental Part 258
10.3.1 Methods of Synthesis of Polymers Containing Luminescent Markers 258
10.3.2 Technique for Measurement of Luminescence Polarization 260
10.3.3 Thermosensitive Water-Soluble Polymers 263
10.3.4 pH and Thermosensitive Water-Soluble Polymers 268
10.3.5 Temperature-Induced Transitions in Polymers in Nonaqueous
Solutions 271
10.4 Conclusion 272
References 273
Part III Applications of Temperature-responsive Polymers 279
11 Applications of Temperature-Responsive Polymers Grafted onto Solid
Core Nanoparticles 281
Edward D. H. Mansfield, Adrian C. Williams, and Vitaliy V. Khutoryanskiy
11.1 Introduction 281
11.2 Silica Nanoparticles 282
11.2.1 pNIPAM-functionalised Silica Nanoparticles 282
11.2.2 Poloxamer-functionalised Silica Nanoparticles 284
11.2.3 Other Polymers 286
X
Contents
11.3
11.3.1
11.3.2
11.3.3
11.3.4
11.4
11.4.1
11.4.2
11.4.3
11.4.4
11.5
12
12.1
12.1.1
12.1.2
12.1.3
12.1.4
12.1.5
12.1.6
12.2
13
13.1
13.2
13.3
13.4
13.5
13.6
13.6.1
13.6.2
13.6.3
13.7
14
14.1
14.2
Metallic Nanoparticles 286
pNIPAM-functionalised Metallic Nanoparticles 287
Poloxamer-functionalised Metallic Nanoparticles 288
Elastin-functionalised Metallic Nanoparticles 288
Other Polymer-functionalised Metallic Nanoparticles 289
Magnetic Nanoparticles 290
pNIPAM-functionalised Magnetic Nanoparticles 290
Poloxamer-functionalised Magnetic Nanoparticles 291
Other TRP-functionalised Magnetic Nanoparticles 293
Summary 293
Conclusions 294
References 294
Temperature-responsive Polymers for Tissue Engineering 301
Kenichi Nagase, Masayuki Yamato, and Teruo Okano
Introduction 301
Thermo-responsive Cell Culture Dishes and Cell Sheets 301
Thermo-responsive Cell Culture Dishes Prepared by Electron-beam-induced
Polymerization 302
Thermo-responsive Cell Culture Dishes for Enhancing Cell Adhesion and
Proliferation by Immobilized Biological Ligands 303
Thermo-responsive Cell Culture Dish Prepared by Living Radical
Polymerization 304
Patterned Thermo-responsive Cell Culture Substrates 306
Thermo-responsive Surfaces for Cell Separation 309
Conclusions 309
Acknowledgments 309
References 311
Thermogel Polymers for Injectable Drug Delivery Systems 313
Vidhi M. Shah, DucX. Nguyen, Deepa A. Rao, Raid G. Aiany, and Adam W.G. Alani
Introduction 313
Pluronics® 314
Polyester-based Polymers 315
Chitosan and Derivatives 317
Polypeptides 318
Clinical Application of Thermogel Polymers 319
Ocular Delivery 319
Nasal Delivery 320
Antitumor Delivery/Drug Delivery Systems 321
Summary 323
References 323
Thermoresponsive Electrospun Polymer-based (Nano)fibers 329
Mariliz Achiileos and Theodora Krasia-Christoforou
Introduction 329
Basic Principles of Electrospinning 330
14.3 PNIPAM-based Electrospun (Nano)fibers 332
14.3.1 Temperature-triggered Wettability 332
14.3.2 Biomedicine 335
14.3.2.1 Drug Delivery 336
14.3.2.2 Tissue Engineering 339
14.3.2.3 Biosensing 341
14.3.2.4 Solid-phase Microextraction 341
14.3.2.5 Molecular Recognition 342
14.3.2.6 Organic-Inorganic PNIPAM-based Electrospun (Nano)fibers 342
14.3.3 Sensing 343
14.3.4 Other Applications 344
14.4 Other Types of Thermoresponsive Electrospun (Nano)iibers 345
14.5 Conclusions and Outlook 348
References 348
15 Catalysis by Thermoresponsive Polymers 357
Natalya A. Dolya and Sarkyt E. Kudaibergenov
15.1 Introduction 357
15.2 Metal Complexes Immobilized Within Thermosensitive Polymers 358
15.3 Thermoresponsive Polyampholytes 358
15.4 Thermosensitive Hydrogels in Catalysis 361
15.5 Thermoresponsive Catalytically Active Nano- and Microgels, Spheres,
Capsules, and Micelles 364
15.6 Thermosensitive Self-Assemblies 367
15.7 Mono- and Bimetallic Nanoparticles Stabilized by Thermoresponsive
Polymers 368
15.8 Enzymes-Embedded TTiermoresponsive Polymers 369
15.9 Immobilization of Magnetic Nanoparticles into the Matrix of
Thermoresponsive Polymers for Efficient Separation of Catalysts 369
15.10 Summary 370
Acknowledgments 3 71
References 371
Index 379
An authoritative resource that offers an understanding of the chemistry,
properties, and applications of temperature-responsive polymers
With contributions from a distinguished
panel of experts, Temperature-Responsive
Polymers puts the focus on hydrophilic
polymers capable of changing their physico-
chemical properties in response to changes
in environmental temperature. The contrib-
utors review the chemistry of these systems,
and discuss a variety of synthetic approaches
for preparation of temperature-responsive
polymers, physicochemical methods of their
characterisation and potential applications in
biomedical areas.
The text reviews a wide-variety of topics includ-
ing: The characterisation of temperature-
responsive polymers; Infrared and Raman
spectroscopy; Applications of temperature-
responsive polymers grafted onto solid core
nanoparticles; and much more. The contribu-
tors also explore how temperature-responsive
polymers can be used in the biomedical field
for applications such as tissue engineering.
This important resource:
• Offers an important synthesis of the
current research on temperature-
responsive polymers
• Covers the chemistry, the synthetic
approaches for presentation and the
physiochemical method of temperature-
responsive polymers
• Includes a review of the fundamental charac-
teristics of temperature-responsive polymers
• Explores many of the potential applications
in biomedical science, including drug
delivery and gene therapy
Written for polymer scientists in both academia
and industry as well as postgraduate students
working in the area of stimuli-responsive mate-
rials, this vital text offers an exploration of the
chemistry, properties and current applications
of temperature-responsive polymers.
Edited by:
Vitaliy V. Khutoryanskiy, Ph.D., is Professor of Formulation Science,
Reading School of Pharmacy, University of Reading, Whiteknights,
Reading, UK.
Theoni K. Georgiou, Ph.D., is a Senior Lecturer in Polymer Chemistry,
Department of Materials, Imperial College London, UK.
Cover Design: Wiley
Cover Image: Courtesy of Dr. Daulet Kaldybekov
www.wiley.com
Wiley b
ISBN 978-1-119-15778-6
Also available
as an e-book
9
157786
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| id | DE-604.BV044933608 |
| illustrated | Illustrated |
| indexdate | 2024-12-24T06:25:22Z |
| institution | BVB |
| isbn | 9781119157786 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-030326621 |
| oclc_num | 1050937471 |
| open_access_boolean | |
| owner | DE-703 DE-29T DE-83 |
| owner_facet | DE-703 DE-29T DE-83 |
| physical | xxii, 384 Seiten Illustrationen, Diagramme |
| publishDate | 2018 |
| publishDateSearch | 2018 |
| publishDateSort | 2018 |
| publisher | Wiley |
| record_format | marc |
| spellingShingle | Temperature-responsive polymers chemistry, properties, and applications Thermoresponsive Polymere (DE-588)1118761898 gnd |
| subject_GND | (DE-588)1118761898 |
| title | Temperature-responsive polymers chemistry, properties, and applications |
| title_auth | Temperature-responsive polymers chemistry, properties, and applications |
| title_exact_search | Temperature-responsive polymers chemistry, properties, and applications |
| title_full | Temperature-responsive polymers chemistry, properties, and applications edited by Vitaliy Khutoryanskiy (University of Reading, UK), Theoni K. Georgiou (Imperial College London, UK) |
| title_fullStr | Temperature-responsive polymers chemistry, properties, and applications edited by Vitaliy Khutoryanskiy (University of Reading, UK), Theoni K. Georgiou (Imperial College London, UK) |
| title_full_unstemmed | Temperature-responsive polymers chemistry, properties, and applications edited by Vitaliy Khutoryanskiy (University of Reading, UK), Theoni K. Georgiou (Imperial College London, UK) |
| title_short | Temperature-responsive polymers |
| title_sort | temperature responsive polymers chemistry properties and applications |
| title_sub | chemistry, properties, and applications |
| topic | Thermoresponsive Polymere (DE-588)1118761898 gnd |
| topic_facet | Thermoresponsive Polymere |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030326621&sequence=000003&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030326621&sequence=000004&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA |
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