Synthesis techniques for polymer nanocomposites

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Veröffentlicht: Weinheim Wiley-VCH 2015
Schriftenreihe:Polymer nano-, micro- & macrocomposites 6
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Datensatz im Suchindex

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adam_text WlLEY-VCH The book series ‘Polymer Nano-, Micro- and Macrocomposites’ provides complete and comprehensive information on all important aspects of polymer composite research and development, including, but not limited to synthesis, filler modification, modeling, characterization as well as application and commercialization issues. Each book focuses on a particular topic and gives a balanced in-depth overview of the respective subfield of polymer composite science and its relation to industrial applications. With the books the readers obtain dedicated resources with information relevant to their research, thereby helping to save time and money. Summarizing all the most important synthesis techniques used in the lab as well as in industry, this book is comprehensive in its coverage from chemical, physical and mechanical viewpoints. This book helps readers to choose the correct synthesis routes, such as suspension and miniemulsion polymerization, living polymerization, sonication, mechanical methods or the use of radiation, and so achieve the desired composite properties. Vikas Mittal is an Associate Professor at the Chemical Engineering Department of The Petroleum Institute, Abu Dhabi. He obtained his PhD in 2006 in Polymer and Materials Engineering from the Swiss Federal Institute of Technology in Zurich, Switzerland. Later, he worked as Materials Scientist in the Active and Intelligent Coatings section of SunChemical in London, UK and as Polymer Engineer at BASF Polymer Research in Ludwigshafen, Germany. His research interests include polymer nanocomposites, novel filler surface modifications, thermal stability enhancements, polymer latexes with functionalized surfaces etc. He has authored over 40 scientific publications, book chapters and patents on these subjects. Volume 6 Contents^ Preface XI List of Contributors XIII 1 Synthesis of Polymer Nanocomposites: Review of Various Techniques 1 Joel Fowoz and Vikas Mittal 1.1 Introduction 1 1.2 Synthesis Methods 4 1.2.1 Melt Intercalation 4 1 /2.2 Exfoliation Adsorption 9 L2.2.1 Solution Intercalation 9 1.2.2.2 Emulsion Polymerization 11 1.2.3 /« Situ Polymerization i6 1.2.4 Nontraditional Methods 23 References 26 2 Masterbatch Approach to Generate HDPE/CPE/Graphene Nanocomposites 31 AH U. Chaudhry and Vikas Mittal 2.1 Introduction 31 2.2 Experimental 33 2.2.1 Materials 33 2.2.2 Preparation of Graphite Oxide and Graphene Oxide 34 2.2.3 Nanocomposite Generation 35 2.2.4 Material Characterization 36 2.3 Results and Discussion 37 2.4 Conclusions 47 Acknowledgments 48 References 48 VI Contents 3 Preparation and Applications of Hydroxyapatite Nanocomposites Based on Biodegradable and Natural Polymers 51 Pou Turon, LuisJ. del Valle, Carlos Aleman, and Jordi Puiggali 3.1 Introduction 51 3.2 Preparation of HAp Nanocrystals 52 3.3 Preparation of HAp Nanocomposites 58 3.4 Applications of HAp/DNA Nanocomplexes as Gene Carriers 61 3.5 Tissue Engineering Applications of HAp Nanocomposites Based on Biodegradable Polymers 65 3.6 Applications of HAp Nanocomposites Based on Biodegradable Polymers as Drug Delivery Systems 72 3.7 Miscellaneous Applications of HAp Nanocomposites Based on Biodegradable Polymers 76 3.8 Concluding Remarks 79 Acknowledgments 80 References 80 4 Synthetic Methods for Nanocomposites Based on Polyester Resins 8 Michał Kędzierski 4.1 Introduction 87 4.2 Nanocomposites with Zero-Dimensional Nanorillers 89 4.2.1 Silicon-Containing Nanospheres 89 4.2.2 Metal Oxides 91 4.2.3 Other 0-D Nanoparticles 93 4.3 Nanocomposites with One-Dimensional Nanofillers 93 4.3.1 Carbon Nanotubes and Nanofibers 93 4.3.2 Cellulose Nanofibers 96 4.3.3 Other 1-D Nanofillers 97 4.4 Nanocomposites with Two-Dimensional Nanorillers 97 4.4.1 Layered Aluminosilicate Clays 97 4.4.1.1 Mixing Methods 98 4.4.1.2 Effects of the Clay Modification 99 4.4.1.3 Nanocomposites with MMT Introduced during the Synthesis of Pre-polymer 102 4.4.1.4 Various Properties and Multiphase Nanocomposites 103 4.4.1.5 Vinyl Ester-Clay Nanocomposites 106 4.4.2 Layered Double Hydroxides 106 4.4.3 Graphene-Based Nanofillers 107 4.5 Conclusions 109 Abbreviations 110 References 110 Contents VII 5 5.1 5.2 5.3 5.3.1 5.3.2 5.3.3 5.3.4 5.3.5 5.3.6 5.4 6 6.1 6.2 6.2.1 6.2.1.1 6.3 6.4 6.5 6.6 7 7.1 7.2 7.2.1 7.2.1.1 7.2.1.2 7.2.2 7.2.2.1 7.2.2.2 Synthesis Fabrication and Characterization of Ag/CNT-Polymer Nanocomposites 115 Vijoya K. Rongari and Sanchit Dey Introduction 115 Experimental Procedure 118 Results and Discussion 119 XRD analysis 119 Transmission Electron Microscopy 119 TGA Analysis of Nanoparticles 121 Thermal Response of the Polymer Composites 121 Compression Test Results of Polymer Composites 124 Flexure Test Results of Polymer Composites 125 Conclusion 127 Acknowledgments 127 References 127 Preparation and Characterization of PVDF-Based Nanocomposites 131 Derman Vatansever Bayramol, Tahir Shah, Navneet Soin, and Elias Siores Synthesis of Poly(vinylidene fluoride) (PVDF) 131 Structure and Piezoelectric Properties of PVDF 131 Relationships and Equations 135 The Piezoelectric Charge Constant and Piezoelectric Voltage Constant 136 Processing of PVDF for Energy Harvesting Applications 137 Processing of PVDF Based Materials: Polymer/Polymer, Polymer/Nanofiller, Polymer/Ionomer Blends 138 PVDF Based Nanocomposites for Energy Harvesting Applications 139 Conclusion 140 References 141 In Situ Thermal, Photon, and Electron-Beam Synthesis of Polymer Nanocomposites 145 Luana Persa no, Andrea Camposeo, Anna Maria Laera, Francesca Di Benedetto, Vincenzo Resta, Leander Tapfer, and Dario Pisignano Introduction 145 Thermal-Assisted In Situ Synthesis: Material Choice and Nanocomposite Characterization 146 Precursor Molecules 146 Metal Salts 147 Organometallic Compounds 147 Thermal Synthesis and Composites Characterization 151 Microstructural Characterization 152 Optical Spectroscopy Experiments 154 VIII Contents 7.3 Fabrication of Nanocomposites and Patterning 155 7.3.1 Nanocomposites by Photoirradiation 157 7.3.1.1 UV and Visible Irradiation 157 7.3.1.2 Multiphoton Irradiation 160 7.3.2 Nanocomposites by Electron-Beam Writing 160 7.3.3 Nanocomposite Polymer Fibers 765 7.3.3.1 Photo-Assisted Synthesis 167 7.3.3.2 Thermal-Assisted Synthesis 169 7.4 Conclusions 171 Acknowledgments 172 References 172 8 Synthesis of Polymer Nanocomposites by Water-Assisted Extrusion 179 Naïma Sallem֊ldrissi, Michel Sclavons, and Jacques Devaux 8.1 Introduction 179 8.2 Nanocomposites Structure and Characterization 180 8.2.1 Clays 180 8.2.2 Organomodification of Layered Silicates 181 8.2.3 Nanocomposites Structure and Characterization 182 8.3 Nanocomposites Preparation 183 8.3.1 Intercalation from Solution 183 8.3.2 In Situ Polymerization 183 8.3.3 Melt Compounding 184 8.3.3.1 Melt Blending of Polymer/Organoclay Nanocomposites 184 8.3.3.2 Melt Blending of Polymer/Pristine Clay Nanocomposites 186 8.4 Nanocomposite Properties 195 8.4.1 Thermal Stability 195 8.4.2 Flame Retardancy 197 8.5 Toward Fully Green Composites? 198 References 201 9 In Situ Preparation of Conducting Polymer Nanocomposites 211 Liping Yang, Cher Ling Toh, and Xuehong Lu 9.1 Introduction 211 9.1.1 Electrically Conductive Polymer Nanocomposites and Their Applications 212 9.1.2 Percolation Theory 213 9.1.3 Factors Affecting the Electrical Conductivity of Nanocomposites 214 9.1.3.1 Physical Properties of the Fillers 214 9.1.3.2 Filler Distribution and Dispersion 216 9.1.3.3 Physical Properties of Polymer Matrices 216 9.1.3.4 Filler Orientation and Alignment 217 9.1.3.5 Nanocomposite Fabrication Methods and Conditions 218 Contents IX 9.2 9.2.1 9.2.1.1 9.2.1.2 9.2.1.3 9.2.2 9.2.2.1 9.2.2.2 9.3 In Situ Preparation of Conductive Nanocomposites 219 In Situ Polymerization Strategy 219 Step Growth 220 Chain Growth 224 Aligning Conductive Fillers in in situ Polymerization Processes 227 In Situ Formation of Conducting Polymer Nanocomposites 228 In Situ Formation of rGO-Based Polymer Nanocomposites 228 In Situ Formation of Metallic Conductive Pathways 232 Challenges and Outlook 233 References 235 10 Near [R Spectroscopy for the Characterization of Dispersion in Polymer-Clay Nanocomposites 241 Ana Vera Machado՝, Joana Margarida Barbas, and Jose Antonio Covas 10.1 10.2 10.3 10.4 10.5 10.6 10.7 Introduction 241 Morphology and Properties 241 Preparation Methods 243 Characterization Techniques 243 Dispersion by Melt Mixing 247 Online and Inline Monitoring of Dispersion 249 Conclusions 259 References 259 11 Synthesis of Polymer Nanocomposites in Supercritical C02 267 Yuvaraj Haldorai andJae֊Jin Shim 11.1 11.2 11.3 11.4 Introduction 267 Background on Supercritical C02 268 Physical and Chemical Properties of scC02 270 Preparation of Polymer/Inorganic Filler Nanocomposites in Supercritical C02 272 11.4.1 11.4.1.1 11.4.1.2 11.4.2 11.4.2.1 11.4.2.2 11.5 Ex Situ Method 272 Solution Blending 272 Melt Blending 272 In Situ Method 276 Synthesis of Nanocomposites by Dispersion Polymerization 277 Synthesis of Nanocomposites by Other Techniques 281 Conclusions 286 References 286 Index 291
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Nanokomposit (DE-588)4768127-5 gnd rswk-swf
Polymere (DE-588)4046699-1 gnd rswk-swf
Herstellung (DE-588)4159653-5 gnd rswk-swf
Synthese (DE-588)4418958-8 gnd rswk-swf
Verbundwerkstoff (DE-588)4062670-2 gnd rswk-swf
Kunststoff (DE-588)4033676-1 gnd rswk-swf
Nanostrukturiertes Material (DE-588)4342626-8 gnd rswk-swf
Polymere (DE-588)4046699-1 s
Nanokomposit (DE-588)4768127-5 s
Synthese (DE-588)4418958-8 s
DE-604
Kunststoff (DE-588)4033676-1 s
Verbundwerkstoff (DE-588)4062670-2 s
Nanostrukturiertes Material (DE-588)4342626-8 s
Herstellung (DE-588)4159653-5 s
Polymergemisch (DE-588)4175243-0 s
Mittal, Vikas Sonstige (DE-588)1022155490 oth
Erscheint auch als Online-Ausgabe, EPUB 978-3-527-67032-1
Erscheint auch als Online-Ausgabe, MOBI 978-3-527-67031-4
Erscheint auch als Online-Ausgabe, PDF 978-3-527-67033-8
Polymer nano-, micro- & macrocomposites 6 (DE-604)BV040393302 6
Digitalisierung UB Bayreuth - ADAM Catalogue Enrichment application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027649887&sequence=000003&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Klappentext
Digitalisierung UB Bayreuth - ADAM Catalogue Enrichment application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027649887&sequence=000004&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis
spellingShingle Synthesis techniques for polymer nanocomposites
Polymer nano-, micro- & macrocomposites
Polymergemisch (DE-588)4175243-0 gnd
Nanokomposit (DE-588)4768127-5 gnd
Polymere (DE-588)4046699-1 gnd
Herstellung (DE-588)4159653-5 gnd
Synthese (DE-588)4418958-8 gnd
Verbundwerkstoff (DE-588)4062670-2 gnd
Kunststoff (DE-588)4033676-1 gnd
Nanostrukturiertes Material (DE-588)4342626-8 gnd
subject_GND (DE-588)4175243-0
(DE-588)4768127-5
(DE-588)4046699-1
(DE-588)4159653-5
(DE-588)4418958-8
(DE-588)4062670-2
(DE-588)4033676-1
(DE-588)4342626-8
title Synthesis techniques for polymer nanocomposites
title_auth Synthesis techniques for polymer nanocomposites
title_exact_search Synthesis techniques for polymer nanocomposites
title_full Synthesis techniques for polymer nanocomposites ed. by Vikas Mittal
title_fullStr Synthesis techniques for polymer nanocomposites ed. by Vikas Mittal
title_full_unstemmed Synthesis techniques for polymer nanocomposites ed. by Vikas Mittal
title_short Synthesis techniques for polymer nanocomposites
title_sort synthesis techniques for polymer nanocomposites
topic Polymergemisch (DE-588)4175243-0 gnd
Nanokomposit (DE-588)4768127-5 gnd
Polymere (DE-588)4046699-1 gnd
Herstellung (DE-588)4159653-5 gnd
Synthese (DE-588)4418958-8 gnd
Verbundwerkstoff (DE-588)4062670-2 gnd
Kunststoff (DE-588)4033676-1 gnd
Nanostrukturiertes Material (DE-588)4342626-8 gnd
topic_facet Polymergemisch
Nanokomposit
Polymere
Herstellung
Synthese
Verbundwerkstoff
Kunststoff
Nanostrukturiertes Material
url http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027649887&sequence=000003&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA
http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027649887&sequence=000004&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA
volume_link (DE-604)BV040393302
work_keys_str_mv AT mittalvikas synthesistechniquesforpolymernanocomposites