Advanced distillation technologies design, control and applications
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2013
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| 008 | 130613s2013 xx d||| |||| 00||| eng d | ||
| 020 | |a 9781119993612 |9 978-1-119-99361-2 | ||
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| 100 | 1 | |a Kiss, Anton Alexandru |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Advanced distillation technologies |b design, control and applications |c Anton Alexandru Kiss |
| 250 | |a 1. publ. | ||
| 264 | 1 | |a Chichester |b Wiley |c 2013 | |
| 300 | |a XVI, 397 S. |b graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
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Datensatz im Suchindex
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| _version_ | 1823055788424298496 |
| adam_text | Contents/?
Preface
xiii
Acknowledgements
xv
1
Basic Concepts in Distillation
1
1.1
Introduction
1
1.2
Physical Property Methods
2
1.3
Vapor Pressure
6
1.4
Vapor—Liquid Equilibrium and VLE Non-ideality
8
1.4.1
Vapor-Liquid Equilibrium
8
1.4.2
VLE Non-ideality
11
1.5
Relative Volatility
13
1.6
Bubble Point Calculations
14
1.7
Ternary Diagrams and Residue Curve Maps
16
1.7.1
Ternary Diagrams
16
1.7.2
Residue Curve Maps
18
1.8
Analysis of Distillation Columns
24
1.8.1
Degrees of Freedom Analysis
26
1.8.2
McCabe-Thiele Method
27
1-8.3
Approximate Multicomponent Methods
33
1.9
Concluding Remarks
34
References
35
2
Design, Control and Economics of Distillation
37
2.1
Introduction
37
2.2
Design Principles
38
2.2.1
Operating Pressure
39
2.2.2
Heuristic Optimization
40
ii
CONTENTS
2.2.3
Rigorous Optimization
41
2.2.4
Feed Preheating
42
2.2.5
Intermediate Reboilers and Condensers
42
2.2.6
Heat Integration
43
2.3
Basics of Distillation Control
44
2.3.1
Single-End Control
46
2.3.2
Dual-End Control
49
2.3.3
Alternative Control Structures
52
23.4
Constraint Control
53
2.3.5 Multivariable
Control
54
2.4
Economic Evaluation
55
2.4.1
Equipment Sizing
56
2.4.2
Equipment Cost
59
2.4.3
Utilities and Energy Cost
62
2.4.4
Cost of Chemicals
63
2.5
Concluding Remarks
63
References
64
3
Dividing-Wall Column
67
3.1
Introduction
67
3.2
DWC Configurations
70
3.3
Design of DWCs
75
3.3.1
Heuristic Rules for DWC Design
77
3.3.2
Approximate Design Methods
78
3.3.3
Vmin Diagram Method
79
3.3.4
Optimal Design of a DWC
82
3.4
Modeling of a DWC
83
3.4.1
Pump-Around Model
84
3.4.2
Two Columns Sequence Model
84
3.4.3
Four Columns Sequence Model
85
3.4.4
Simultaneous Models
86
3.4.5
Simulation of a Four-Product DWC
86
3.4.6
Optimization Methods
86
3.5
DWC Equipment
87
3.5.1
Liquid/Reflux Splitter
89
3.5.2
Column Internals
91
3.5.3
Equipment Sizing
91
3.5.4
Constructional Aspects
94
3.6
Case Study: Separation of Aromatics
97
3.7
Concluding Remarks
103
References
107
CONTENTS ix
4 Optimal Operation and
Control
of DWC 111
4.1
Introduction 111
4.2
Degrees of Freedom Analysis
112
4.3
Optimal Operation and Vmin Diagram
114
4.4
Overview of DWC Control Structures
117
4.4.1
Three-Point Control Structure
118
4.4.2
Three-Point Control Structure with
Alternative Pairing
120
4.4.3
Four-Point Control Structure
121
4.4.4
Three-Point Control Structure with
Nested Loops
121
4.4.5
Performance Control of Prefractionator
Sub-system using the Liquid Split
122
4.4.6
Control Structures Based on Inferential
Temperature Measurements
123
4.4.7
Feedforward Control to Reject Frequent
Measurable Disturbances
126
4.4.8
Advanced Control Techniques
127
4.5
Control Guidelines and Rules
128
4.6
Case Study: Pentane—Hexane-Heptane Separation
129
4.7
Case Study: Energy Efficient Control of a BTX DWC
132
4.7.1
Energy Efficient Control Strategies
135
4.7.2
Dynamic Simulations
139
4.8
Concluding Remarks
148
References
149
5
Advanced Control Strategies for DWC
153
5.1
Introduction
153
5.2
Overview of Previous Work
154
5.3
Dynamic Model of a DWC
156
5.4
Conventional versus Advanced Control Strategies
163
5.4.1 PID
Loops within a Multi-loop Framework
163
5.4.2
Linear Quadratic Gaussian Control
165
5.4.3
Generic Model Control
167
5.4.4 Multivariable
Controller Synthesis
167
5.5
Energy Efficient Control Strategies
171
5.5.1
Background of Model Predictive Control
173
5.5.2
Controller Tuning Parameters
175
5.5.3
Dynamic Simulations
176
5Љ
Concluding Remarks
180
; CONTENTS
Notation 181
References
183
6 Applications
of Dividing-Wall Columns
187
6.1
Introduction
187
6.2
Separation of Ternary and Multicomponent Mixtures
188
6.3
Reactive Dividing-Wall Column
195
6.4
Azeotropic Dividing-Wall Column
198
6.5
Extractive Dividing-Wall Column
199
6.6
Revamping of Conventional Columns to DWC
203
6.7
Case Study: Dimethyl Ether Synthesis by R-DWC
205
6.8
Case Study: Bioethanol Dehydration by A-DWC and
E-DWC
212
6.9
Concluding Remarks
223
References
223
7
Heat Pump Assisted Distillation
229
7.1
Introduction
229
7.2
Working Principle
231
7.3
Vapor (Rejcompression
232
7.3.1
Vapor Compression
233
7.3.2
Mechanical Vapor
Recompression
233
7.3.3
Thermal Vapor
Recompression
234
7.4 Absorption-Resorption
Heat Pumps
234
7.4.1
Absorption Heat Pump
234
7.4.2
Compression—
Resorption
Heat Pump
235
7.5
Thermo-acoustic Heat Pump
236
7.6
Other Heat Pumps
240
7.6.1
Stirling Cycle
240
7.6.2
Vuilleumier Cycle
241
7.6.3
Brayton Cycle
241
7.6.4
Malone Cycle
242
7.6.5
Solid-Sorption Cycle
242
7.7
Heat-Integrated Distillation Column
244
7.8
Technology Selection Scheme
245
7.8.1
Energy Efficient Distillation
Technologies
246
7.8.2
Multicomponent Separations
249
7.8.3
Binary Distillation
254
7.8.4
Selected Scheme Applications
263
CONTENTS xi
7.9
Concluding Remarks
265
References
265
8
Heat-Integrated Distillation Column
271
8.1
Introduction
271
8.2
Working Principle
273
8.3
Thermodynamic Analysis
277
8.4
Potential Energy Savings
280
8.4.1
Partial Heat Integrated Distillation Column
(p-HIDiC)
280
8.4.2
Ideal Heat Integrated Distillation Column
(i-HIDiC)
281
8.5
Design and Construction Options
282
8.5.1
Inter-coupled Distillation Columns
284
8.5.2
Distillation Column with Partition Wall
285
8.5.3
Concentric Distillation Column
287
8.5.4
Concentric Column with Heat Panels
288
8.5.5
Shell
&
Tube Heat-Exchanger Column
289
8.5.6
Plate-Fin Heat-Exchanger Column
290
8.5.7
Heat Transfer Means
292
8.6
Modeling and Simulation
295
8.7
Process Dynamics, Control, and Operation
297
8.8
Applications of HIDiC
300
8.9
Concluding Remarks
304
References
305
9
Cyclic Distillation
311
9.1
Introduction
311
9.2
Overview of Cyclic Distillation Processes
313
9.3
Process Description
316
9.4
Mathematical and Hydrodynamic Model
319
9.4.1
Mathematical Model
319
9.4.2
Hydrodynamic Model
321
9.4.3
Sensitivity Analysis
323
9.5
Modeling and Design of Cyclic Distillation
327
9.5.1
Modeling Approach
329
9.5.2
Comparison with Classic Distillation
331
9.5.3
Design Methodology
331
9.5.4
Demonstration of the Design Procedure
333
9.6
Control of Cyclic Distillation
335
xii CONTENTS
9.7
Cyclic Distillation Case Studies
338
9.7.1
Ethanol-Water Stripping and Concentration
338
9.7.2
Methanol-Water Separation
341
9.8
Concluding Remarks
347
References
349
10
Reactive Distillation
353
10.1
Introduction
353
10.2
Principles of Reactive Distillation
354
10.3
Design, Control and Applications
357
10.4
Modeling Reactive Distillation
362
10.5
Feasibility and Technical Evaluation
364
10.5.1
Feasibility Evaluation
364
10.5.2
Technical Evaluation
367
10.6
Case Study: Advanced Control of a Reactive
Distillation Column
371
10.6.1
Mathematical Model
371
10.6.2
Open-Loop Dynamic Analysis
374
10.6.3
Closed-Loop Performance
374
10.7
Case Study:
Biodiesel
Production by
Heat-Integrated RD
378
10.8
Case Study: Fatty Esters Synthesis by Dual RD
383
10.9
Concluding Remarks
387
References
388
Index
393
ADVANCED
DISTILLATION
TECHNOLOGIES
Design,
Control and Applications
Anton
A. Kiss
Distillation has
histoncally
been the main method for separating mixtures in the chemical process
industry. However, despite the flexibility and widespread use of distillation processes, they
still remain extremely energy inefficient. Increased optimization and novel distillation concepts
can deliver substantial benefits, not just in terms of significantly lower energy use, but also in
reducing capital investment and improving eco-efficiency. While likely to remain the separation
technology of choice for the next few decades, there is no doubt that distillation technologies
need to make radical changes in order to meet the demands of the energy-conscious society.
Advanced Distillation Technologies: Design, Control and Applications gives a deep and
broad insight into integrated separations using non-conventional arrangements, including both
current and upcoming process intensification technologies. It includes:
Key concepts in distillation technology
•
Principles of design, control, sizing and economics of distillation
•
Dividing-wall column (DWC)
-
design, configurations, optimal operation
and energy efficient and advanced control
•
DWC applications in ternary separations, azeotropic, extractive and reactive
distillation
•
Heat integrated distillation column
(HIDÍC)
~ design, equipment and configurations
-
Heat-pump assisted applications
(MVR,
TVR,
AHR CHRR TAHP and others)
•
Cyclic distillation technology
-
concepts, modeling approach, design
and control issues
•
Reactive distillation
-
fundamentals, equipment, applications, feasibility scheme
•
Results of rigorous simulations in
Mathworks
Matlab
&
Simulink, Aspen Plus,
Dynamics and Custom Modeler
Containing abundant examples and industrial case studies, this is a unique resource that tackles
the most advanced distillation technologies
-
all the way from the conceptual design to practical
implementation.
Also available
as an e-book
ISBN
978-1-119-99361-2
WILEY
wiley.com
9 »781 1
T
9 993 6 12
|
| any_adam_object | 1 |
| author | Kiss, Anton Alexandru |
| author_facet | Kiss, Anton Alexandru |
| author_role | aut |
| author_sort | Kiss, Anton Alexandru |
| author_variant | a a k aa aak |
| building | Verbundindex |
| bvnumber | BV041087542 |
| classification_rvk | VN 7220 |
| classification_tum | CIT 215f |
| ctrlnum | (OCoLC)844613827 (DE-599)BVBBV041087542 |
| dewey-full | 542/.4 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 542 - Techniques, equipment & materials |
| dewey-raw | 542/.4 |
| dewey-search | 542/.4 |
| dewey-sort | 3542 14 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| edition | 1. publ. |
| format | Book |
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| id | DE-604.BV041087542 |
| illustrated | Illustrated |
| indexdate | 2025-02-03T17:41:49Z |
| institution | BVB |
| isbn | 9781119993612 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-026064204 |
| oclc_num | 844613827 |
| open_access_boolean | |
| owner | DE-91G DE-BY-TUM DE-29T DE-703 DE-19 DE-BY-UBM DE-92 |
| owner_facet | DE-91G DE-BY-TUM DE-29T DE-703 DE-19 DE-BY-UBM DE-92 |
| physical | XVI, 397 S. graph. Darst. |
| publishDate | 2013 |
| publishDateSearch | 2013 |
| publishDateSort | 2013 |
| publisher | Wiley |
| record_format | marc |
| spellingShingle | Kiss, Anton Alexandru Advanced distillation technologies design, control and applications Trennverfahren (DE-588)4078395-9 gnd Destillation (DE-588)4011543-4 gnd Chemische Verfahrenstechnik (DE-588)4069941-9 gnd Technische Chemie (DE-588)4078178-1 gnd |
| subject_GND | (DE-588)4078395-9 (DE-588)4011543-4 (DE-588)4069941-9 (DE-588)4078178-1 |
| title | Advanced distillation technologies design, control and applications |
| title_auth | Advanced distillation technologies design, control and applications |
| title_exact_search | Advanced distillation technologies design, control and applications |
| title_full | Advanced distillation technologies design, control and applications Anton Alexandru Kiss |
| title_fullStr | Advanced distillation technologies design, control and applications Anton Alexandru Kiss |
| title_full_unstemmed | Advanced distillation technologies design, control and applications Anton Alexandru Kiss |
| title_short | Advanced distillation technologies |
| title_sort | advanced distillation technologies design control and applications |
| title_sub | design, control and applications |
| topic | Trennverfahren (DE-588)4078395-9 gnd Destillation (DE-588)4011543-4 gnd Chemische Verfahrenstechnik (DE-588)4069941-9 gnd Technische Chemie (DE-588)4078178-1 gnd |
| topic_facet | Trennverfahren Destillation Chemische Verfahrenstechnik Technische Chemie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026064204&sequence=000003&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026064204&sequence=000004&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT kissantonalexandru advanceddistillationtechnologiesdesigncontrolandapplications |