Chemical process technology
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2013
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| 100 | 1 | |a Moulijn, Jacob A. |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Chemical process technology |c Jacob A. Moulijn ; Michiel Makkee ; Annelies E. van Diepen |
| 250 | |a 2nd ed. | ||
| 264 | 1 | |a Chichester |b Wiley |c 2013 | |
| 300 | |a XIV, 552 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
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| 650 | 0 | 7 | |a Technische Chemie |0 (DE-588)4078178-1 |2 gnd |9 rswk-swf |
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| 700 | 1 | |a Makkee, Michiel |e Verfasser |4 aut | |
| 700 | 1 | |a Diepen, Annelies van |e Verfasser |4 aut | |
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Datensatz im Suchindex
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| DE-BY-UBR_media_number | 069040043642 |
| _version_ | 1822728195605004288 |
| adam_text | Contents
Preface
xiii
1
Introduction
1
References
6
General
Literature
6
2
The Chemical Industry
7
2.1
A Brief History
7
2.1.1
Inorganic Chemicals
7
2.1.2
Organic Chemicals
10
2.1.3
The Oil Era
11
2.1.4
The Age of Sustainability
] 2
2.2
Structure of the Chemicallndustry
13
2.3
Raw Materials and Energy
16
2.3.1
Fossil Fuel Consumption and Reserves
16
2.3.2
Biomass as an Alternative for Fossil Fuels
19
2.3.3
Energy and the Chemical Industry
21
2.3.4
Composition of Fossil Fuels and Biomass
23
2.4
Base Chemicals
35
2.5
Global Trends in the Chemical Industry
37
References
39
General Literature
40
3
Processes in the Oil Refinery
41
3.1
The Oil Refinery
-
An Overview
41
3.2
Physical Processes
42
3.2.1
Desalting and Dehydration
42
3.2.2
Crude Distillation
43
3.2.3
Propane Deasphalting
45
3.3
Thermal Processes
46
3.3.1
Visbreaking
46
3.3.2
Delayed Coking
47
3.3.3
Flexicoking
48
3.4
Catalytic Processes
49
3.4.1
Octane and Cetane Numbers
49
3.4.2
Catalytic Cracking
51
3.4.3
Catalytic Reforming
63
3.4.4
Alkylation
69
3.4.5
Hydroprocessing
76
vi
Contents
3.5
Current and Future Trends in Oil Refining
91
3.5.1
Stricter Environmental Regulations
92
3.5.2
Refinery Configurations
94
References
96
Production
of Light
Alkenes
99
4.1
Introduction
99
4.2
Cracking Reactions
100
4.2.1
Thermodynamics
100
4.2.2
Mechanism
101
4.2.3
Kinetics
102
4.3
The Industrial Process
103
4.3.1
Influence of Feedstock on Steam Cracker Operation and Products
103
4.3.2
Cracking Furnace
106
4.3.3
Heat Exchanger
109
4.3.4
Coke Formation
110
4.4
Product Processing
111
4.5
Novel Developments
113
4.5.1
Selective Dehydrogenation of Light Alkanes
114
4.5.2
Metathesis of Alkenes
116
4.5.3
Production of Light Alkenes from Synthesis Gas
118
4.5.4
Dehydration of Bioethanol
121
4.5.5
Direct Conversion of Methane
122
References
123
Production of Synthesis Gas
127
5.1
Introduction
127
5.2
Synthesis Gas from Natural Gas
129
5.2.1
Reactions and Thermodynamics
129
5.2.2
Steam Reforming Process
131
5.2.3
Autothermal
Reforming Process
137
5.2.4
Novel Developments
139
5.3
Coal Gasification
142
5.3.1
Gasification Reactions
142
5.3.2
Thermodynamics
143
5.3.3
Gasification Technologies
146
5.3.4
Recent Developments in Gasification Technology
151
5.3.5
Applications of Coal Gasification
154
5.3.6
Integrated Gasification Combined Cycle
156
5.3.7
Why Gasify, Not Burn for Electricity Generation?
158
5.3.8
Carbon Capture and Storage (CCS)
159
5.4
Cleaning and Conditioning of Synthesis Gas
161
5.4.1
Acid Gas Removal
161
5.4.2
Water-Gas Shift Reaction
163
5.4.3
Methanation
166
References
168
Contents
vii
6
Bulk Chemicals and Synthetic Fuels Derived from Synthesis Gas
171
6.1
Ammonia
171
6.1.1
Background Information
171
6.1.2
Thermodynamics
173
6.1.3
Commercial Ammonia Synthesis Reactors
175
6.1.4
Ammonia Synthesis Loop
178
6.1.5
Integrated Ammonia Plant
180
6.1.6
Hydrogen Recovery
182
6.1.7
Production of Urea
185
6.2 Methanol 191
6.2.1
Background Information
191
6.2.2
Reactions, Thermodynamics, and Catalysts
192
6.2.3
Synthesis Gas for
Methanol
Production
195
6.2.4 Methanol
Synthesis
196
6.2.5
Production of Formaldehyde
199
6.3
Synthetic Fuels and Fuel Additives
201
6.3.1
Fischer-Tropsch Process
202
6.3.2
Methanol-to-Gasoline (MTG) Process
212
6.3.3
Recent Developments in the Production of Synthetic Fuels
214
6.3.4
Fuel Additives
-
Methyl Tert-Butyl Ether
215
References
218
7
Processes for the Conversion of Biomass
221
7.1
Introduction
221
7.2
Production of Biofuels
223
7.2.1
Bioethanol and Biobutanol
224
7.2.2
Diesel
-Туре
Biofuels
226
7.3
Production of Bio-based Chemicals
231
7.3.1
Ethanol
232
7.3.2
Glycerol
233
7.3.3
Succinic Acid
234
7.3.4
Hydroxymethylfurfural (HMF)
236
7.4
The Biorefinery
236
7.4.1
Biorefinery Design Criteria and Products
236
7.4.2
Biorefinery Concepts
238
7.4.3
Core Technologies of a Thermochemical Biorefinery
239
7.4.4
Existing and Projected Biorefineries
243
7.4.5
Possibility of Integrating a Biorefinery with Existing Plants
243
7.4.6
Biorefinery versus Oil Refinery
245
7.5
Conclusions
246
References
246
8
Inorganic Bulk Chemicals
249
8.1
The Inorganic Chemicals Industry
249
8.2
Sulfuric Acid
250
8.2.1
Reactions and Thermodynamics
252
8.2.2
SO- Conversion Reactor
252
viii Contents
8.2.3
Modern Sulfuric Acid
Production
Process
254
8.2.4
Catalyst Deactivation
256
8.3
Sulfur Production
256
8.4
Nitric Acid
260
8.4.1
Reactions and Thermodynamics
260
8.4.2
Processes
262
8.4.3
NOX Abatement
266
8.5
Chlorine
268
8.5.1
Reactions for the Electrolysis of NaCl
269
8.5.2
Technologies for the Electrolysis of NaCl
270
References
274
9
Homogeneous Transition Metal Catalysis in the Production of Bulk Chemicals
275
9.1
Introduction
275
9.2
Acetic Acid Production
278
9.2.1
Background Information
278
9.2.2 Methanol Carbonylation -
Reactions, Thermodynamics, and Catalysis
281
9.2.3 Methanol
Carbonylation
-
Processes
284
9.3
Hydroformylation
286
9.3.1
Background Information
286
9.3.2
Thermodynamics
288
9.3.3
Catalyst Development
289
9.3.4
Processes for the Hydroformylation of
Propene
292
9.3.5
Processes for the Hydroformylation of Higher Alkenes
294
9.3.6
Comparison of Hydroformylation Processes
296
9.4
Ethene Oligomerization and More
297
9.4.1
Background Information
297
9.4.2
Reactions of the SHOP Process
298
9.4.3
The SHOP Process
299
9.5
Oxidation of p-Xylene: Dimethyl Terephthalate and Terephthalic Acid Production
301
9.5.1
Background Information
301
9.5.2
Conversion of p-Toluic Acid Intermediate
302
9.5.3
Processes
303
9.5.4
Process Comparison
305
9.6
Review of Reactors Used in Homogeneous Catalysis
305
9.6.1
Choice of Reactor
306
9.6.2
Exchanging Heat
308
9.7
Approaches for Catalyst/Product Separation
308
9.7.1
Biphasic Catalyst Systems
309
9.7.2
Immobilized Catalyst Systems
309
References
311
10
Heterogeneous Catalysis
-
Concepts and Examples
313
10.1
Introduction
313
10.2
Catalyst Design
314
10.2.1
Catalyst Size and Shape
314
10.2.2
Mechanical Properties of Catalyst Particles
316
Contents ix
10.3
Reactor
Types and Their Characteristics
316
10.3.1
Reactor Types
316
10.3.2
Exchanging Heat
319
10.3.3
Role of Catalyst Deactivation
321
10.3.4
Other Issues
322
10.4
Shape Selectivity
-
Zeolites
323
10.4.1
Production of Isobutene
325
10.4.2
Isomerization of Pentanes and Hexanes
328
10.4.3
Production of Ethylbenzene
330
10.5
Some Challenges and (Unconventional) Solutions
334
10.5
Л
Adiabatic Reactor with Periodic Flow Reversal
334
10.5.2
Highly Exothermic Reactions with a Selectivity Challenge
—
Selective
Oxidations
338
10.6
Monolith Reactors
—
Automotive Emission Control
344
10.6.1
Exhaust Gas Composition
346
10.6.2
Reduction of Exhaust Gas Emissions
347
References
354
General Literature
355
11
Production of Polymers
—
Polyethene
357
11.1
Introduction
357
11.2
Polymerization Reactions
357
11.2.1
Step growth Polymerization
358
11.2.2
Chain growth Polymerization
-
Radical and Coordination Pathways
360
1
Î
.3
Polyethenes
-
Background Information
363
11.3.1
Catalyst Development
363
11.3.2
Classification and Properties
364
11.3.3
Applications
365
11.4
Processes for the Production of Polyethenes
366
11.4.1
Monomer Production and Purification
366
11.4.2
Polymerization
-
Exothermicity
367
11.4.3
Production of Polyethenes
367
References
375
12
Production of Fine Chemicals
377
12.1
Introduction
377
12.2
Role of Catalysis
380
12.2.1
Atom Economy
380
12.2.2
Alternative Reagents and Catalysts
381
12.2.3
Novel Reaction Routes
384
12.2.4
Selectivity
384
12.2.5
Biocatalysis
392
12.3
Solvents
394
12.3.1
Conventional Solvents
394
12.3.2
Alternative Solvents
395
χ
Contents
12.4
Production Plants
398
12.4.1
Multiproduct
and Multipurpose
Plants (MMPs)
398
12.4.2
Dedicated Continuous
Plants
406
12.5
Batch Reactor Selection
407
12.5.1
Reactors for Liquid and Gas-Liquid Systems
408
12.5.2
Reactors for Gas-Liquid-Solid Systems
409
12.6
Batch Reactor Scale-up Effects
41
1
12.6.1
Temperature Control
411
12.6.2
Heat Transfer
411
12.6.3
Example of the Scale-up of a Batch and Semi-Batch Reactor
412
12.6.4
Summary of the Scale-up of Batch Reactors
416
12.7
Safety Aspects of Fine Chemicals
416
12.7.1
Thermal Risks
416
12.7.2
Safety and Process Development
417
References
419
13
Biotechnology
423
13.1
Introduction
423
13.2
Principles of Fermentation Technology
424
13.2.1
Mode of Operation
425
13.2.2
Reactor Types
426
13.2.3
Sterilization
432
13.3
Cell Biomass
-
Bakers Yeast Production
433
13.3.1
Process Layout
433
13.3.2
Cultivation Equipment
434
13.3.3
Downstream Processing
434
13.4
Metabolic Products
-
Biomass as Source of Renewable Energy
435
13.4.1
Bioethanol and Biobutanol
435
13.4.2 Biogas 438
13.5
Environmental Application
-
Wastewater Treatment
438
13.5.1
Introduction
438
13.5.2
Process Layout
438
13.5.3
Aerobic Treatment Processes
440
13.5.4
Anaerobic Treatment Processes
443
13.6
Enzyme Technology
-
Biocatalysts for Transformations
445
13.6.1
General Aspects
445
13.6.2
Immobilization of Enzymes
446
13.6.3
Production of L-Amino Acids
447
13.6.4
Production of Artificial Sweeteners
448
References
452
General Literature
453
14
Process Intensification
455
14.1
Introduction
455
14.1.1
What is Process Intensification
455
14.1.2
How to Intensify Processes
457
14.2
Structured Catalytic Reactors
459
14.2.1
Types of Structured Catalysts and Reactors
460
Contents
xi
14.2.2 Monoliths 462
14.2.3
Microreactors
468
14.3
Multifuncţional
Reactors/Reactive Separation 472
14.3.1
Reactive
Distillation
473
14.3.2
Coupling Reaction and
Membrane Separation 477
14.3.3
Coupling Reaction and Adsorption
481
References
482
15
Process Development
485
15.1
Dependence of Strategy on Product Type and Raw Materials
485
15.2
The Course of Process Development
487
15.3
Development of Individual Steps
489
15.3.1
Exploratory Phase
489
15.3.2
From Process Concept to Preliminary Flow Sheet
489
15.3.3
Pilot Plants/Miniplants
494
15.4
Scale-up
499
15.4.1
Reactors with a Single Fluid Phase
499
15.4.2
Fixed Bed Catalytic Reactors with One or More Fluid Phases
501
15.5
Safety and Loss Prevention
505
15.5.1
Safety Issues
505
15.5.2
Reactivity Hazards
511
15.5.3
Design Approaches to Safety
513
15.6
Process Evaluation
514
15.6.1
Capital Cost Estimation
515
15.6.2
Operating Costs and Earnings
523
15.6.3
Profitability Measures
524
15.7
Current and Future Trends
526
References
528
General Literature
529
Magazines
529
Appendix A Chemical Industry
-
Figures
531
Appendix
В
Main Symbols Used in Flow Schemes
535
Index
539
|
| any_adam_object | 1 |
| author | Moulijn, Jacob A. Makkee, Michiel Diepen, Annelies van |
| author_facet | Moulijn, Jacob A. Makkee, Michiel Diepen, Annelies van |
| author_role | aut aut aut |
| author_sort | Moulijn, Jacob A. |
| author_variant | j a m ja jam m m mm a v d av avd |
| building | Verbundindex |
| bvnumber | BV040995137 |
| classification_rvk | VN 5000 VN 5010 VN 7000 VN 7001 |
| classification_tum | CIT 300f |
| ctrlnum | (OCoLC)852633475 (DE-599)BVBBV040995137 |
| dewey-full | 660.281 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 660 - Chemical engineering |
| dewey-raw | 660.281 |
| dewey-search | 660.281 |
| dewey-sort | 3660.281 |
| dewey-tens | 660 - Chemical engineering |
| discipline | Chemie / Pharmazie |
| edition | 2nd ed. |
| format | Book |
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| id | DE-604.BV040995137 |
| illustrated | Illustrated |
| indexdate | 2024-12-24T03:15:19Z |
| institution | BVB |
| isbn | 9781444320251 9781444320244 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-025972858 |
| oclc_num | 852633475 |
| open_access_boolean | |
| owner | DE-29T DE-91G DE-BY-TUM DE-11 DE-634 DE-83 DE-703 DE-355 DE-BY-UBR |
| owner_facet | DE-29T DE-91G DE-BY-TUM DE-11 DE-634 DE-83 DE-703 DE-355 DE-BY-UBR |
| physical | XIV, 552 S. Ill., graph. Darst. |
| publishDate | 2013 |
| publishDateSearch | 2013 |
| publishDateSort | 2013 |
| publisher | Wiley |
| record_format | marc |
| spellingShingle | Moulijn, Jacob A. Makkee, Michiel Diepen, Annelies van Chemical process technology aChemical processes Chemische Industrie (DE-588)4009848-5 gnd Technische organische Chemie (DE-588)4184575-4 gnd Technische anorganische Chemie (DE-588)4300470-2 gnd Technische Chemie (DE-588)4078178-1 gnd Reaktionstechnik (DE-588)4136173-8 gnd Chemische Verfahrenstechnik (DE-588)4069941-9 gnd |
| subject_GND | (DE-588)4009848-5 (DE-588)4184575-4 (DE-588)4300470-2 (DE-588)4078178-1 (DE-588)4136173-8 (DE-588)4069941-9 |
| title | Chemical process technology |
| title_auth | Chemical process technology |
| title_exact_search | Chemical process technology |
| title_full | Chemical process technology Jacob A. Moulijn ; Michiel Makkee ; Annelies E. van Diepen |
| title_fullStr | Chemical process technology Jacob A. Moulijn ; Michiel Makkee ; Annelies E. van Diepen |
| title_full_unstemmed | Chemical process technology Jacob A. Moulijn ; Michiel Makkee ; Annelies E. van Diepen |
| title_short | Chemical process technology |
| title_sort | chemical process technology |
| topic | aChemical processes Chemische Industrie (DE-588)4009848-5 gnd Technische organische Chemie (DE-588)4184575-4 gnd Technische anorganische Chemie (DE-588)4300470-2 gnd Technische Chemie (DE-588)4078178-1 gnd Reaktionstechnik (DE-588)4136173-8 gnd Chemische Verfahrenstechnik (DE-588)4069941-9 gnd |
| topic_facet | aChemical processes Chemische Industrie Technische organische Chemie Technische anorganische Chemie Technische Chemie Reaktionstechnik Chemische Verfahrenstechnik |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025972858&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT moulijnjacoba chemicalprocesstechnology AT makkeemichiel chemicalprocesstechnology AT diepenanneliesvan chemicalprocesstechnology |