Monolithic silicas in separation science concepts, syntheses, characterization, modeling and applications
Gespeichert in:
| Weitere Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Weinheim
Wiley-VCH
2011
|
| Schlagworte: | |
| Online-Zugang: | Inhaltstext Inhaltsverzeichnis |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
MARC
| LEADER | 00000nam a2200000 c 4500 | ||
|---|---|---|---|
| 001 | BV036780754 | ||
| 003 | DE-604 | ||
| 005 | 20110225 | ||
| 007 | t| | ||
| 008 | 101117s2011 gw ad|| |||| 00||| eng d | ||
| 015 | |a 10,N32 |2 dnb | ||
| 016 | 7 | |a 1005391335 |2 DE-101 | |
| 020 | |a 9783527325757 |c GB. : EUR 109.00 (freier Pr.) |9 978-3-527-32575-7 | ||
| 024 | 3 | |a 9783527325757 | |
| 028 | 5 | 2 | |a 1132575 000 |
| 035 | |a (OCoLC)703885077 | ||
| 035 | |a (DE-599)DNB1005391335 | ||
| 040 | |a DE-604 |b ger |e rakddb | ||
| 041 | 0 | |a eng | |
| 044 | |a gw |c XA-DE-BW | ||
| 049 | |a DE-29T | ||
| 082 | 0 | |a 546.6832 |2 22/ger | |
| 082 | 0 | |a 543 |2 22/ger | |
| 084 | |a VG 7500 |0 (DE-625)147206:253 |2 rvk | ||
| 084 | |a 540 |2 sdnb | ||
| 245 | 1 | 0 | |a Monolithic silicas in separation science |b concepts, syntheses, characterization, modeling and applications |c ed. by Klaus K. Unger ... |
| 264 | 1 | |a Weinheim |b Wiley-VCH |c 2011 | |
| 300 | |a XVIII, 344 S. |b Ill., graph. Darst. |c 240 mm x 170 mm | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 650 | 0 | 7 | |a HPLC |0 (DE-588)4072641-1 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Trennverfahren |0 (DE-588)4078395-9 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Monolith |0 (DE-588)4352271-3 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Siliciumdioxid |0 (DE-588)4077447-8 |2 gnd |9 rswk-swf |
| 689 | 0 | 0 | |a Siliciumdioxid |0 (DE-588)4077447-8 |D s |
| 689 | 0 | 1 | |a Monolith |0 (DE-588)4352271-3 |D s |
| 689 | 0 | 2 | |a Trennverfahren |0 (DE-588)4078395-9 |D s |
| 689 | 0 | |5 DE-604 | |
| 689 | 1 | 0 | |a Siliciumdioxid |0 (DE-588)4077447-8 |D s |
| 689 | 1 | 1 | |a Monolith |0 (DE-588)4352271-3 |D s |
| 689 | 1 | 2 | |a HPLC |0 (DE-588)4072641-1 |D s |
| 689 | 1 | |8 1\p |5 DE-604 | |
| 700 | 1 | |a Unger, Klaus K. |d 1936-2020 |0 (DE-588)121177246 |4 edt | |
| 856 | 4 | 2 | |m X:MVB |q text/html |u http://deposit.dnb.de/cgi-bin/dokserv?id=3520443&prov=M&dok_var=1&dok_ext=htm |3 Inhaltstext |
| 856 | 4 | 2 | |m DNB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=020697409&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 883 | 1 | |8 1\p |a cgwrk |d 20201028 |q DE-101 |u https://d-nb.info/provenance/plan#cgwrk | |
| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-020697409 | |
Datensatz im Suchindex
| _version_ | 1819737385915645952 |
|---|---|
| adam_text | IMAGE 1
CONTENTS
PREFACE XIII LIST OF CONTRIBUTORS XV
1 THE BASIC IDEA AND THE DRIVERS 1
NOBUO TANAKA AND KLAUS K. UNGER 1.1 DEFINITIONS 1
1.2 MONOLITHS AS HETEROGENEOUS CATALYSTS 1 1.3 MONOLITHS IN
CHROMATOGRAPHIE SEPARATIONS 2 1.4 CONCLUSION AND PERSPECTIVES 4
REFERENCES 5
PART ONE PREPARATION 9
2 SYNTHESIS CONCEPTS AND PREPARATION OF SILICA MONOLITHS 11 KAZUKI
NAKANISHI 2.1 INTRODUCTION 11
2.2 BACKGROUND AND CONCEPTS 12 2.2.1 SOL-GEL REACTIONS OF SILICA 12
2.2.2 POLYMERIZATION-INDUCED PHASE SEPARATION 14 2.2.3 DOMAIN FORMATION
BY PHASE SEPARATION 35
2.2.4 ARRESTING TRANSIENT STRUCTURE WITHIN A SOLIDIFYING NETWORK 17
2.2.5 MACROPORE CONTROL 19 2.2.6 MESOPORE CONTROL 21 2.3 SYNTHESIS OF
SILICA MONOLITHS 21
2.3.1 SILICA SOURCE AND CATALYST 21 2.3.2 ADDITIVES TO INDUCE PHASE
SEPARATION 22 2.3.3 PREPARATION PROCEDURE FOR BULK MONOLITH 24 2.3.3.1
DISSOLUTION OF PEO IN ACIDIC WATER 25 2.3.3.2 ADDITION OFTMOS FOR
HYDROLYSIS 25 2.3.3.3 TRANSFERRING THE SOLUTION TO A MOLD 25 2.3.3.4
GELATION AND AGING 26
BIBLIOGRAFISCHE INFORMATIONEN HTTP://D-NB.INFO/1005391335
DIGITALISIERT DURCH
IMAGE 2
VI I CONTENTS
2.3.4 PREPARATION PROCEDURE FOR CAPILLARY MONOLITH 26
2.3.5 AGING OF WET MONOLITH TO TAILOR MESOPORES 27 2.3.6 DRYING AND HEAT
TREATMENT 28 2.3.7 MISCELLANEOUS FACTORS FOR BETTER REPRODUCIBILITY 28
2.4 MONOLITHIC COLUMNS PREPARED IN THE LABORATORY 29
2.4.1 EPOXY-CLAD COLUMNS 29 2.4.2 CAPILLARY COLUMNS 30 2.4.3 OTHER TYPES
31
2.5 SUMMARY 31
REFERENCES 31
3 PREPARATION AND PROPERTIES OF VARIOUS TYPES OF MONOLITHIC SILICA
STATIONARY PHASES FOR REVERSED-PHASE, HYDROPHILIC INTERACTION, AND
ION-EXCHANGE CHROMATOGRAPHY BASED ON POLYMER-COATED MATERIALS 35 OSCAR
NUNEZ AND TOHRU IKEGAMI 3.1 STATIONARY PHASES FOR REVERSED-PHASE
CHROMATOGRAPHY 35 3.2 STATIONARY PHASES FOR HYDROPHILIC-INTERACTION
CHROMATOGRAPHY
SEPARATIONS 38
3.3 STATIONARY PHASES FOR ION-EXCHANGE SEPARATIONS 42 3.4 ADVANTAGES OF
POLYMER-COATED MONOLITHIC SILICA COLUMNS 43 REFERENCES 45
PART TWO CHARACTERIZATION AND MODELING 47
4 CHARACTERIZATION OF THE PORE STRUCTURE OF MONOLITHIC SILICAS 49 ROMAS
SKUDAS, MATTHIAS THOMMES, AND KLAUS K. UNGER 4.1 MONOLITHIC SILICAS 49
4.2 GENERAL ASPECTS DESCRIBING POROUS MATERIALS 50 4.3 CHARACTERIZATION
METHODS OF THE PORE STRUCTURE OF MONOLITHIC SILICAS 53 4.3.1 MERCURY
INTRUSION-EXTRUSION 53 4.3.2 INVERSE SIZE-EXCLUSION CHROMATOGRAPHY 60
4.3.3 NITROGEN SORPTION 64
4.3.4 LIQUID PERMEATION 67 4.3.5 MICROSCOPY AND IMAGE ANALYSIS 70 4.4
COMPARISON OF THE SILICA MONOLITH MESOPORE-CHARACTERIZATION DATA 73 4.5
COMPARISON OF THE SILICA MONOLITH FLOW-THROUGH PORE-
CHARACTERIZATION DATA 74 REFERENCES 75
5 MICROSCOPIC CHARACTERIZATIONS 81 HARUKO SAITO, KAZUYOSHI KANAMORI, AND
KAZUKI NAKANISHI 5.1 INTRODUCTION 81
IMAGE 3
CONTENTS VII
5.2 PREPARATION OF MACROPOROUS SILICA MONOLITH 82
5.3 LASER SCANNING CONFOCAL MICROSCOPE OBSERVATION 83 5.4 IMAGE
PROCESSING 84
5.5 FUNDAMENTAL PARAMETERS 84 5.5.1 POROSITY 85
5.5.2 SURFACE AREA 86
5.5.3 CHARACTERISTIC WAVELENGTH 86 5.5.4 MACROPORE SIZE AND SKELETON
THICKNESS 89 5.5.5 CHORD LENGTH 90
5.5.6 MEAN CURVATURE AND GAUSSIAN CURVATURE 91 5.5.7 CURVATURE
DISTRIBUTIONS 93 5.5.7.1 COMPARISON BETWEEN DIFFERENT POROSITIES 93
5.5.7.2 COMPARISON BETWEEN DIFFERENT MACROPORE SIZES 94 5.6
THREE-DIMENSIONAL OBSERVATION OF DEFORMATIONS IN CONFINED
GEOMETRY 95
5.6.1 SYNTHESIS AND CHARACTERS OF ORGANIC-INORGANIC HYBRID MONOLITHS 95
5.6.2 DEFORMED MACROPOROUS STRUCTURES BETWEEN PLATES IN MF SYSTEM 96
5.6.3 DEFORMED MACROPOROUS STRUCTURES BETWEEN PLATES IN MM
SYSTEM 99 REFERENCES 202
6 MODELING CHROMATOGRAPHIE BAND BROADENING IN MONOLITHIC COLUMNS 105
FREDERIK DETOBEL AND CERT DESMET
6.1 INTRODUCTION 105
6.2 THE GENERAL PLATE-HEIGHT MODEL 106 6.2.1 MEANING OF K , U AND KP
107 6.2.2 EXPRESSIONS FOR H AX 108 6.2.3 ESTIMATION OF D MO AND D SKEL
109 6.2.4 EXPRESSIONS FOR FC FTP AND FE FSKEL 110 6.2.5 SELECTION OF THE
CHARACTERISTIC REFERENCE
LENGTHS 111
6.2.6 COMPLETE PLATE-HEIGHT EQUATION 113 6.3 USE OF THE GENERAL
PLATE-HEIGHT MODEL TO PREDICT BAND BROADENING IN TSM STRUCTURES 114
6.3.1 NONPOROUS SKELETON CASE 115
6.3.2 POROUS SKELETON CASE 116 6.4 CONCLUSION 120
ACKNOWLEDGMENTS 121 SYMBOLS 121 GREEK SYMBOLS 122 SUBSCRIPTS 122
REFERENCES 122
IMAGE 4
VIII CONTENTS
7 COMPARISON OF THE PERFORMANCE OF PARTICLE-PACKED AND MONOLITHIC
COLUMNS IN HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY 127 CEORGES CUIOCHON
7.1 INTRODUCTION 127
7.2 BASIC COLUMNS PROPERTIES 128 7.2.1 TOTAL, EXTERNAL AND INTERNAL
COLUMN POROSITY 129 7.2.1.1 DEFINITION OF THE TOTAL COLUMN POROSITY 129
7.2.1.2 MEASUREMENT OF THE TOTAL COLUMN POROSITY 129 7.2.1.3 DEFINITIONS
OF THE COLUMN EXTERNAL AND INTERNAL
POROSITIES 131
7.2.1.4 MEASUREMENT OF THE COLUMN EXTERNAL AND INTERNAL POROSITIES 131
7.2.2 COLUMN PERMEABILITY 132 7.2.2.1 PERMEABILITY OF PACKED COLUMNS 132
7.2.2.2 PERMEABILITY OF MONOLITHIC COLUMNS 132
7.2.3 COLUMN EFFICIENCY 135 7.2.3.1 THE HETP EQUATION 136 7.2.3.2
REDUCED HETP AND REDUCED VELOCITY 137 7.2.4 COLUMN IMPEDANCE 137
7.3 COMPARISON OF THE THROUGH-PORE STRUCTURES AND RELATED PROPERTIES 138
7.3.1 POROSITY AND THROUGH-PORE STRUCTURE 138 7.3.1.1 EXTERNAL POROSITY
OF PACKED AND MONOLITHIC COLUMNS 138
7.3.1.2 IMPORTANCE OF THE SIZE OF THE THROUGH-PORES 139 7.3.1.3 AVERAGE
SIZE OF THE THROUGH-PORES IN PACKED COLUMNS 139 7.3.1.4 AVERAGE SIZE OF
THE THROUGH-PORES OF MONOLITHIC COLUMNS 140 7.3.2 COLUMN PERMEABILITY
140 7.3.2.1 PERMEABILITY OF PACKED COLUMNS 140
7.3.2.2 PERMEABILITY OF MONOLITHIC COLUMNS 140 7.3.3 COLUMN RADIAL
HOMOGENEITY 142 7.3.3.1 RADIAL HETEROGENEITY OF PACKED COLUMNS 142
7.3.3.2 RADIAL HETEROGENEITY OF MONOLITHIC COLUMNS 143 7.3.3.3
CONSEQUENCES OF COLUMN RADIAL HETEROGENEITY 144 7.4 THERMODYNAMIC
PROPERTIES 144 7.4.1 RETENTION 144
7.4.1.1 RETENTION FACTORS 145 7.4.1.2 REPRODUCIBILITY OF RETENTION
FACTORS AND ISOTHERMS 146 7.4.2 COLUMN LOADABILITY 146 7.5 KINETIC
PROPERTIES AND COLUMN EFFICIENCY 147 7.5.1 AXIAL DISPERSION 147 7.5.2
MASS-TRANSFER KINETICS 148 7.5.3 COLUMN IMPEDANCE 150 7.5.4 KINETIC
PROPERTIES 151 7.6 CONCLUSIONS 151
ACKNOWLEDGMENTS 153
IMAGE 5
CONTENTS IX
SYMBOLS 153
GREEK SYMBOLS 154 REFERENCES 154
PART THREE APPLICATIONS 157
8 QUANTITATIVE STRUCTURE-RETENTION RELATIONSHIPS IN STUDIES OF
MONOLITHIC MATERIALS 159 ROMAN KALISZAN AND MICHALJ. MARKUSZEWSKI 8.1
FUNDAMENTALS OF QUANTITATIVE STRUCTURE-RETENTION RELATIONSHIPS
(QSRR) 159
8.2 QUANTITATIVE RELATIONSHIPS BETWEEN ANALYTE HYDROPHOBICITY AND
RETENTION ON MONOLITHIC COLUMNS 163 8.3 QSRR BASED ON STRUCTURAL
DESCRIPTORS FROM CALCULATION CHEMISTRY 166 8.4 LSER ON MONOLITHIC
COLUMNS 269 8.5 CONCLUDING REMARKS 172
REFERENCES 272
9 PERFORMANCE OF SILICA MONOLITHS FOR BASIC COMPOUNDS. SILANOL ACTIVITY
173 DAVID V. MCCALLEY
9.1 INTRODUCTION 273
9.2 REPRODUCIBILITY OF COMMERCIAL MONOLITHS FOR ANALYSIS OF BASES 174
9.3 ACTIVITY OF MONOLITHS TOWARDS BASIC SOLUTES 275 9.4 CONTRIBUTION OF
OVERLOAD TO PEAK SHAPES OF BASIC SOLUTES 180 9.5 VAN DEEMTER PLOTS FOR
COMMERCIAL MONOLITHS 280 9.6 PERFORMANCE OF HYBRID CAPILLARY SILICA
MONOLITHS FOR BASIC
COMPOUNDS 183
9.7 CONCLUSIONS 286
REFERENCES 287
10 QUALITY CONTROL OF DRUGS 289 MOHAMMED TAHA, ABDELKAREM ABED, AND SAMI
EL DEEB 10.1 INTRODUCTION 289
10.2 ANALYSIS OF PHARMACEUTICS 189 10.3 NATURAL PRODUCTS ANALYSIS 190
10.4 ANALYSIS SPEED AND PERFORMANCE 191 10.5 METHOD TRANSFER 193
10.6 SEPARATION OF COMPLEX MIXTURES 296 10.7 MONOLITH DERIVATIVES AND
VERSATILE APPLICATION 198 10.8 SUMMARY AND CONCLUSIONS 201 REFERENCES
202
IMAGE 6
X| CONTENTS
11 MONOLITHIC STATIONARY PHASES FOR FAST ION CHROMATOGRAPHY 207
PAVEL N. NESTERENKO AND PAUL R. HADDAD 11.1 FAST ION CHROMATOGRAPHY 207
11.2 HISTORICAL DEVELOPMENT OF FAST ION CHROMATOGRAPHY 207 11.3 3
ADVANTAGES OF THE BIMODAL POROUS STRUCTURE OF THE SILICA MONOLITH
MATRIX 210
11.4 TYPE AND PROPERTIES OF SILICA MONOLITHIC COLUMNS USED IN IC 222
11.5 MODIFICATION OF SILICA MONOLITHS FOR IC SEPARATIONS 226 11.5.1
BARE-SILICA MONOLITHS AS ION EXCHANGERS 216 11.5.2 COATED REVERSED-PHASE
SILICA MONOLITHIC ION-EXCHANGE COLUMNS 217 11.5.3 SILICA MONOLITHS WITH
COVALENTLY BONDED ION-EXCHANGE GROUPS 221 11.6 OPERATIONAL PARAMETERS
221
11.7 ANALYTICAL APPLICATIONS 223 11.8 FUTURE WORK 225
REFERENCES 226
12 MONOLITHIC CHIRAL STATIONARY PHASES FOR LIQUID-PHASE
ENANTIOSEPARATION TECHNIQUES 232 BEZHAN CHANKVETADZE 12.1 INTRODUCTION
232
12.2 ORGANIC MONOLITHIC MATERIALS FOR THE SEPARATION OF ENANTIOMERS 233
12.3 SILICA-BASED MONOLITHIC MATERIALS FOR THE SEPARATION OF ENANTIOMERS
235 12.3.1 MONOLITHIC SILICA COLUMNS WITH PHYSICALLY ADSORBED CHIRAL
SELECTOR 236
12.3.2 MONOLITHIC SILICA COLUMNS WITH COVALENTLY ATTACHED CHIRAL
SELECTOR 237 12.4 SUMMARY OF THE PRESENT STATE-OF-THE-ART AND PROBLEMS
TO BE SOLVED IN THE FUTURE 245
REFERENCES 245
13 HIGH-SPEED AND HIGH-EFFICIENCY SEPARATIONS BY UTILIZING MONOLITHIC
SILICA CAPILLARY COLUMNS 249 TAKESHI HARA, KOSUKE MIYAMOTO, SATOSHI
MAKINO, SHOHEI MIWA, TOHRU IKEGAMI, MASAYOSHI OHIRA, AND NOBUO TANAKA
13.1 INTRODUCTION 249
13.2 PREPARATION OF MONOLITHIC SILICA CAPILLARY COLUMNS 250 13.3
PROPERTIES OF MONOLITHIC SILICA CAPILLARY COLUMNS 252 13.4 MONOLITHIC
SILICA CAPILLARY COLUMNS FOR HIGH-EFFICIENCY SEPARATIONS 254
13.4.1 PERFORMANCE OF LONG MONOLITHIC SILICA CAPILLARY COLUMNS 254
13.4.2 EXAMPLES OF HIGH-EFFICIENCY SEPARATIONS 256 13.4.2.1 ISOCRATIC
MODE 256 13.4.3 PERFORMANCE OF LONG CAPILLARY COLUMNS FOR PEPTIDES IN
GRADIENT
MODE 259
IMAGE 7
CONTENTS XI
13.5 MONOLITHIC SILICA CAPILLARY COLUMNS FOR HIGH-SPEED SEPARATIONS 261
13.5.1 MONOLITHIC SILICA COLUMNS HAVING INCREASED PHASE RATIOS 261
13.5.2 PERFORMANCE OF HIGH-SPEED MONOLITHIC SILICA COLUMNS 265 13.5.3
COMPARISON OF PERFORMANCE WITH A PARTICLE-PACKED COLUMN 266
13.6 FUTURE CONSIDERATIONS 267 13.7 CONCLUSION 268
REFERENCES 269
14 SILICA MONOLITHIC COLUMNS AND MASS SPECTROMETRY 273 KEITH ASHMAN 14.1
INTRODUCTION 273
14.2 OFFLINE CHROMATOGRAPHY, LC M ALDI MS 274 14.3 ONLINE ESI LC/MS/MS
FOR PROTEOMICS AND SELECTED REACTION MONITORING (SRM) 275
14.4 ONLINE REACTORS AND AFFINITY COLUMNS COUPLED TO MASS SPECTROMETRY
278 14.5 CONCLUSION 279
REFERENCES 280
15 SILICA MONOLITHS FOR SMALL-SCALE PURIFICATION OF DRUG-DISCOVERY
COMPOUNDS 285 ALFONSO ESPADA, CRISTINA ANTA, AND MANUEL MOLINA-MARTIN
15.1 INTRODUCTION 285
15.2 INSTRUMENTAL AND OPERATING CONSIDERATIONS 286 15.2.1 ANALYTICAL
CONDITIONS 286 15.2.2 PREPARATIVE CONDITIONS 287 15.3 PREPARATIVE
SEPARATIONS AND SAMPLE LOADING 288
15.3.1 SEMIPREPARATIVE MONOLITHIC 10 X 100 MM COLUMN 288 15.3.2
PREPARATIVE MONOLITHIC 25 X 100 MM COLUMN 290 15.4 PURIFICATION OF
DRUG-DISCOVERY COMPOUNDS 292 15.5 CONCLUSIONS 294
ACKNOWLEDGMENT 295 REFERENCES 295
16 MONOLITHIC SILICA COLUMNS IN MULTIDIMENSIONAL LC-MS FOR PROTEOMICS
AND PEPTIDOMICS 297 EGIDIJUS MACHTEJEVAS AND EGLE MACHTEJEVIENE 16.1
INTRODUCTION 297
16.2 LIQUID CHROMATOGRAPHY AS A TOOL BOX FOR PROTEOMICS 300 16.3
SELECTIVITY OF COLUMNS FOR MD-LC 303 16.4 DIMENSIONS OF COLUMNS IN MD-LC
305 16.5 MONOLITHIC SILICA COLUMNS 307 16.6 APPLICATIONS OF MONOLITHIC
SILICA IN PROTEOMICS-A BRIEF SURVEY 310
16.7 SUMMARY AND CONCLUSIONS 314 REFERENCES 324
IMAGE 8
XII CONTENTS
17 SILICA MONOLITHS IN SOLID-PHASE EXTRACTION AND SOLID-PHASE
MICROEXTRACTION 319 ZHI-CUO SHI, LI XU, AND HIAN KEE LEE 17.1
INTRODUCTION 319
17.2 EXTRACTION PROCESS 320 17.3 EXTRACTION PLATFORMS 321 17.3.1 ONLINE
EXTRACTION 321 17.3.2 OFFLINE EXTRACTION 322 VIA APPLICATIONS 322
17.4.1 SPE AND SPME 322 17.4.1.1 SILICA MONOLITH FROM ENTRAPPED
PARTICLES 322 17.4.1.2 SILICA MONOLITH FROM DIRECT SOL-GEL STRATEGY 327
17.4.2 OTHER APPLICATIONS OF SILICA MONOLITH 332 17.5 CONCLUSION AND
OUTLOOK 332
REFERENCES 333
INDEX 335
|
| any_adam_object | 1 |
| author2 | Unger, Klaus K. 1936-2020 |
| author2_role | edt |
| author2_variant | k k u kk kku |
| author_GND | (DE-588)121177246 |
| author_facet | Unger, Klaus K. 1936-2020 |
| building | Verbundindex |
| bvnumber | BV036780754 |
| classification_rvk | VG 7500 |
| ctrlnum | (OCoLC)703885077 (DE-599)DNB1005391335 |
| dewey-full | 546.6832 543 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 546 - Inorganic chemistry 543 - Analytical chemistry |
| dewey-raw | 546.6832 543 |
| dewey-search | 546.6832 543 |
| dewey-sort | 3546.6832 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| format | Book |
| fullrecord | <?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>02200nam a2200541 c 4500</leader><controlfield tag="001">BV036780754</controlfield><controlfield tag="003">DE-604</controlfield><controlfield tag="005">20110225 </controlfield><controlfield tag="007">t|</controlfield><controlfield tag="008">101117s2011 gw ad|| |||| 00||| eng d</controlfield><datafield tag="015" ind1=" " ind2=" "><subfield code="a">10,N32</subfield><subfield code="2">dnb</subfield></datafield><datafield tag="016" ind1="7" ind2=" "><subfield code="a">1005391335</subfield><subfield code="2">DE-101</subfield></datafield><datafield tag="020" ind1=" " ind2=" "><subfield code="a">9783527325757</subfield><subfield code="c">GB. : EUR 109.00 (freier Pr.)</subfield><subfield code="9">978-3-527-32575-7</subfield></datafield><datafield tag="024" ind1="3" ind2=" "><subfield code="a">9783527325757</subfield></datafield><datafield tag="028" ind1="5" ind2="2"><subfield code="a">1132575 000</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(OCoLC)703885077</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-599)DNB1005391335</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-604</subfield><subfield code="b">ger</subfield><subfield code="e">rakddb</subfield></datafield><datafield tag="041" ind1="0" ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="044" ind1=" " ind2=" "><subfield code="a">gw</subfield><subfield code="c">XA-DE-BW</subfield></datafield><datafield tag="049" ind1=" " ind2=" "><subfield code="a">DE-29T</subfield></datafield><datafield tag="082" ind1="0" ind2=" "><subfield code="a">546.6832</subfield><subfield code="2">22/ger</subfield></datafield><datafield tag="082" ind1="0" ind2=" "><subfield code="a">543</subfield><subfield code="2">22/ger</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">VG 7500</subfield><subfield code="0">(DE-625)147206:253</subfield><subfield code="2">rvk</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">540</subfield><subfield code="2">sdnb</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Monolithic silicas in separation science</subfield><subfield code="b">concepts, syntheses, characterization, modeling and applications</subfield><subfield code="c">ed. by Klaus K. Unger ...</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="a">Weinheim</subfield><subfield code="b">Wiley-VCH</subfield><subfield code="c">2011</subfield></datafield><datafield tag="300" ind1=" " ind2=" "><subfield code="a">XVIII, 344 S.</subfield><subfield code="b">Ill., graph. Darst.</subfield><subfield code="c">240 mm x 170 mm</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">HPLC</subfield><subfield code="0">(DE-588)4072641-1</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Trennverfahren</subfield><subfield code="0">(DE-588)4078395-9</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Monolith</subfield><subfield code="0">(DE-588)4352271-3</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Siliciumdioxid</subfield><subfield code="0">(DE-588)4077447-8</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="689" ind1="0" ind2="0"><subfield code="a">Siliciumdioxid</subfield><subfield code="0">(DE-588)4077447-8</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2="1"><subfield code="a">Monolith</subfield><subfield code="0">(DE-588)4352271-3</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2="2"><subfield code="a">Trennverfahren</subfield><subfield code="0">(DE-588)4078395-9</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2=" "><subfield code="5">DE-604</subfield></datafield><datafield tag="689" ind1="1" ind2="0"><subfield code="a">Siliciumdioxid</subfield><subfield code="0">(DE-588)4077447-8</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="1" ind2="1"><subfield code="a">Monolith</subfield><subfield code="0">(DE-588)4352271-3</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="1" ind2="2"><subfield code="a">HPLC</subfield><subfield code="0">(DE-588)4072641-1</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="1" ind2=" "><subfield code="8">1\p</subfield><subfield code="5">DE-604</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Unger, Klaus K.</subfield><subfield code="d">1936-2020</subfield><subfield code="0">(DE-588)121177246</subfield><subfield code="4">edt</subfield></datafield><datafield tag="856" ind1="4" ind2="2"><subfield code="m">X:MVB</subfield><subfield code="q">text/html</subfield><subfield code="u">http://deposit.dnb.de/cgi-bin/dokserv?id=3520443&prov=M&dok_var=1&dok_ext=htm</subfield><subfield code="3">Inhaltstext</subfield></datafield><datafield tag="856" ind1="4" ind2="2"><subfield code="m">DNB Datenaustausch</subfield><subfield code="q">application/pdf</subfield><subfield code="u">http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=020697409&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA</subfield><subfield code="3">Inhaltsverzeichnis</subfield></datafield><datafield tag="883" ind1="1" ind2=" "><subfield code="8">1\p</subfield><subfield code="a">cgwrk</subfield><subfield code="d">20201028</subfield><subfield code="q">DE-101</subfield><subfield code="u">https://d-nb.info/provenance/plan#cgwrk</subfield></datafield><datafield tag="943" ind1="1" ind2=" "><subfield code="a">oai:aleph.bib-bvb.de:BVB01-020697409</subfield></datafield></record></collection> |
| id | DE-604.BV036780754 |
| illustrated | Illustrated |
| indexdate | 2024-12-24T00:13:20Z |
| institution | BVB |
| isbn | 9783527325757 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-020697409 |
| oclc_num | 703885077 |
| open_access_boolean | |
| owner | DE-29T |
| owner_facet | DE-29T |
| physical | XVIII, 344 S. Ill., graph. Darst. 240 mm x 170 mm |
| publishDate | 2011 |
| publishDateSearch | 2011 |
| publishDateSort | 2011 |
| publisher | Wiley-VCH |
| record_format | marc |
| spellingShingle | Monolithic silicas in separation science concepts, syntheses, characterization, modeling and applications HPLC (DE-588)4072641-1 gnd Trennverfahren (DE-588)4078395-9 gnd Monolith (DE-588)4352271-3 gnd Siliciumdioxid (DE-588)4077447-8 gnd |
| subject_GND | (DE-588)4072641-1 (DE-588)4078395-9 (DE-588)4352271-3 (DE-588)4077447-8 |
| title | Monolithic silicas in separation science concepts, syntheses, characterization, modeling and applications |
| title_auth | Monolithic silicas in separation science concepts, syntheses, characterization, modeling and applications |
| title_exact_search | Monolithic silicas in separation science concepts, syntheses, characterization, modeling and applications |
| title_full | Monolithic silicas in separation science concepts, syntheses, characterization, modeling and applications ed. by Klaus K. Unger ... |
| title_fullStr | Monolithic silicas in separation science concepts, syntheses, characterization, modeling and applications ed. by Klaus K. Unger ... |
| title_full_unstemmed | Monolithic silicas in separation science concepts, syntheses, characterization, modeling and applications ed. by Klaus K. Unger ... |
| title_short | Monolithic silicas in separation science |
| title_sort | monolithic silicas in separation science concepts syntheses characterization modeling and applications |
| title_sub | concepts, syntheses, characterization, modeling and applications |
| topic | HPLC (DE-588)4072641-1 gnd Trennverfahren (DE-588)4078395-9 gnd Monolith (DE-588)4352271-3 gnd Siliciumdioxid (DE-588)4077447-8 gnd |
| topic_facet | HPLC Trennverfahren Monolith Siliciumdioxid |
| url | http://deposit.dnb.de/cgi-bin/dokserv?id=3520443&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=020697409&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT ungerklausk monolithicsilicasinseparationscienceconceptssynthesescharacterizationmodelingandapplications |