Concepts of chemical engineering 4 chemists
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| 245 | 1 | 0 | |a Concepts of chemical engineering 4 chemists |c [ed. by] Stefaan J. R. Simons |
| 264 | 1 | |a Cambridge |b RSC Publ. |c 2007 | |
| 300 | |a XX, 350 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 650 | 4 | |a Chemical engineering | |
| 650 | 7 | |a Chemische reacties. |2 gtt | |
| 650 | 7 | |a Chemische technologie. |2 gtt | |
| 650 | 7 | |a Kostenanalyse. |2 gtt | |
| 650 | 7 | |a Procestechnologie. |2 gtt | |
| 650 | 7 | |a Reologie. |2 gtt | |
| 650 | 7 | |a Risicoanalyse. |2 gtt | |
| 650 | 7 | |a Schaalvergroting. |2 gtt | |
| 650 | 7 | |a Stoftransport. |2 gtt | |
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| 700 | 1 | |a Simons, Stefaan J. R. |e Sonstige |4 oth | |
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Datensatz im Suchindex
| _version_ | 1819659604790870016 |
|---|---|
| adam_text | Contents
Chapter 1 Process Analysis - The Importance of Mass and Energy
Balances 1
Eric S. Fraga
1.1 Introduction 1
1.1.1 Nomenclature and Units of Measurement 1
1.2 Mass Balances 3
1.2.1 Process Analysis Procedure 4
1.2.2 Example 1: Mass Balance on a Continuous
Distillation Process 5
1.2.3 Example 2: Mass Balance on a Process with
Reaction 9
1.3 Energy Balances 13
1.3.1 Example 3: Energy Balance on a Distillation
Column 16
1.4 Summary 20
Recommended Reading 20
Chapter 2 Introduction to Chemical Reaction Engineering 21
George Manos
2.1 Introduction 21
2.1.1 Classification of Reactors 22
2.2 Chemical Reaction Kinetics 23
2.2.1 Definitions 23
2.2.2 Chemical Reaction Thermodynamics 27
2.2.3 Kinetics 30
2.2.4 Importance of Mass and Heat Transfer
Processes 33
2.2.5 Kinetics of a Catalytic Reaction 35
xii
Contents xjjj
2.3 Concepts of Chemical Reactor Design 37
2.3.1 Mole Balances for Chemical Reactors 37
2.3.2 Reactor Design Equation 41
2.3.3 Comparison between Continuous Stirred Tank
Reactor and Plug Flow Reactor 44
2.3.4 Recycle Reactor 46
2.3.5 CSTRs in Series 48
2.3.6 Multiple Reactions 50
2.3.7 PFR with Continuous Uniform Feed of
Reactant along the Whole Reactor 52
Recommended Reading 54
Chapter 3 Concepts of Fluid Flow 55
Tim Elson
3.1 Introduction 55
3.2 Dimensionless Groups 56
3.2.1 Example: Pipe Flow 56
3.3 Viscosity 57
3.3.1 Newton s Law of Viscosity 57
3.3.2 Dynamic and Kinematic Viscosity 58
3.3.3 Typical Values of Viscosity 58
3.4 Laminar and Turbulent Flow 59
3.4.1 Boundary Layers 59
3.5 Balance or Conservation Equations 61
3.5.1 General Form of the Conservation
Equations 61
3.5.2 Control Volumes 62
3.5.3 Continuity Equation (Mass Balance) 62
3.5.4 Steady-State Momentum (Force) Balance
Equation 63
3.5.5 Steady-State Energy Balances 64
3.5.6 Example of use of the Conservation
Equations 66
3.6 Pipe Flow 68
3.6.1 Friction Factors 68
3.6.2 Losses in Fittings 70
3.6.3 Economic Velocities 73
3.7 Flow Measurement 73
3.7.1 Variable Head Meters 73
3.7.2 Variable Area Meters 75
3.7.3 Some Other Flowmeters 75
xiv Contents
3.8 Pumps and Pumping 76
3.8.1 Positive Displacement Pumps 76
3.8.2 Non-Positive Displacement Pumps 78
3.8.3 Matching Centrifugal Pumps to Flow
Requirements 79
3.8.4 Pump Power Requirements 81
3.9 Other Flows 81
3.9.1 Equivalent Hydraulic Diameter 81
3.9.2 Flow Around Bodies 82
3.9.3 Stirred Tanks 84
3.10 Example Calculations for the Pipe-Flow
System 85
3.10.1 Data 87
3.10.2 Friction Losses 88
3.10.3 Orifice Meter 89
3.10.4 Pump Shaft Work 89
3.10.5 System Head 90
3.10.6 Pump Characteristics 90
3.10.7 Control Valve 90
3.10.8 Net Positive Suction Head 91
Nomenclature 92
References 94
Chapter 4 An Introduction to Heat Transfer 96
Tim Elson and Paola Lettieri
4.1 Introduction and Objectives 96
4.1.1 Modes of Heat Transfer 96
4.1.2 Scope and Objectives 97
4.2 Modes of Heat Transfer 97
4.2.1 Conduction 97
4.2.2 Convection 101
4.2.3 Radiation 103
4.3 The Overall Heat Transfer Coefficient, U 106
4.3.1 Example Calculation of U 108
4.3.2 Overall Heat Transfer Coefficients with
Curvature, for Example, Transfer through a
Pipe Wall 108
4.3.3 Overall Heat Transfer Coefficients with
Convection and Radiation 109
4.4 Transient Heat Transfer 110
Contents xv
4.4.1 Example Calculation, Small Bi Case: Cooling
of a Copper Sphere in Air 111
4.4.2 Example Calculation, Large Bi Case: Cooling
of a Perspex Plate in Water 113
4.5 Heat Exchangers 114
4.5.1 Double Pipe Heat Exchanger 114
4.5.2 Heat Transfer in Heat Exchangers 117
4.5.3 Performance of Heat Exchangers Fouling 122
4.5.4 Types of Heat Exchangers 122
4.5.5 Numerical Examples 126
4.6 Conclusions 134
Nomenclature 135
References 137
Chapter 5 An Introduction to Mass-Transfer Operations 139
Eva Sorensen
5.1 Introduction 139
5.2 Mechanisms of Separation 140
5.3 General Separation Techniques 143
5.3.1 Separation by Phase Addition or Phase
Creation 143
5.3.2 Separation by Barrier 146
5.3.3 Separation by Solid Agent 148
5.4 Mass Transfer Calculations 149
5.4.1 Equilibrium-Stage Processes 149
5.4.2 Stage Calculations 151
5.4.3 Graphical Methods 153
5.4.4 Diffusional Rate Processes 153
5.4.5 Diffusion Calculations 154
5.5 Separation by Distillation 156
5.5.1 Trays and Packing 157
5.5.2 Design Range 158
5.5.3 Operating Range 158
5.5.4 Design Calculations 159
5.5.5 Distillation Column Height 161
5.6 Separation by Absorption 162
5.6.1 Design Range 163
5.6.2 Operating Range 163
5.6.3 Design Calculations 164
xvi Contents
5.6.4 Amount of Solvent 166
5.6.5 Absorption Column Height 168
5.7 Further Reading 168
5.8 Relevant Material not Considered in this Chapter 169
5.8.1 Combined Reaction and Separation 169
5.8.2 Combined Separation Units 169
5.8.3 Batch Operation 169
References 170
Chapter 6 Scale-Up in Chemical Engineering 171
Tim Elson
6.1 Introduction and Objectives 171
6.2 Units and Fundamental Dimensions 172
6.3 Physical Similarity 172
6.3.1 Geometric Similarity 173
6.3.2 Dynamic Similarity 174
6.3.3 Dimensionless Groups 174
6.4 Dimensional Homogeneity 175
6.5 Dimensional Analysis and Dimensionless
Groups 175
6.5.1 Example: Dimensional Analysis 176
6.6 Buckingham Pi Theorem and Method 178
6.6.1 Buckingham Pi Theorem 178
6.6.2 Buckingham s Method - Procedure 179
6.6.3 Example: Drag Force on a Sphere 179
6.7 Use of Dimensionless Groups in Scale-Up 181
6.7.1 Drag Force on a Particle 182
6.7.2 Pressure Drop in a Pipe 183
6.7.3 Modelling Flow Around a Body Immersed in a
Fluid 184
6.7.4 Heat Transfer 186
6.7.5 Mass Transfer 189
6.7.6 Correlation of Experimental
Data - Formation of Gas Bubbles at an
Orifice 193
6.7.7 Application of Scale-Up in Stirred Vessels 195
6.7.8 Incompatibility of Some Equations 196
6.8 Conclusions 198
Nomenclature 198
References 201
Contents
Chapter 7 An Introduction to Particle Systems
Paola Lettieri
203
204
204
207
209
210
211
214
217
218
220
223
225
232
235
235
235
237
240
242
244
245
247
Chapter 8 An Introduction to Process Control 249
Eva Sorensen
8.1 Introduction 249
8.2 Process Dynamics 250
8.2.1 Process Dynamics Example 250
8.2.2 Stability 252
8.2.3 Typical Open Loop Responses 253
8.3 Feedback Control Systems 255
8.3.1 Disturbance Rejection and Set Point Tracking 255
8.3.2 Feedback Control Loop 256
7.1 Introduction
7.2 Characterisation of Solid Materials
7.2.1 Size and Size Distribution
7.2.2 Particle Shape
7.2.3 Particle Density
7.3 Interaction between Particles and Fluids
7.3.1 Single Particles
7.3.2 Flow Through Packed Beds
7.4 Fluidised Beds
7.4.1 Minimum Fluidisation Velocity
7.4.2 Types of Fluidisation Regimes
7.4.3 Classification of Powders
7.4.4 Interparticle Forces, Measurement of
Cohesiveness and Flowability of Solid
Particles at Ambient Conditions
7.4.5 Some Industrial Fluid-Bed Applications
7.5 Worked Examples
7.5.1 Example El
7.5.2 Example E2
7.5.3 Example E3
7.5.4 Example E4
7.5.5 Example E5
7.6 Concluding Remarks
Nomenclature
References
uction to Particle Systems
.etiieri
Introduction
. Characterisation of Solid Materials
7.2.1 Size and Size Distribution
7.2.2 Particle Shape
7.2.3 Particle Density
7.3 Interaction between Particles and Fluids
7.3.1 Single Particles
7.3.2 Flow Through Packed Beds
7.4 Fluidised Beds
7.4.1 Minimum Fluidisation Velocity
7.4.2 Types of Fluidisation Regimes
7.4.3 Classification of Powders
7.4.4 Interparticle Forces, Measurement of
Cohesiveness and Flowability of Solid
Particles at Ambient Conditions
7.4.5 Some Industrial Fluid-Bed Applications
7.5 Worked Examples
7.5.1 Example El
7.5.2 Example E2
7.5.3 Example E3
7.5.4 Example E4
7.5.5 Example E5
7.6 Concluding Remarks
Nomenclature
References
Chapter 8 An Introduction to Process Control
Eva Sorensen
8.1 Introduction
8.2 Process Dynamics
8.2.1 Process Dynamics Example
8.2.2 Stability
8.2.3 Typical Open Loop Responses
8.3 Feedback Control Systems
8.3.1 Disturbance Rejection and Set Po»
8.3.2 Feedback Control Loop
xviii Contents
8.3.3 P, PI and PID Controllers 257
8.3.4 Closed Loop Responses 258
8.3.5 Controller Tuning 259
8.3.6 Advantages and Disadvantages of Feedback
Controllers 262
8.4 Advanced Control Systems 263
8.4.1 Feedforward Control 263
8.4.2 Ratio Control 264
8.4.3 Cascade Control 265
8.4.4 Inferential Control 266
8.4.5 Adaptive Control 266
8.5 Batch Control 268
8.6 Plant-Wide Control Issues 268
8.7 Worked Example 269
8.7.1 Solution 269
References 271
Chapter 9 Economic Appraisal of Large Projects 272
Ken Sutherland
9.1 Introduction 272
9.2 Time Value of Money 272
9.3 The Company 273
9.3.1 The Balance Sheet 274
9.3.2 The Profit/Loss Account 275
9.4 Sources of Money 276
9.4.1 Owners Funds 277
9.4.2 Shares and Bonds 277
9.5 Valuing a Company 278
9.6 The Cost of Capital 280
9.6.1 Cost of Company s Own Funds 280
9.6.2 Average Cost of Several Sources 282
9.7 Cost of Construction 283
9.8 Revenue Calculation and Net Cash Flow 285
9.8.1 Operating Cost 285
9.8.2 Depreciation 286
9.8.3 Annual Profit 287
9.8.4 Net Cash Flow 288
9.9 Financial Requirement of New Project 288
9.10 The Appraisal Process 289
9.10.1 The Discounted Cash Flow Process 290
9.10.2 Present Value 291
Contents xjx
9.10.3 Net Present Value 293
9.10.4 Project Lifetime 294
9.11 The Internal Rate of Return 294
9.12 The DCF Appraisal Process 295
9.12.1 Graphical Interpolation 297
9.12.2 Computer Calculation 297
9.12.3 Interest during Construction 298
9.12.4 Repayment of Loans 298
9.12.5 Effect of Plant Size 299
9.13 Other Aspects 299
9.13.1 Non-Profit Projects 299
9.13.2 Sensitivity Analyses 299
9.13.3 Inflation 300
9.13.4 Post-Construction Audit 300
Appendix - Worked Example 300
Recommended Reading 307
Chapter 10 Hazard Studies and Risk Assessment 309
Robert Thornton
10.1 Responsibilities of Designers 309
10.2 Definitions 310
10.3 Identification of Hazards 312
10.3.1 An Overview of the Hazard Study Framework 312
10.3.2 Hazard Study 1 314
10.3.3 Hazard Study 2 318
10.3.4 Hazard Study 3 (Hazard and Operability
Study, HAZOP) 323
10.3.5 Hazard Study 3 (HAZOP) Preliminaries 324
10.3.6 Information Needed by the Team 325
10.3.7 Carrying out a HAZOP 325
10.4 Assessment of Risk 332
10.4.1 Qualitative Risk Assessment 332
10.4.2 Quantitative Risk Assessment 333
10.4.3 Calculation of Hazard Severity 334
10.4.4 Calculation of Frequency of Occurrence of
Hazards 334
10.4.5 The Concept of Testing Trips and Safety
Devices 335
10.4.6 Calculation of the Risk 336
10.4.7 Example 3 336
10.4.8 The Numerical Perspective 338
xx Contents
10.5 Control of Chemical Plant 340
10.6 Summary 341
References 341
Subject Index 342
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| id | DE-604.BV022266381 |
| illustrated | Illustrated |
| indexdate | 2024-12-23T19:56:33Z |
| institution | BVB |
| isbn | 0854049517 9780854049516 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-015476947 |
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| open_access_boolean | |
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| owner_facet | DE-703 |
| physical | XX, 350 S. Ill., graph. Darst. |
| publishDate | 2007 |
| publishDateSearch | 2007 |
| publishDateSort | 2007 |
| publisher | RSC Publ. |
| record_format | marc |
| spellingShingle | Concepts of chemical engineering 4 chemists Chemical engineering Chemische reacties. gtt Chemische technologie. gtt Kostenanalyse. gtt Procestechnologie. gtt Reologie. gtt Risicoanalyse. gtt Schaalvergroting. gtt Stoftransport. gtt Warmtetransport. gtt Chemische Verfahrenstechnik (DE-588)4069941-9 gnd |
| subject_GND | (DE-588)4069941-9 |
| title | Concepts of chemical engineering 4 chemists |
| title_auth | Concepts of chemical engineering 4 chemists |
| title_exact_search | Concepts of chemical engineering 4 chemists |
| title_full | Concepts of chemical engineering 4 chemists [ed. by] Stefaan J. R. Simons |
| title_fullStr | Concepts of chemical engineering 4 chemists [ed. by] Stefaan J. R. Simons |
| title_full_unstemmed | Concepts of chemical engineering 4 chemists [ed. by] Stefaan J. R. Simons |
| title_short | Concepts of chemical engineering 4 chemists |
| title_sort | concepts of chemical engineering 4 chemists |
| topic | Chemical engineering Chemische reacties. gtt Chemische technologie. gtt Kostenanalyse. gtt Procestechnologie. gtt Reologie. gtt Risicoanalyse. gtt Schaalvergroting. gtt Stoftransport. gtt Warmtetransport. gtt Chemische Verfahrenstechnik (DE-588)4069941-9 gnd |
| topic_facet | Chemical engineering Chemische reacties. Chemische technologie. Kostenanalyse. Procestechnologie. Reologie. Risicoanalyse. Schaalvergroting. Stoftransport. Warmtetransport. Chemische Verfahrenstechnik |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=015476947&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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