Principles of thermal analysis and calorimetry
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| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Cambridge
Royal Soc. of Chemistry
2002
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| Schriftenreihe: | RSC paperbacks
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| Online-Zugang: | Inhaltsverzeichnis |
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| 100 | 1 | |a Haines, Peter J. |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Principles of thermal analysis and calorimetry |c ed. by P. J. Haines |
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| adam_text | RSC PAPERBACKS PRINCIPLES OF THERMAL ANALYSIS AND CALORIMETRY EDITED BY
P. J. HAINES OAKLAND ANALYTICAL SERVICES, FARNHAM, SURREY, UK
CONTRIBUTORS G. R. HEAL UNIVERSITY OFSALFORD, UK P. G. LAYE UNIVERSITY
OF HUDDERSFIELD, UK D. M. PRICE LOUGHBOROUGH UNIVERSITY, UK S. B.
WARRINGTON LOUGHBOROUGH UNIVERSITY, UK R. J. WILSON GLAXOSMITHKLINE,
HARLOW, UK RS*C ROYAL SOCIETY OF CHEMISTRY CONTENTS CHAPTER 1
INTRODUCTION 1 P. J. HAINES MATERIALS, HEAT AND CHANGES 1 DEFINITIONS OF
THERMAL AND CALORIMETRIC METHODS 3 THE FAMILY OF THERMAL METHODS 4
INSTRUMENTATION FOR THERMAL ANALYSIS AND CALORIMETRY 4 THE REASONS FOR
USING THERMAL AND CALORIMETRIC METHODS 6 THE NEED FOR PROPER PRACTICE 6
FURTHER READING 8 REFERENCES 8 CHAPTER 2 THERMOGRAVIMETRY AND DERIVATIVE
THERMOGRAVIMETRY 10 G. R. HEAL INTRODUCTION AND DEFINITIONS 10
INSTRUMENTATION 12 BALANCE 12 FURNACE 14 ATMOSPHERE CONTROL 15 CRUCIBLES
15 THERMOCOUPLES 16 TEMPERATURE CONTROL 16 DATA COLLECTION 17 ISOTHERMAL
EXPERIMENTS 18 CALIBRATION FOR MASS AND TEMPERATURE 19 EFFECT OF
EXPERIMENTAL VARIABLES 20 REPORTING THERMOGRAVIMETRY RESULTS 24 A.
PROPERTIES OF THE SAMPLE 24 B. EXPERIMENTAL CONDITIONS 24 VII VLLL
CONTENTS C. DATA ACQUISITION AND MANIPULATION METHODS 24 D. RESULTS 25 A
TYPICAL THERMOGRAVIMETRIC EXPERIMENT 26 PRELIMINARY STEPS 26 CRUCIBLE
TREATMENT 26 ZERO SETTING 27 ADDING THE SAMPLE 28 STARTING THE RUN 28
ENDING THE RUN 28 EXAMPLE EXPERIMENT 29 RESULTS 29 APPLICATIONS 31
OXYSALT DECOMPOSITION 31 POLYMER STABILITY AND CHARCOAL PRODUCTION 33
METAL OXIDATION 37 COMPOSITIONAL ANALYSIS 38 GLASS-MAKING REACTIONS 40
KINETICS OF SOLID-STATE REACTIONS 42 ANCILLARY TECHNIQUES 50 RESIDUE
ANALYSIS 50 OTHER TEMPERATURE REGIMES 51 HIGH RESOLUTION
THERMOGRAVIMETRY 51 FURTHER READING 52 REFERENCES 53 CHAPTER 3
DIFFERENTIAL THERMAL ANALYSIS AND DIFFERENTIAL SCANNING CALORIMETRY 55
P. G. LAYE INTRODUCTION 55 DEFINITIONS AND NOMENCLATURE 57 APPLICATIONS
60 THEORETICAL CONSIDERATIONS 65 INSTRUMENTATION 69 SPECIFICATION 69
TEMPERATURE SENSORS 69 CRUCIBLES 70 TEMPERATURE AND ATMOSPHERE CONTROL
70 COOLING SYSTEMS AND ACCESSORIES 71 CALVET-TYPE EQUIPMENT 71
EXPERIMENTAL CONSIDERATIONS 72 VARIABLES 72 CONTENTS IX DO S AND DO
NOT S 73 REFERENCE 75 CALIBRATION 76 PRELIMINARIES 76 TEMPERATURE
CALIBRATION 77 ENERGY CALIBRATION 79 MEASUREMENTS 82 MEASUREMENT OF HEAT
CAPACITY 82 MEASUREMENT OF ENERGY 85 MEASUREMENT OF PURITY 87 KINETICS
89 FINAL THOUGHTS ON MEASUREMENT 91 FURTHER READING 91 REFERENCES 92
CHAPTER 4 THERMOMECHANICAL, DYNAMIC MECHANICAL AND DIELECTRIC METHODS 94
D. M. PRICE INTRODUCTION AND PRINCIPLES THERMOMECHANICAL ANALYSIS AND
THERMODILATOMETRY DYNAMIC MECHANICAL ANALYSIS DIELECTRIC TECHNIQUES
INSTRUMENTATION THERMOMECHANICAL ANALYSIS DYNAMIC MECHANICAL ANALYSIS
DIELECTRIC TECHNIQUES TYPICAL EXPERIMENTS THERMOMECHANICAL ANALYSIS
DYNAMIC MECHANICAL ANALYSIS DIELECTRIC TECHNIQUES APPLICATIONS
THERMOMECHANICAL ANALYSIS DYNAMIC MECHANICAL ANALYSIS DIELECTRIC THERMAL
ANALYSIS MODULATED TEMPERATURE THERMOMECHANICAL AND DIELECTRIC
TECHNIQUES CONCLUDING REMARKS ACKNOWLEDGEMENTS FURTHER READING
REFERENCES 94 94 96 99 101 101 103 105 106 107 109 113 117 117 120 123
126 126 127 127 127 X CONTENTS CHAPTER 5 CALORIMETRY 129 R. J. WILLSON
INTRODUCTION 129 DEFINITION OF CALORIMETRY 130 THERMOCHEMISTRY AND
THERMODYNAMICS 131 THE FIRST LAW OF THERMODYNAMICS 132 THE SECOND LAW OF
THERMODYNAMICS 133 THE THIRD LAW OF THERMODYNAMICS 133 CALORIMETERS 136
CLASSIFICATION OF CALORIMETERS 137 CALIBRATION 138 INSTRUMENTATION:
CALORIMETERS FOR SPECIAL PURPOSES 139 SOLUTION CALORIMETERS 139
COMBUSTION CALORIMETERS 141 REACTION HAZARD CALORIMETERS 144 ISOTHERMAL
CALORIMETERS 145 APPLICATIONS OF ISOTHERMAL CALORIMETRY 146 CALORIMETRIC
INFORMATION 148 THE CALORIMETRIC SIGNAL 148 REACTION MECHANISM 150
KINETIC INFORMATION 152 EXAMPLES OF CALORIMETRIC APPLICATIONS 153
CHEMICAL REACTIONS 153 PHYSICAL CHANGES 156 SUMMARY 160 ACKNOWLEDGEMENTS
161 REFERENCES 161 CHAPTER 6 SIMULTANEOUS THERMAL ANALYSIS TECHNIQUES
166 S. B. WARRINGTON INTRODUCTION: THE RATIONALE BEHIND THE SIMULTANEOUS
APPROACH 166 SIMULTANEOUS THERMOGRAVIMETRY-DIFFERENTIAL THERMAL ANALYSIS
(TG-DTA) 167 INSTRUMENTATION 167 APPLICATIONS OF TG-DTA 170 SIMULTANEOUS
THERMOGRAVIMETRY-DIFFERENTIAL SCANNING CALORIMETRY (TG-DSC) 172
INSTRUMENTATION 172 CONTENTS XI APPLICATIONS OFTG-DSC 173 EVOLVED GAS
ANALYSIS (EGA) 174 INTRODUCTION 174 INSTRUMENTATION FOR EGA 175
APPLICATIONS OF EGA 177 LESS COMMON TECHNIQUES 181 OPTICAL TECHNIQUES
181 SPECTROSCOPIC TECHNIQUES 183 X-RAY TECHNIQUES 183 DTA-RHEOMETRY 185
MICRO-THERMAL ANALYSIS (/Z-TA) 185 SUMMARY 187 REFERENCES 187 APPENDICES
190 LA SYMBOLS FOR PHYSICAL QUANTITIES AND UNITS 190 NOMENCLATURE FOR
THERMAL ANALYSIS AND CALORIMETRY 191 L.B SOURCES OF INFORMATION 191
L.B.L JOURNALS 191 1.B.2 MAJOR TEXTBOOKS ON THERMAL ANALYSIS AND
CALORIMETRY 192 1 .B.3 VIDEOS, CD-ROMS ETC. 197 1.B.4 CONFERENCE
PROCEEDINGS 197 2 ICTAC AND ITS AFFILIATED SOCIETIES IN EUROPE AND THE
USA 199 3 AMERICAN AND OTHER STANDARD TEST METHODS 200 3.1 AMERICAN
SOCIETY FOR TESTING AND MATERIALS (ASTM) METHODS 201 3.2 BRITISH
STANDARDS 205 4 MANUFACTURERS, CONSULTANTS AND OTHER SUPPLIERS 207 5
CONSULTANCIES AND OTHER GROUPS 214 SUBJECT INDEX 216
|
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| indexdate | 2025-02-03T16:57:40Z |
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| isbn | 0854046100 |
| language | English |
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| physical | XIII, 220 S. Ill., graph. Darst. |
| publishDate | 2002 |
| publishDateSearch | 2002 |
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| publisher | Royal Soc. of Chemistry |
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| series2 | RSC paperbacks |
| spellingShingle | Haines, Peter J. Principles of thermal analysis and calorimetry Thermoanalyse (DE-588)4135675-5 gnd Kalorimetrie (DE-588)4029367-1 gnd |
| subject_GND | (DE-588)4135675-5 (DE-588)4029367-1 (DE-588)4151278-9 |
| title | Principles of thermal analysis and calorimetry |
| title_auth | Principles of thermal analysis and calorimetry |
| title_exact_search | Principles of thermal analysis and calorimetry |
| title_full | Principles of thermal analysis and calorimetry ed. by P. J. Haines |
| title_fullStr | Principles of thermal analysis and calorimetry ed. by P. J. Haines |
| title_full_unstemmed | Principles of thermal analysis and calorimetry ed. by P. J. Haines |
| title_short | Principles of thermal analysis and calorimetry |
| title_sort | principles of thermal analysis and calorimetry |
| topic | Thermoanalyse (DE-588)4135675-5 gnd Kalorimetrie (DE-588)4029367-1 gnd |
| topic_facet | Thermoanalyse Kalorimetrie Einführung |
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