In-situ microscopy in materials research leading international research in electron and scanning probe microscopies

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adam_text IN-SITU MICROSCOPY IN MATERIALS RESEARCH LEADING INTERNATIONAL RESEARCH IN ELECTRON AND SCANNING PROBE MICROSCOPIES EDITED BY PRATIBHA L. GAI CENTRAL RESEARCH AND DEVELOPMENT DUPONT WILMINGTON, DELEWARE, USA W KLUWER ACADEMIC PUBLISHERS BOSTON/DORDRECHT/LONDON ** CONTENTS LIST OF CONTRIBUTORS XI FOREWORD DAVID B. WILLIAMS XV PREFACE PRATIBHA L. GAI XVII 1. IN-SITU APPLICATIONS OF LOW ENERGY ELECTRON MICROSCOPY (LEEM) : 1 BY E. BAUER 1. INTRODUCTION 1 2. PHASE TRANSITIONS ON CLEAN SURFACES 1 3. SEGREGATION 3 4. GAS-SURFACE INTERACTIONS 4 5. EPITAXY 6 6. SUMMARY 10 ACKNOWLEDGEMENTS AND REFERENCES 11 2. ENVIRONMENTAL SCANNING ELECTRON MICROSCOPY 13 BY GERASIMOS DANIEL DANILATOS 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. INTRODUCTION GAS DYNAMICS ELECTRON BEAM TRANSFER CONTRAST AND RESOLUTION DETECTION CATHODOLUMINESCENCE X-RAYS BEAM IRRADIATION EFFECTS OPERATION AND APPLICATIONS CONCLUSIONS ACKNOWLEDGEMENTS AND REFERENCES 14 15 19 23 25 29 29 31 33 41 42 VI 3. ESEM DEVELOPMENT AND APPLICATION IN CULTURAL HERITAGE CONSERVATION 45 BY ERIC DOEHNE 1. INTRODUCTION 45 2. APPLICATIONS 47 2.1 SODIUM SULFATE DYNAMICS 47 2.2 FORMALDEHYDE CORROSION 49 2.3 CLEANING THE SISTINE CHAPEL 53 2.4 DEAD SEA SCROLLS 53 3. ESEM AND SEM: OPERATIONAL DIFFERENCES 55 4. ESEM/EDS DEVELOPMENT (1990-1997) 57 4.1 DYNAMIC IMAGING SYSTEM 57 4.2 STILL IMAGE SYSTEM 58 4.3 EDS ANALYSIS 59 5. FUTURE WORK 60 ACKNOWLEDGEMENTS AND REFERENCES 61 4. INTRINSIC POINT DEFECT CLUSTERING IN SI: A STUDY BY HVEM AND HREM IN-SITU ELECTRON IRRADIATION 63 BY LUDMILA FEDINA, ANTON GUTAKOVSKII ALEXANDER ASEEV, JOSEPH VAN LANDUYT AND JAN VANHELLEMONT 1. INTRODUCTION 63 2. EXPERIMENTAL DETAILS 65 3. RESULTS AND DISCUSSION 66 3.1 POINT DEFECT CLUSTERING 66 3.2 POINT DEFECT CLUSTERING (500C-700C) BY HVEM 81 4. CONCLUSION 90 ACKNOWLEDGEMENTS AND REFERENCES 91 5. IN-SITU OBSERVATION AND QUANTITATIVE ANALYSIS OF ELECTROMIGRATION VOID DYNAMICS 93 BY RICHARD FRANKOVIC AND GARY H. BERNSTEIN 1. INTRODUCTION 94 2. SAMPLE FABRICATION AND IN-SITU TEST TECHNIQUE 96 3. SINGLE VOID BEHAVIOR 99 3.1 DIRECT VOID SHAPE CHANGES 99 3.2 SECONDARY, INDUCED VOIDS AND HILLOCKS 103 /- VLL 4. VOID-VOID INTERACTIONS 108 4.1 QUAL ITATI VE RESULTS 110 4.2 QUANTITATIVE RESULTS 110 5. VOID-HILLOCK INTERACTIONS 117 5.1 QUALITATIVE RESULTS 119 5.2 QUANTITATIVE RESULTS 120 6. SUMMARY AND CONCLUSIONS 120 ACKNOWLEDGEMENTS AND REFERENCES 122 6. ENVIRONMENTAL HIGH RESOLUTION ELECTRON MICROSCOPY (EHREM) IN MATERIALS SCIENCE 123 BY PRATIBHA L. GAI AND EDWARD D. BOYES 1. INTRODUCTION 124 2. EXPERIMENTAL: IN-SITU CONTROLLED ENVIRONMENTAL HIGH RESOLUTION TRANSMISSION EM (EHREM) DEVELOPMENT FOR GAS-SOLID REACTIONS ON THE ATOMIC SCALE 126 3. APPLICATIONS 128 3.1 GAS MOLECULE - SOLID SURFACE INTERACTIONS 128 3.2 SILICA BASED CERAMICS 131 CHEMICALLY STABILIZED CRISTOBALITE CERAMICS 131 3.3 EHREM OF COMPLEX CATALYSTS: 141 4. CONCLUSIONS 146 ACKNOWLEDGEMENTS AND REFERENCES 146 7. IN-SITU TRANSMISSION ELECTRON MICROSCOPY OF THIN FILM GROWTH 149 BY J. MURRAY GIBSON 1. INTRODUCTION 149 2. ROLE OF *** IN STUDIES OF THIN FILM GROWTH 150 3. INSTRUMENTAL APPROACHES 159 4. SOME RESULTS 165 5. CONCLUSIONS 169 ACKNOWLEDGEMENTS AND REFERENCES 169 8. HREM IN-SITU EXPERIMENT AT VERY HIGH TEMPERATURES 173 BY TAKEO KAMINO AND HIROYASU SAKA 1. INTRODUCTION 173 2. SPECIMEN-HEATING HOLDERS 174 VLLL 3. 4. 5. ELECTRON MICROSCOPE 177 HREM OBSERVATION OF SI PARTICLE JUST BELOW THE MELTING POINT 179 FORMATION OF SIC THROUGH SOLID STATE CHEMICAL REACTIONS BETWEEN SI AND GRAPHITE 181 5.1 SPECIMENS 181 5.2 RESULTS AND DISCUSSION 181 SINTERING OF SIC CRYSTALS 186 SURFACE RECONSTRUCTION OF AU-DEPOSITED SI 191 7.1 SPECIMENS 191 7.2 RESULTS AND DISCUSSION 191 ACKNOWLEDGEMENTS AND REFERENCES 199 IN-SITU REM AND *** STUDIES OF HOMO AND HETERO-EPITAXY ON SI SURFACES 201 BY HIROKI MINODA AND KATSUMICHI YAGI 1. INTRODUCTION 2. EXPERIMENTAL 2.1 GENERAL REMARKS ON REM AND *** 2.2 SAMPLE PREPARATION 3. RESULTS AND DISCUSSION 3.1 GROWTHS OF SI ON SI (111) SURFACES 3.2 GROWTHS OF GE ON SI (111) SURFACES 3.3 GROWTHS OFGE ON SI (001) SURFACES 4. CONCLUSIONS REFERENCES 10. ATOMIC-SCALE FABRICATION OF METAL SURFACES BY ADSORPTION AND CHEMICAL REACTION 201 204 204 204 206 206 208 215 223 223 225 BY KEN-ICHI TANAKA, YUJI MATSUMOTO, TAKAYA FUJITA AND YUJI OKAWA 1. INTRODUCTION 2. FABRICATION OF METAL SURFACES BY PHYSICAL PROCESSES 3. FABRICATION OF METAL SURFACES BY CHEMICAL REACTION 4. NANO-METER SCALE PATTERNING BY CHEMICAL REACTIONS REFERENCES 226 228 240 251 259 11. HIGH TEMPERATURE DYNAMIC BEHAVIOR OF SILICON SURFACES STUDIED BY SCANNING TUNNELING MICROSCOPY (STM) 263 BY HIROSHI TOKUMOTO R** IX 1. INTRODUCTION J 263 2. HIGH TEMPERATURE UHV-STM SYSTEM 264 3. HYDROGEN DESORPTION PROCESS ON SI (111) SURFACE 264 4. (7X7) - (LXL) PHASE TRANSITION ON SI (111) SURFACE 271 5. STEP SHIFTING UNDER DC ELECTRIC FIELDS 275 6. CONCLUSIONS 280 ACKNOWLEDGEMENTS AND REFERENCES 281 12. DYNAMIC OBSERVATION OF VORTICES IN SUPERCONDUCTORS USING ELECTRON WAVES 283 BY AKIRA TONOMURA 1. 2. 3. 4. INTRODUCTION EXPERIMENTAL METHOD 2.1 INTERFERENCE MICROSCOPY 2.2 LORENTZ MICROSCOPY OBSERVATION OF SUPERCONDUCTING VORTICES 3.1 SUPERCONDUCTING VORTICES OBSERVED BY INTERFERENCE MICROSCOPY 3.1.1 PROFILE MODE 3.1.2 TRANSMISSION MODE 3.2 SUPERCONDUCTING VORTICES OBSERVED BY LORENTZ MICROSCOPY 3.3 OBSERVATION OF VORTEX INTERACTION WITH PINNING CENTERS 3.3.1 SURFACE STEPS 3.3.2 IRRADIATED POINT DEFECTS CONCLUSION REFERENCES 283 284 284 287 288 288 288 291 293 294 295 296 298 299 13. *** STUDIES OF SOME STRUCTURALLY FLEXIBLE SOLIDS AND THEIR ASSOCIATED PHASE TRANSFORMATIONS 301 BY RAY L. WITHERS AND JOHN G. THOMPSON 1. INTRODUCTION 301 2. TETRAHEDRALLY CORNER-CONNECTED FRAMEWORK STRUCTURES 302 3. TETRAGONAL A-PBO 311 4. COMPOSITIONAL LY FLEXIBLE ANION-DEFICIENT FLUORITES AND THE DEFECT FLUORITE TO C-TYPE SESQUIOXIDE TRANSITION 320 5. SUMMARY AND CONCLUSIONS 327 ACKNOWLEDGEMENTS AND REFERENCES 327 AUTHOR INDEX 331 SUBJECT INDEX 333
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spellingShingle In-situ microscopy in materials research leading international research in electron and scanning probe microscopies
Electron microscopy
Materials Microscopy
Scanning probe microscopy
Werkstoffprüfung (DE-588)4037934-6 gnd
Elektronenmikroskopie (DE-588)4014327-2 gnd
subject_GND (DE-588)4037934-6
(DE-588)4014327-2
title In-situ microscopy in materials research leading international research in electron and scanning probe microscopies
title_auth In-situ microscopy in materials research leading international research in electron and scanning probe microscopies
title_exact_search In-situ microscopy in materials research leading international research in electron and scanning probe microscopies
title_full In-situ microscopy in materials research leading international research in electron and scanning probe microscopies ed. by Pratibha L. Gai
title_fullStr In-situ microscopy in materials research leading international research in electron and scanning probe microscopies ed. by Pratibha L. Gai
title_full_unstemmed In-situ microscopy in materials research leading international research in electron and scanning probe microscopies ed. by Pratibha L. Gai
title_short In-situ microscopy in materials research
title_sort in situ microscopy in materials research leading international research in electron and scanning probe microscopies
title_sub leading international research in electron and scanning probe microscopies
topic Electron microscopy
Materials Microscopy
Scanning probe microscopy
Werkstoffprüfung (DE-588)4037934-6 gnd
Elektronenmikroskopie (DE-588)4014327-2 gnd
topic_facet Electron microscopy
Materials Microscopy
Scanning probe microscopy
Werkstoffprüfung
Elektronenmikroskopie
url http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008133760&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA
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