The analysis of gases by chromatography
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| Hauptverfasser: | , |
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| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Oxford [u.a.]
Pergamon Press
1983
|
| Ausgabe: | 1. ed. |
| Schriftenreihe: | Pergamon series in analytical chemistry
7 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
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| 007 | t| | ||
| 008 | 930421s1983 xx d||| |||| 00||| eng d | ||
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| 100 | 1 | |a Cowper, C. J. |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a The analysis of gases by chromatography |c C. J. Cowper ; A. J. DeRose* |
| 250 | |a 1. ed. | ||
| 264 | 1 | |a Oxford [u.a.] |b Pergamon Press |c 1983 | |
| 300 | |a XII, 147 S. |b graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 1 | |a Pergamon series in analytical chemistry |v 7 | |
| 650 | 4 | |a Chromatographie en phase gazeuse | |
| 650 | 7 | |a Cromatografia Em Camada Delgada |2 larpcal | |
| 650 | 4 | |a Gaz - Analyse | |
| 650 | 4 | |a Gas chromatography | |
| 650 | 4 | |a Gases |x Analysis | |
| 650 | 0 | 7 | |a Gaschromatographie |0 (DE-588)4019330-5 |2 gnd |9 rswk-swf |
| 689 | 0 | 0 | |a Gaschromatographie |0 (DE-588)4019330-5 |D s |
| 689 | 0 | |5 DE-604 | |
| 700 | 1 | |a De Rose, A. J. |e Verfasser |4 aut | |
| 830 | 0 | |a Pergamon series in analytical chemistry |v 7 |w (DE-604)BV001898412 |9 7 | |
| 856 | 4 | 2 | |m HBZ Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=004973316&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-004973316 | |
Datensatz im Suchindex
| _version_ | 1819637323285921792 |
|---|---|
| adam_text | Contents
Chapter 1. INTRODUCTION
1.1 History
1.2 Differences between Gas and Liquid Analysis
1.2.1 Equipment and Materials
1.2.2 Theory
1.2.3 Techniques and Tactics
1.3 Process Gas Analysis
1.4 Ideal and Non—Ideal Behaviour
1.5 Units
1.6 Drawing Conventions
Chapter 2. EQUIPMENT
2.1 Introduction
2.2 Gas Controls
2.2.1 Pressure Regulators
2.2.2 Mass Flow Controllers
2.2.3 Pressure and Flow Measurement
2.2.4 Choice of Method of Control and Measurement
2.3 Sample Introduction
2.4 Columns and Column Ovens
2.5 Detectors
2.5.1 Thermal Conductivity Detector (TCD)
2.5.2 Flame Ionisation Detector (FID)
2.5.3 Electron Capture Detector (ECD)
2.5.4 Flame Photometric Detector (FPD)
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26
THE ANALYSIS OF GASES BY CHROMATOGRAPHY
2.5.5 Ultrasonic Detector
2.5.6 Fhoto-ionisatlon Detector
2.5.7 Helium Detector
2.5.8 Other Detectors
2.6 Auxiliary Devices
2.6.1 Methanator
2.6.2 Hydrogen Transfer System
2.6.3 Palladium Transmodulator
2.7 Recorder/Integrator
Chapter 3 SEPARATION IN THE COLUMN
3.1 Tube Materials and Physical Form
3.2 Adsorbents
3.2.1 Molecular Sieve
3.2.2 Silica
3.2.3 Alumina
3.2.4 Carbon
3.2.5 Dusted Columns
3.3 Porous Polymers
3.3.1 Commercial Polymer Beads
3.3.2 The Century Series
3.3.3 The Porapak Series
3.3.4 Separations by the Different Members of the Two
3.3.5 Porapak Q and Chromosorb 102
3.3.6 Others in the Two Series
3.4 Gas Liquid Columns
Chapter 4 CHOICE OF CARRIER GAS
4.1 Introduction
4.2 Thermal Conductivity Detector
4.3 Flame Ionisation Detector
4.4 Electron Capture Detector
4.5 Other Detectors
4.6 Carrier Gas Purity
4.7 Mixed Carrier Gases
4.7.1 Trace Additives
4.7.2 Addition of Sample Component
Chapter 5 TACTICS FOR THE ANALYSIS OF GAS MIXTURES
5.1 Introduction
5.2 Isothermal Analysis
5.3 The Use of two Columns with two Detectors
5.3.1 Series Operation
5.3.2 Parallel Operation
5.4 Switching Valves
5.4.1 Configuration of Valves
Series
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61
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64
CONTENTS xi
5.4.2 Column Selection 66
5.4.3 Backflushing 67
5.4.4 Column Isolation 69
5.4.5 Foreflushing 70
5.4.6 Multiple Functions 71
5.4.7 Advantages and Disadvantages of Valves 73
5.5 Pressure Balancing 74
5.5.1 Backflush to Vent 74
5.5.2 Heart-cutting 75
5.5.3 Column Selection 76
5.5.4 Peak Storage 77
5.5.5 Adjustment of Separation Characteristics 78
5.5.6 Advantages and Disadvantages of Pressure Balancing 80
5.6 Temperature Programming 80
Chapter 6. EXAMPLES OF APPLICATIONS 82
6.1 Introduction 82
6.2 Air Components and the Rare Gases 82
6.3 Natural Gas and Associated Gas 85
6.4 Refinery Gas and Liquefied Petroleum Gas 90
6.5 Synthesis Gas and Fuel Gas 92
6.6 Flue Gas 93
6.7 Gaseous Sulphur Compounds 94
6.8 Gaseous Nitrogen Compounds 96
6.8.1 The Separation of Nitrogen and its Oxides 96
6.8.2 The Separation of Ammonia and Methylamines 96
6.8.3 The Separation of Cyanogen Compounds 97
6.9 Gaseous Halogen Compounds 97
6.9.1 Organic Halogen Compounds 97
6.9.2 Inorganic Halogen Compounds 99
6.10 Tracers 100
6.11 Isotopes 101
6.12 Miscellaneous Gases 101
Chapter 7. GASES IN LIQUIDS 103
7.1 Introduction 103
7.2 Gases Liquefied by Pressure 103
7.2.1 Vaporisation 104
7.2.2 Liquid Injection 105
7.2.3 Analysis 105
7.3 Gases Liquefied by Temperature 105
7.3.1 Sample handling 105
7.3.2 Analysis 106
7.4 Dissolved Gases 106
7.4.1 Handling of Stabilised Samples 107
7.4.2 Handling of High Pressure Samples 108
THE ANALYSIS OF GASES BY CHROMATOGRAPHY
7.4.3 Analysis - Gas Only
7.4.4 Analysis - Gas and Liquid
7.5 Headspace Analysis
Chapter 8 QUANTIFICATION
8.1 Introduction
8.2 Detector
8.2.1 Thermal Conductivity Detector
8.2.2 Flame Ionisation Detector
8.2.3 Flame Photometric Detector
8.3 Significance of Non-Linear Response
8.4 Peak Area or Peak Height
8.5 Integrators
8.6 Methods of Calculation
8.6.1 External Standard
8.6.2 Measurement by Difference
8.6.3 Normalisation
Chapter 9. THE PREPARATION OF STANDARD MIXTURES
9.1 Introduction
9.2 Direct Standards and Derived Standards
9.3 Errors involved in Standard Preparation
9.4 Categories of Methods
9.4.1 Static Methods
9.4.2 Dynamic Methods
9.5 Description of Methods
9.5.1 Gravimetric Method
9.5.2 Volume Increment Method
9.5.3 Pressure Increment Method
9.5.4 Proportioning Pump Method
9.5.5 Syringe Pump Method
9.5.6 Permeation Method
9.6 Choice of Method
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APPENDIX
A.I
A.2
A.3
A.4
A.5
REFERENCES
AUTHOR INDEX
SUBJECT INDEX
THE SAMPLING OF GASES
Introduction
Representative Nature of Sample
Sample - Transfer
Sample Containers
Sampling into the Chromatograph
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145
|
| any_adam_object | 1 |
| author | Cowper, C. J. De Rose, A. J. |
| author_facet | Cowper, C. J. De Rose, A. J. |
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| discipline | Chemie / Pharmazie |
| edition | 1. ed. |
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| id | DE-604.BV007606270 |
| illustrated | Illustrated |
| indexdate | 2024-12-23T12:31:15Z |
| institution | BVB |
| isbn | 0080240275 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-004973316 |
| oclc_num | 9412520 |
| open_access_boolean | |
| owner | DE-355 DE-BY-UBR DE-11 DE-188 |
| owner_facet | DE-355 DE-BY-UBR DE-11 DE-188 |
| physical | XII, 147 S. graph. Darst. |
| publishDate | 1983 |
| publishDateSearch | 1983 |
| publishDateSort | 1983 |
| publisher | Pergamon Press |
| record_format | marc |
| series | Pergamon series in analytical chemistry |
| series2 | Pergamon series in analytical chemistry |
| spellingShingle | Cowper, C. J. De Rose, A. J. The analysis of gases by chromatography Pergamon series in analytical chemistry Chromatographie en phase gazeuse Cromatografia Em Camada Delgada larpcal Gaz - Analyse Gas chromatography Gases Analysis Gaschromatographie (DE-588)4019330-5 gnd |
| subject_GND | (DE-588)4019330-5 |
| title | The analysis of gases by chromatography |
| title_auth | The analysis of gases by chromatography |
| title_exact_search | The analysis of gases by chromatography |
| title_full | The analysis of gases by chromatography C. J. Cowper ; A. J. DeRose* |
| title_fullStr | The analysis of gases by chromatography C. J. Cowper ; A. J. DeRose* |
| title_full_unstemmed | The analysis of gases by chromatography C. J. Cowper ; A. J. DeRose* |
| title_short | The analysis of gases by chromatography |
| title_sort | the analysis of gases by chromatography |
| topic | Chromatographie en phase gazeuse Cromatografia Em Camada Delgada larpcal Gaz - Analyse Gas chromatography Gases Analysis Gaschromatographie (DE-588)4019330-5 gnd |
| topic_facet | Chromatographie en phase gazeuse Cromatografia Em Camada Delgada Gaz - Analyse Gas chromatography Gases Analysis Gaschromatographie |
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