Analysis of substances in the gaseous phase
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| Hauptverfasser: | , |
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| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Amsterdam [u.a.]
Elsevier
1991
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| Schriftenreihe: | Wilson and Wilson's comprehensive analytical chemistry
28 |
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| Online-Zugang: | Inhaltsverzeichnis |
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| 245 | 1 | 0 | |a Analysis of substances in the gaseous phase |c by E. Smolková-Keulemansová and L. Feltl |
| 264 | 1 | |a Amsterdam [u.a.] |b Elsevier |c 1991 | |
| 300 | |a XII, 479 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 1 | |a Wilson and Wilson's comprehensive analytical chemistry |v 28 | |
| 500 | |a Literaturverz. S. 462 - 473 | ||
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| 650 | 4 | |a Chromatographie en phase gazeuse | |
| 650 | 7 | |a Chromatographie en phase gazeuse |2 ram | |
| 650 | 4 | |a Gaz - Analyse | |
| 650 | 7 | |a Gaz - Analyse |2 ram | |
| 650 | 4 | |a Gas chromatography | |
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Datensatz im Suchindex
| _version_ | 1804118785275199488 |
|---|---|
| adam_text | Wilson and Wilson s
COMPREHENSIVE ANALYTICAL CHEMISTRY
Edited by
G SVEHLA, Ph D,D Sc ,FRSC,F LC I
Professor of Analytical Chemistry
University College, Cork, Ireland
VOLUME XXVIII
ANALYSIS OF SUBSTANCES
IN THE
GASEOUS PHASE
by
E SMOLKOVA-KEULEMANSOVA and L FELTL
ELSEVIER
AMSTERDAM-OXFORD-NEW YORK-TOKYO
Contents
Editor s Preface XIII
Chapter 1 INTRODUCTION 1
Chapter 2 THE HISTORY OF THE CHEMISTRY OF GASES 3
Chapter 3 CHARACTERISTICS OF GAS ANALYSIS 7
3 1 Basic gas laws 7
3 2 Working conditions 11
Chapter 4 DETERMINATION OF THE TEMPERATURE,
PRESSURE AND VOLUME 15
4 1 Temperature measurement 15
4 2 Pressure measurement 17
4 3 Volume measurement 27
Chapter 5 SAMPLE STORAGE AND TREATMENT 35
5 1 Basic equipment 36
511 Basic sampler requirements 37
5 2 Practical sampling problems 44
Chapter 6 QUALITATIVE AND SEMI-QUANTITATIVE
METHODS OF GAS ANALYSIS 47
Chapter 7 METHODS OF QUANTITATIVE ANALYSIS 55
Chapter 8 CHEMICAL AND PHYSICO-CHEMICAL METH
ODS OF GAS ANALYSIS 57
8 1 Absorption volumetric analysis 57
811 Confining fluids 57
812 Absorption reagents 58
ix
813 Instrumentation 64
814 Apparatus for the analysis of gas mixtures 68
815 The procedure in the analysis of individual compo
nents 73
816 Factors affecting the precision of the determination 74
817 Volumetric analyzers 77
8 2 Manometric analysis 79
8 3 Absorption separation and gravimetric or titration deter
mination 81
8 4 Separation by absorption and determination by optical
methods 84
841 Optical gas analyzers 88
8 5 Separation by absorption and determination by electro
chemical methods 90
851 Conductometry 91
852 Voltammetric methods 94
853 Potentiometry 102
854 Coulometry 108
8 6 Separation by absorption and determination by thermo-
chemical methods Ill
8 7 Combustion methods 113
871 Total combustion methods 113
872 Fractional combustion methods 117
873 Methods based on measuring the heat of combustion 119
8 8 Evaluation of chemical methods of gas analysis 121
Chapters PHYSICAL METHODS OF GAS ANALYSIS 123
9 1 Thermal conductivity 123
911 Basic relationships 124
912 Working conditions 127
913 Sensor design 132
914 Utilization of measurement of the theimal conduc
tivity 134
9 2 Interferometry 136
921 Basic relationships 137
922 Instrumentation 140
923 Determination methods 143
924 The use of interferometry 145
9 3 Absorption and emission spectrometry 147
931 Basic relationships 147
932 The absorption spectrometry of gases and vapours 149
x
933 Emission spectral analysis 161
934 Optoacoustical methods 168
9 4 Mass spectrometry 170
941 Principle of the method 170
942 Instruments, their basic components and function 171
943 Applications 179
9 5 The magnetic properties of gases 181
951 Basic concepts and relationships 182
952 Measuring methods 184
9 6 Determinations based on density measurements 188
9 7 Determinations based on viscosity measurements 193
9 8 Diffusion process analysis 196
981 Effusion 196
982 Transfusion 198
983 Thermal diffusion 199
9 9 The utilization of adsorption in gas anal ysis 200
991 Basic relationships 202
992 Adsorbents 204
993 Adsorption methods in gas analysis 209
994 The use of adsorbents in trace analysis 210
9 10 Radiometric methods 212
9 11 Preparation of mixtures of gases and vapours 215
9 11 1 Static methods 216
9 11 2 Dynamic methods 218
Chapter 10 GAS CHROMATOGRAPHY 223
10 1 The development of chromatographic methods 223
10 1 1 The importance of gas chromatoijraphy 225
10 2 Basic chromatography data 227
10 2 1 Apparatus and procedure 227
10 2 2 Definition and classification of gas chromatogra
phy 228
10 2 3 Nomenclature and symbols em) loved in gas chro
matography 238
10 3 The physico-chemical basis of gas chromatography 242
10 3 1 Adsorption 242
10 311 Basic concepts 242
10 312 Adsorption isotherms 243
10 313 The utilization of adsorption phenomena
in gas chromatography 258
XI
10 3 2 Dissolution 259
10 3 3 Adsorption at the gas-liquid interface 268
10 3 4 Transport phenomena in the chromatographic col
umn 270
10 4 The theory of gas chromatography 282
10 4 1 The plate theory 283
10 4 2 The rate theory 287
10 4 3 Practical consequences of the theory 295
10 4 4 Expression of the column efficiency 300
10 4 5 Optimal conditions for gas chromatographic analy
sis 307
10 5- Instrumentation 308
10 5 1 Source, regulation and measuring of carrier gas
flow-rates 309
10 5 2 Sample introduction 311
10 5 3 Types of columns 315
10 5 4 Liquid stationary phases 323
10 5 5 The chromatographic support 337
10 5 6 Adsorbents 345
10 5 7 Programmed gas chromatography 355
10 5 8 Detectors 359
10 5 9 Recording and evaluation 387
10 6 Qualitative analysis 397
10 6 1 Identification on the basis of ret ention data 397
10 6 2 Identification employing ancillary methods 404
10 6 3 Identification using selective det ectors 416
10 6 4 The combination of gas chromatography with mass
spectrometry 419
10 7 Quantitative analysis 430
10 7 1 Sources of error 431
10 7 2 Methods of quantitative chromatogram evalua
tion 436
10 7 3 Working technique in quantitative analysis 441
10 8 Application of gas chromatography 448
10 8 1 Gases 449
10 8 2 Volatile substances 450
10 8 3 Substances with low volatility and solids 451
10 8 4 Separation of chiral substances 454
10 8 5 Trace analysis 455
Bibliography 462
Subject Index 475
xii
|
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| dewey-ones | 543 - Analytical chemistry |
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| discipline | Chemie / Pharmazie |
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| id | DE-604.BV004666547 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T16:15:49Z |
| institution | BVB |
| isbn | 0444891226 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-002866831 |
| oclc_num | 24285483 |
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| physical | XII, 479 S. Ill., graph. Darst. |
| publishDate | 1991 |
| publishDateSearch | 1991 |
| publishDateSort | 1991 |
| publisher | Elsevier |
| record_format | marc |
| series | Wilson and Wilson's comprehensive analytical chemistry |
| series2 | Wilson and Wilson's comprehensive analytical chemistry |
| spelling | Smolková-Keulemansová, E. Verfasser aut Analysis of substances in the gaseous phase by E. Smolková-Keulemansová and L. Feltl Amsterdam [u.a.] Elsevier 1991 XII, 479 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Wilson and Wilson's comprehensive analytical chemistry 28 Literaturverz. S. 462 - 473 Chimie analytique ram Chromatographie en phase gazeuse Chromatographie en phase gazeuse ram Gaz - Analyse Gaz - Analyse ram Gas chromatography Gases Analysis Gasanalyse (DE-588)4155993-9 gnd rswk-swf Gaschromatographie (DE-588)4019330-5 gnd rswk-swf Gasanalyse (DE-588)4155993-9 s DE-604 Gaschromatographie (DE-588)4019330-5 s Feltl, Ladislav Verfasser aut Wilson and Wilson's comprehensive analytical chemistry 28 (DE-604)BV000900805 28 HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=002866831&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Smolková-Keulemansová, E. Feltl, Ladislav Analysis of substances in the gaseous phase Wilson and Wilson's comprehensive analytical chemistry Chimie analytique ram Chromatographie en phase gazeuse Chromatographie en phase gazeuse ram Gaz - Analyse Gaz - Analyse ram Gas chromatography Gases Analysis Gasanalyse (DE-588)4155993-9 gnd Gaschromatographie (DE-588)4019330-5 gnd |
| subject_GND | (DE-588)4155993-9 (DE-588)4019330-5 |
| title | Analysis of substances in the gaseous phase |
| title_auth | Analysis of substances in the gaseous phase |
| title_exact_search | Analysis of substances in the gaseous phase |
| title_full | Analysis of substances in the gaseous phase by E. Smolková-Keulemansová and L. Feltl |
| title_fullStr | Analysis of substances in the gaseous phase by E. Smolková-Keulemansová and L. Feltl |
| title_full_unstemmed | Analysis of substances in the gaseous phase by E. Smolková-Keulemansová and L. Feltl |
| title_short | Analysis of substances in the gaseous phase |
| title_sort | analysis of substances in the gaseous phase |
| topic | Chimie analytique ram Chromatographie en phase gazeuse Chromatographie en phase gazeuse ram Gaz - Analyse Gaz - Analyse ram Gas chromatography Gases Analysis Gasanalyse (DE-588)4155993-9 gnd Gaschromatographie (DE-588)4019330-5 gnd |
| topic_facet | Chimie analytique Chromatographie en phase gazeuse Gaz - Analyse Gas chromatography Gases Analysis Gasanalyse Gaschromatographie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=002866831&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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