Infrared spectrometry of industrial polymers
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| Format: | Buch |
| Sprache: | English |
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London
Acad. Press
1967
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| 245 | 1 | 0 | |a Infrared spectrometry of industrial polymers |c John C. Henniker |
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Datensatz im Suchindex
| DE-BY-TUM_call_number | 0701 0013 A 989 |
|---|---|
| DE-BY-TUM_katkey | 377621 |
| DE-BY-TUM_location | Mag |
| DE-BY-TUM_media_number | 040020690388 |
| _version_ | 1820891755383357440 |
| adam_text | Infrared Spectrometry
of Industrial Polymers
John C HENNIKER
Chef du Service Chimie Physique
Centre d Etude des Matieres Plastiques
Paris, France
ACADEMIC PRESS I M
LONDON AND NEW YORK • 1967
CONTENTS
PREFACE v
CHAPTER 1 PRINCIPLES OF MOLECULAR SPECTROMETRY 1
V11 Introduct ion 1
1 2 Absorpt ion of Radiat ion by Molecules 1
1 3 Orig in o f Energy Levels 5
1 4 Spectra l Frequencies and Molecular Structure 10
1 5 Intens i t ies o f Spectra l Peaks 12
References15
CHAPTER 2 SPECTROMETERS 16
2 1 Princ ip les 16
2 2 Dispers ing Device 19
2 3 Infrared Sources 22
2 4 Detectors 23
2 5 Sl its and Resolut ion 24
2 6 Modulator 25
2 7 Attenuator 26
2 8 Electronics 27
2 9 Recording System 27
2 10 Atmosphere • 29
2 11 Commercia l Models 29
2 12 Operat ing Condit ions 30
2 13 Cal ibrat ion 33
2 14 Sample Cel l s 35
References37
CHAPTER 3 PRELIMINARY SEPARATIONS 38
3 1 Extract ion 38
3 2 Dif ferent ia l So lut ion 41
3 3 Dif ferent ia l Prec ip i tat ion 42
3 4 Subl imat ion in Vacuum 42
3 5 Drying 44
3 3 Steam Dist i l la t ion 44
3 7 Preparat ive Gas Chromatography 45
3 8 Pyrolys i s 47
3 9 Chemical React ion 50
References 51
CHAPTER 4 SAMPLE PREPARATION 52
4 1 Thickness 52
4 2 Opt ica l Requirements 54
4 3 Sample Preparat ion Techniques 58
4 4 Press ing in a Heated Mould 58
4 5 The Microtome Technique 61
4 6 Cold Sinter ing 64
4 7 Suspens ions o f Powder 69
via CONTENTS
CHAPTER 4 SAMPLE PREPARATION—contd
4 8 Fi lms on Ref lect ing Surfaces
4 9 Fi lms by Cast ing from Solut ion
4 10 Fi lms of Varying Thickness
4 11 Spectrometry o f Solut ions
4 12 Oriented Samples
4 13 Surfaces for Ref lex ion Spectrometry
4 14 Samples for Di lTus ion Spectrometry
References
CHAPTER 5 SPECIAL SPECTROMETRY TECHNIQUES
5 1 Specular Ref lex ion
5 2 Dif fuse Ref lex ion
5 3 Attenuated Tota l Ref lex ion
5 4 Dif ferent ia l Spectrometry (Solut ions)
5 5 Dif ferent ia l Spectrometry (Sol ids)
5 6 Scale Expans ion
5 7 Beam Condensers
5 8 Polar izat ion Spectrometry
5 9 Refract ive Index
5 10 Dif fus ion Spectra
5 11 Near Infrared Spectrometry
5 12 Far Infrared Spectrometry
5 13 Emiss ion Spectra
5 14 Derivat ive Spectrograms
5 15 Ultravio le t Frozen Matr ix Spectra
References
CHAPTER 6 THE INFRARED IDENTIFICATION OF POLYMERS
6 1 Sui table Spectra
6 2 The Comparison and the Funct ional Approaches
6 3 Extens ions o f the Comparison Approach
6 4 Spectra o f Copolymers and Mixed Polymers
6 5 Ident i f icat ion o f Components
6 6 Examples
6 7 References to Spectra
References
CHAPTER 7 QUANTITATIVE ANALYSIS
7 1 The Beer-Lambert Law
7 2 The Internal Standard
7 3 The Base Line
7 4 Multicomponent Systems
7 5 Appl icat ions
References
CONTENTS ix
CHAPTER 8 POLYMER STRUCTURE 160
8 1 Studies o f React ions 160
8 2 Isotope Subst i tut ion 164
8 3Dichroism 167
8 4 The Hydrogen Bond 173
8 5 Stereoisomerism and Crysta l ! in i ty 181
8 6 Model Compounds 189
8 7 Symmetry 193
8 8 Normal Coordinate Calculat ions 194
References201-
CHAPTER 9 APPENDIX—SPECULAR REFLEXION SPECTRA 205
AUTHOR INDEX 217
SUBJECT INDEX 225
|
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| id | DE-604.BV002280202 |
| illustrated | Not Illustrated |
| indexdate | 2024-12-23T10:33:42Z |
| institution | BVB |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-001498349 |
| oclc_num | 234618 |
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| owner | DE-91G DE-BY-TUM DE-29T DE-83 DE-188 |
| owner_facet | DE-91G DE-BY-TUM DE-29T DE-83 DE-188 |
| physical | IX, 229 S. |
| psigel | TUB-nveb |
| publishDate | 1967 |
| publishDateSearch | 1967 |
| publishDateSort | 1967 |
| publisher | Acad. Press |
| record_format | marc |
| spellingShingle | Henniker, John C. Infrared spectrometry of industrial polymers Infrared spectroscopy Polymers Spectra Polymere (DE-588)4046699-1 gnd Infrarotspektroskopie (DE-588)4135411-4 gnd |
| subject_GND | (DE-588)4046699-1 (DE-588)4135411-4 |
| title | Infrared spectrometry of industrial polymers |
| title_auth | Infrared spectrometry of industrial polymers |
| title_exact_search | Infrared spectrometry of industrial polymers |
| title_full | Infrared spectrometry of industrial polymers John C. Henniker |
| title_fullStr | Infrared spectrometry of industrial polymers John C. Henniker |
| title_full_unstemmed | Infrared spectrometry of industrial polymers John C. Henniker |
| title_short | Infrared spectrometry of industrial polymers |
| title_sort | infrared spectrometry of industrial polymers |
| topic | Infrared spectroscopy Polymers Spectra Polymere (DE-588)4046699-1 gnd Infrarotspektroskopie (DE-588)4135411-4 gnd |
| topic_facet | Infrared spectroscopy Polymers Spectra Polymere Infrarotspektroskopie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001498349&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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