Advanced chemical methods for soil and clay minerals research Proceedings of the NATO Advanced Study Inst. held at the Univ. of Illinois, July 23-August 4, 1979
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| Format: | Buch |
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| Sprache: | English |
| Veröffentlicht: |
Dordrecht
Reidel
1980
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| Schriftenreihe: | Nato: Nato advanced study institutes series. C
63 |
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| Online-Zugang: | Inhaltsverzeichnis |
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| 245 | 1 | 0 | |a Advanced chemical methods for soil and clay minerals research |b Proceedings of the NATO Advanced Study Inst. held at the Univ. of Illinois, July 23-August 4, 1979 |c ed. by J. W. Stucki ... |
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Datensatz im Suchindex
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| adam_text | TABLE OF CONTENTS
PREFACE ..................................................... vii
1. MÖSSBAUER SPECTROSCOPY-Bernard A. Goodman ......... 1
1-1. Introduction to the Mössbauer Effect ................. 1
1-2. Basic Principles of Mössbauer Spectroscopy . ............. 7
1-3. Instrumentation and Experimental Procedures.............19
1-4. Application of Mössbauer Spectroscopy to the
Study of Silicate Minerals .......................28
1-5. The Study of Mineral Alteration Reactions ..............45
1-6. Iron Oxides and their Characterization in Soils ............65
1-7. Critical Assessment of the Potential of Mössbauer
Spectroscopy, and its Application to Nuclei
Other than Iron ............................80
References..................................90
2. NEUTRON SCATTERING METHODS OF INVESTIGATING
CLAY SYSTEMS- D.K. Ross and P.L Hall.................93
2-1. Introduction..............................93
2-2. Elementary Neutron Scattering Theory ................99
2-3. Neutron Scattering Instrumentation and Methods..........130
2-4. Applications of Neutron Spectroscopy to Studies
of Clay Minerals ...........................138
Appendix 2-1. Macroscopic Cross Section for a
Montmorillonite-Water System.....................160
Appendix 2-2. Calculation of Incoherent Scattering Intensity
Ratios for a Clay-Water System.....................162
References.................................163
3. INTRODUCTION TO X-RAY PHOTOELECTRON
SPECTROSCOPY- C. Defosse and P.G. Rouxhet............. 169
3-1. Introduction............................. 169
3-2. Trend of XPS Spectra ........................ 171
3-3. Instrumentation ........................... 175
3-4. Peak Position............................. 177
3-5. Explored Depth ........................... 182
3-6. Peak Intensity ............................ 185
3-7. Overview of Methods of Characterization of Solids
Based on X-ray, Electron and Ion Beams...............193
References.................................201
yi TABLE OF CONTENTS
4. APPLICATION OF X-RAY PHOTOELECTRON SPECTROSCOPY TO THE
STUDY OF MINERAL SURFACE CHEMISTRY - M.H. Koppelman .. 205
4-1. Uniqueness of XPS for the Investigation of Mineral
Surface Phenomena - Probing Depth ................ 205
4-2. Sample Handling Techniques..................... 206
4-3. Analytical Applications ....................... 211
4-4. Electron Take-Off (Grazing) Angle Analysis Applications...... 216
4-5. Qualitative Bonding Investigations.................. 220
4-6. Summary............................... 241
References................................. 242
5. THE APPLICATION OF NMR TO THE STUDY OF
CLAY MINERALS -J.J. Fripiat..................... 245
5-1. Introduction: Fundamentals of NMR ................ 245
5-2. The Bloch Equations......................... 254
5-3. Line Shape.............................. 262
5-4. Relaxation Mechanisms ....................... 282
5-5. Review of Some Problems: Order and Disorder
in Adsorbed Water Molecules .................... 303
References................................. 314
6. DISTRIBUTION OF IONS IN THE OCTAHEDRAL SHEET OF
MICAS -W.E.E. Stone and J. Sanz.................... 317
6-1. Introduction............................. 317
6-2. Influence of the Fe2+ Ions...................... 318
6-3. H+ Spectra of Phiogopites...................... 319
6-4. H+ Spectra of Biotites........................ 321
6-5. F~ Spectra.............................. 322
6-6. Correlation with I.R. Results..................... 324
References................................. 328
7. GENERAL THEORY AND EXPERIMENTAL ASPECTS OF
ELECTRON SPIN RESONANCE-Jacques C. Védrine ......... 331
7-1. Introduction............................. 331
7-2. G-Factor Tensor........................... 340
7-3. Hyperfine Interaction ........................ 353
7-4. Analysis of ESR Spectra....................... 362
7-5. Fine Structure....................... 368
7-6. Summary.................... 373
Appendix 7-1 .................... ........ 375
Appendix 7-2............................... 377
Appendix 7-3............................... 381
References........................ 386
TABLE OF CONTENTS vii
8. APPLICATIONS OF ESR SPECTROSCOPY TO INORGANIC-CLAY
SYSTEMS-Thomas J. Pinnavaia..................... 391
8-1. Introduction...........v.................. 391
8-2. Surface-Bound Metal Ions ...................... 391
8-3. Framework Paramagnetic Centers.................. 407
References................................. 419
9. APPLICATION OF SPIN PROBES TO ESR STUDIES OF
ORGANIC-CLAY SYSTEMS-Murray B.McBride............ 423
9-1. Nitroxide Spin Probes — Origin of
the ESR Spectrum.......................... 423
9-2. Nitroxides in Low-Viscosity Media -
Rapid Isotropie Motion ....................... 427
9-3. Nitroxides in High-Viscosity Media ................. 429
9-4. Nitroxides Adsorbed on Clay Surfaces................ 437
9-5. Experimental Considerations in Using
Nitroxide Spin Probes ........................ 447
References................................. 449
10. APPLICATIONS OF PHOTOACOUSTIC SPECTROSCOPY TO THE STUDY
OF SOILS AND CLAY MINERALS- Raymond L.Schmidt...... 451
10-1. Introduction............................ 451
10-2. Instrumentation.......................... 454
10-3. Results .............................. 456
10-4. Conclusions............................ 463
References................................ 465
INDEX.................................... 467
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| indexdate | 2024-12-23T10:33:10Z |
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| isbn | 9027711585 |
| language | English |
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| series | Nato: Nato advanced study institutes series. C |
| series2 | Nato: Nato advanced study institutes series. C |
| spellingShingle | Advanced chemical methods for soil and clay minerals research Proceedings of the NATO Advanced Study Inst. held at the Univ. of Illinois, July 23-August 4, 1979 Nato: Nato advanced study institutes series. C Methode (DE-588)4038971-6 gnd Bodenchemie (DE-588)4146134-4 gnd |
| subject_GND | (DE-588)4038971-6 (DE-588)4146134-4 (DE-588)1071861417 |
| title | Advanced chemical methods for soil and clay minerals research Proceedings of the NATO Advanced Study Inst. held at the Univ. of Illinois, July 23-August 4, 1979 |
| title_auth | Advanced chemical methods for soil and clay minerals research Proceedings of the NATO Advanced Study Inst. held at the Univ. of Illinois, July 23-August 4, 1979 |
| title_exact_search | Advanced chemical methods for soil and clay minerals research Proceedings of the NATO Advanced Study Inst. held at the Univ. of Illinois, July 23-August 4, 1979 |
| title_full | Advanced chemical methods for soil and clay minerals research Proceedings of the NATO Advanced Study Inst. held at the Univ. of Illinois, July 23-August 4, 1979 ed. by J. W. Stucki ... |
| title_fullStr | Advanced chemical methods for soil and clay minerals research Proceedings of the NATO Advanced Study Inst. held at the Univ. of Illinois, July 23-August 4, 1979 ed. by J. W. Stucki ... |
| title_full_unstemmed | Advanced chemical methods for soil and clay minerals research Proceedings of the NATO Advanced Study Inst. held at the Univ. of Illinois, July 23-August 4, 1979 ed. by J. W. Stucki ... |
| title_short | Advanced chemical methods for soil and clay minerals research |
| title_sort | advanced chemical methods for soil and clay minerals research proceedings of the nato advanced study inst held at the univ of illinois july 23 august 4 1979 |
| title_sub | Proceedings of the NATO Advanced Study Inst. held at the Univ. of Illinois, July 23-August 4, 1979 |
| topic | Methode (DE-588)4038971-6 gnd Bodenchemie (DE-588)4146134-4 gnd |
| topic_facet | Methode Bodenchemie Konferenzschrift |
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