Selected topics in x-ray crystallography from the Delft X-Ray Institutes

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Veröffentlicht: Amsterdam North-Holland 1951
Schriftenreihe:Monographs on theoretical and applied physics 3
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Datensatz im Suchindex

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adam_text ^ELECTED TOPICS IN X-RAY CRYSTALLOGRAPHY FROM THE DELFT X-RAY INSTITUTES EDITED BY J. BOUMAN TECHNICAL UNIVERSITY OF DELFT ** IN 1951 NORTH-HOLLAND P U B L I S H I N G ~ UE UE M ~ P X N Y AMSTERDAM INTERSCIENCE PUBLISHERS INC., NEW YORK / CONTENTS PREFACE VII PAKT A. GENERAL METHODS, STRUCTURE ANALYSIS PAGE CH. I. J. BOTJMAN, GENERAL INTRODUCTION, THE RECIPROCAL LATTICE 3 § 1. INTRODUCTION, THE RECIPROCAL SPACE 3 § 2. THE FOURIER-SPACE 8 § 3. THE INTENSITY-SPACE_ 12 § 4. THE FUNCTION OF PATTERSON 16 § 5. THE PROPERTIES OF THE FUNCTION OF PATTERSON . . . . 17 CH. II. W. F. DE JONG, THE RETIGRAPH . 19 § 1. INTRODUCTION 19 § 2. THEORY OF THE INSTRUMENT 19 § 3. DETERMINATION OF THE ABSOLUTE AXIAL LENGTH * . . . . 23 § 4. PHOTOGRAPHING THE 1TH (7*-NETPLANE 24 § 6. SETTING UP THE WHOLE RECIPROCAL LATTICE 26 § 6. INTENSITY OF THE SPOTS 27 | 7. DESCRIPTION OF THE APPARATUS 29 CH. III. L. L. VAN REUEN, TERMINATION EFFECTS IN X-RAY FOURIER- SYNTHESES 32 § 1. INTRODUCTION 32 § 2. ERRORS IN FOURIER-SYNTHESES 33 § 3. ACCURACY OF THE RESULTS OF FOURIER-SYNTHESES . . . . 35 § 4. TERMINATION EFFECTS FOR ONE-DIMENSIONAL SYNTHESES . . 36 § 6. CONVERGING FACTOR, FOR ONE-DIMENSIONAL SYNTHESES . . 41 § 6. ELIMINATION OF TERMINATION EFFECTS 42 § 7. EXTENSIONS, TWO- AND THREE DIMENSIONAL SYNTHESES . . 49 § 8. TERMINATION EFFECTS FOR DIAMOND 51 CH. IV. J. BOTJMAN, THE BREADTH OF DEBYE-SCHERRER UNES CAUSED BY THE DIMENSIONS OF THE CRYSTAL PARTICLES 59 § 1. INTRODUCTION 59 § 2. THE EVALUATION OF THE TOTAL INTENSITY . . . . . . . 62 § 3. THE PROFILE AND BREADTH OF THE LINE 63 § 4. THE PROPERTIES OF A X AND * 3 64 § 5. NUMERICAL VALUES 66 § 6. CONCLUSIONS 70 CH. V. W. MAY, CALCULATION OF THE STEREOGRAPHIC POLE FIGURE OF * THE CUBIC LATTICE FOR ANY GIVEN DIRECTION (HKL). . . . 72 § 1. INTRODUCTION 72 § 2. GENERAL COURSE OF THE CALCULATION 73 § 3. CONCLUDING REMARKS 74 XII CONTENTS PART *. DISTORTIONS IN CRYSTALS PAGE CH. I. J. BOUMAN, THEORETICAL CONSIDERATIONS . . 80 § 1. INTRODUCTION 80 § 2. THE DIFFRACTION BY AN UNDISTORTED CRYSTAL . . . . . 82 § 3. THE INTENSITY AND BREADTH FOR A DISTORTED CRYSTAL . . 84 § 4. THE CALCULATION OF THE DIFFRACTED INTENSITY 87 § 5. THE ENERGY AND BREADTH OF THE DEBYE-SCHERRER LINE . 90 § 6. THE THEORY OF SMALL DISTORTIONS 93 § 7. RESTATEMENT OF THE THEORY, CENTRES OF DISTORTION . . 95 § 8. FROZEN HEAT MOTION 97 § 9. THE THEORIES OF DEHLINGER AND BOAS 98 § 10. SURVEY OF THE SEVERAL MODELS 102 CH. II. J. BOUMAN, A SIMPLIFIED THEORY OF THE DIFFUSE SPOTS . 106 § 1. THE GENERAL FORMULA 106 § 2. THE VIBRATIONS IN THE CRYSTAL 107 § 3. THE INTENSITY OF THE DIFFRACTED X-RAYS . . . . . . . 109 § 4. THE DIFFUSE SPOTS 110, § 5. THE ELASTIC THEORY OF DIFFUSE SPOTS ILL CH. III. J. J. ARLMAN AND J. BOUMAN, THE DIFFUSE PATTERN OF TIN SINGLE CRYSTALS 113 § 1. INTRODUCTION 113 § 2. DISCUSSION OF EXPERIMENTS 113 § 3. INTERPRETATION OF THE RESULTS 117 § 4. THE THERMAL THEORY OF DIFFUSE SPOTS 124 § 5. ELASTIC VIBRATIONS IN THE TIN CRYSTAL . . . . . . . . . 126 § 6. THE EXPLANATION OF THE DIFFUSE SPOTS . . . . . . . . 129 § 7. NUMERICAL CALCULATION AND RESULTS 131 CH. IV. W. G. BURGERS AND TAN KOEN HIOK, LATTICE DEFECTS IN SILVERCHLORIDE CRYSTALS . 136 § 1. INTRODUCTION 136 § 2. PREPARATION OF CRYSTALS 136 § 3. OPTICAL ETCHING WITH ULTRA VIOLET LIGHT 137 § 4. DIFFUSE BANDS ON LAUE-PHOTOGRAPHS . . . . . . . . 139 § 5. DISCUSSION OF THE LAUE-PHOTOGRAPHS 139 CH. V. W. G. BURGERS AND F. J. LEBBINK, LATTICE DISTORTIONS IN SHEARED ALUMINIUM SINGLE CRYSTALS 146 § 1. INTRODUCTION 146 § 2. MECHANISM OF GLIDING IN CRYSTALS 146 § 3. LATTICE DISTORTIONS ALONG SLIP PLANES 147 § 4. LOCAL CHARACTER OF THE LATTICE ROTATION . . . . . . . 147 § 6. INFLUENCE OF THE METHOD OF DEFORMATION 160 § 6. SHEARING EXPERIMENTS WITH ALUMINIUM SINGLE CRYSTALS 151 § 7. COMPARISON OF ALUMINIUM AND NAPHTHALENE . . . . . 156 § 8. CRYSTALS SHEARED IN ABNORMAL DIRECTIONS . . . . . 157 / CONTENTS XIII PART *. STIMULATED CRYSTALS, TWINNING AND RATE OF NUCLEATION DURING RECRYSTALLIZATION OF ALUMINIUM J. SANDEE, W. MAY AND W. G. BURGERS PAGE § 1. STIMULATION OF CRYSTAL GROWTH 161 § 2. TWIN RELATIONSHIP 163 § 3. PHYSICAL ASPECT OF STIMULATION 164 § 4. RATE OF NUCLEATION DURING RECRYSTALLIZATION 168 PART D. X-RAY INVESTIGATIONS OF PHOTOGRAPHIC EMULSIONS AND OF SILVERHALIDE CRYSTALS W. G. BURGERS, J. N. KOOY AND E. A. MESRITZ CH. I. ON THE ALLEGED LATTICE DILATION OF SUEVERBROMIDE DURING EXPOSURE 174 § 1. PURPOSE OF INVESTIGATION 174 § 2. EXPERIMENTAL PROCEDURE. 176 § 3. MAGNITUDE OF THE EXPECTED EFFECT 177 § 4. RESULTS OF MEASUREMENTS 177 CH. IL ROENTGENOGRAPHIC OBSERVATION OF THE RIPENING OF SILVER- BROMIDE EMULSIONS 180 § 1. RIPENING OF PHOTOGRAPHIC EMULSIONS 180 § 2. CRYSTAL SIZE IN RIPENED EMULSIONS 180 § 3. DEBYE-SCHERRER-PHOTOGRAPHS 181 CH. III. INFLUENCE OF CADMIUM- AND LEAD HALIDES ON THE PHOTO- SENSIVITY OF SILVER HALIDES 184 § 1. GURNEY AND MOTT S THEORY OF LATENT IMAGE FORMATION 184 § 2. PHOTO-SENSIVITY OF SILVER HALIDES AND ELECTRIC CONDUCTIVITY 184 § 3. MIXED CRYSTALS OF AGCL + CD CL 2 AND AGBR + PBBR 2 186 § 4. COLOURING BY ULTRAVIOLET LIGHT 187 PART E. THE AMORPHOUS STATE OF SOME ELEMENTS (HG, SB, SE, S) J. A. PRINS § 1. AMORPHOUS CATEGORIES 191 § 2. LIQUIDS 192 § 3. SUPERCOOLING 193 § 4. VITRIFICATION 193 § 6. ORIENTATION WITHOUT CRYSTALLIZATION 196 § 6. ORIENTED CRYSTALLIZATION 197 § 7. MERCURY 197 § 8. ANTIMONY 198 § 9. SELENIUM 201 § 10. CAMERAS AND HEATING DEVICES 204 §11. SULPHUR 206 XIV CONTENTS PART F. ON QUANTITATIVE DETERMINATIONS P. M. DE WOLFF PAGE CH. I. PRINCIPLES 214 § 1. THEORY OF POWDER DIFFRACTION 214 § 2. METHOD OF DIRECT COMPARISON 217 § 3. USE OF THE DIRECT BEAM AS A REFERENCE . 217 § 4. INTERNAL STANDARD 219 § 5. CONCLUSIONS 222 CH. II. ERRORS CAUSED BY ABSORBING PARTICLES 224 § 1. INTRODUCTION 224 § 2. RESTRICTION TO CASES IN WHICH NO EXTINCTION OCCURS . 225 § 3. STERIC HINDRANCE . 227 § 4. THREE MODELS 228 § 5. THE MEAN ABSORPTION COEFFICIENT FOR MODEL M X . . . 230 § 6. DISCUSSION 232 § 7. -APPLICATION TO THE MODELS M E AND M A . . . . . . . 236 § 8. FINAL DISCUSSION OF THE MEAN ABSORPTION COEFFICIENT . 238 § 9. THE EFFECT OF PARTICLE ABSORPTION ON SCATTERED INTENSITY 241 CH. III. MULTIPLE GUINIER CAMERA WITH ADJUSTABLE CURVED CRYSTAL MONOCHROMATOR 244 § 1. INTRODUCTION 244 § 2. RESOLVING POWER 246 § 3. MULTIPLE CAMERAS 248 § 4. DISTORTION IN THE EXTRA-EQUATORIAL PATTERNS . . . . . 248 § 5. CONSTRUCTIONAL DETAILS 251 § 6. ADJUSTABLE CURVED CRYSTAL MONOCHROMATOR; INTRODUCTION 254 § 7. SOURCE WIDTH REQUIRED TO COVER A GIVEN APERTURE . . 254 § 8. ABERRATIONS CAUSED BY OBLIQUE RAYS 255 § 9. A NEW WAY OF BENDING 256 § 10. MOUNTING OF THE CRYSTAL 257 § 11. EXAMPLE 259 § 12. DISCUSSION 259 PART G. ON THE DEGREE OF CRYSTALLINITY IN NATURAL RUBBER J. J. ARLMAN AND J. M. GOPPEL CH. I. GENERAL PART 263 § 1. INTRODUCTION 263 § 2. QUANTITATIVE X-RAY ANALYSIS, FIELD S METHOD . . . . 264 § 3. QUANTITATIVE X-RAY ANALYSIS, IMPROVED METHOD . . . 266 § 4. THE IMPROVED METHOD FOR FROZEN SAMPLES 271 § 5. INTERPRETATION OF PHOTOMETERRECORDS 272 § 6. THE ORIENTATION OF THE CRYSTALLITES 275 § 7. ELIMINATING ERRORS OWING TO CRYSTALLITE ORIENTATION . . 278 ~ * F CONTENTS XV PAGE CH. II. EXPERIMENTAL RESULTS 281 § 1. THE CRYSTALLINITY OF FROZEN RAW RUBBER 281 § 2. THE CRYSTALLINITY OF STRETCHED VULCANIZED RUBBER . . 283 § 3. X-RAY RESULTS AND THE WORK OF FLORY E.A 290 PART H. INVESTIGATIONS IN THE BIOLOGICAL FIELD D. R. RREGER CH. I. INTRODUCTION 299 CH. II. A COMPARATIVE OF A NUMBER OF WAXY COATINGS FROM PLANTS ON THE BASIS OF THEIR POWDER DIAGRAMS 303 § 1. SOME INTRODUCTORY AND METHODICAL REMARKS 303 § 2. DESCRIPTION AND CLASSIFICATION OF THE DIAGRAMS . . . 307 § 3. THE INTERPRETATION OF THE LONG SPACINGS 312 § 4. CONCLUSIONS FROM SOME INDIVIDUAL DIAGRAMS 318 § 5. SURVEY OF RESULTS 321 § 6. NOTES ON THE BIOLOGICAL ASPECT OF THE INVESTIGATION . 323 CH. III. INVESTIGATION INTO THE SUBMICROSCOPIC STRUCTURE OF THE WAX RODS OF THE SUGAR CANE STEM 326 § 1. SOME INTRODUCTORY REMARKS 325 § 2. RESULTS ATTAINED BY MEANS OF A STANDARD JT-RAY TECHNIQUE . . 326 § 3. RESULTS ATTAINED BY MEANS OF A NEW MICRO-METHOD . 331 § 4. THE DOUBLE REFRACTION OF THE RODS 335 § 5. THE ELECTRON MICROSCOPIC PICTURE OF THE RODS . . . . 338 CH. IV. A NEW MICRO-METHOD FOR X-RAY DIFFRACTION 340 § 1. INTRODUCTORY 340 § 2. THE COLLIMATOR 340 § 3. THE SCREENING CUP 342 § 4. MOUNTING THE SPECIMEN 344 § 5. THE DESIGN OF THE MICRO-CAMERA 345 § 6. THE LIMITS OF THE METHOD 347 § 7. POSSIBILITIES WITH MICRO-FOCUS TUBES 349 CH. V. THE CHAIN CONFIGURATION IN NATIVE STARCH AS DERIVED FROM A FIBRE PATTERN OF PART OF A SINGLE GRAIN 353 § 1. STARCH GRAINS USED AND X-RAY DIAGRAMS OBTAINED . . 353 § 2. EVALUATION OF THE DIAGRAMS 356 § 3. FIBRE PERIOD AND CHAIN CONFIGURATION 368 § 4. NOTES TO OTHER CHAIN CONFIGURATIONS SUGGESTED . . . 363 § 5. THE PACKING OF THE CHAINS 365
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spellingShingle Selected topics in x-ray crystallography from the Delft X-Ray Institutes
Monographs on theoretical and applied physics
Cristallographie
Rayons X - Diffraction
Crystallography
X-ray crystallography
X-rays Diffraction
Röntgenkristallographie (DE-588)4178310-4 gnd
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title Selected topics in x-ray crystallography from the Delft X-Ray Institutes
title_auth Selected topics in x-ray crystallography from the Delft X-Ray Institutes
title_exact_search Selected topics in x-ray crystallography from the Delft X-Ray Institutes
title_full Selected topics in x-ray crystallography from the Delft X-Ray Institutes ed. by J. Bouman
title_fullStr Selected topics in x-ray crystallography from the Delft X-Ray Institutes ed. by J. Bouman
title_full_unstemmed Selected topics in x-ray crystallography from the Delft X-Ray Institutes ed. by J. Bouman
title_short Selected topics in x-ray crystallography from the Delft X-Ray Institutes
title_sort selected topics in x ray crystallography from the delft x ray institutes
topic Cristallographie
Rayons X - Diffraction
Crystallography
X-ray crystallography
X-rays Diffraction
Röntgenkristallographie (DE-588)4178310-4 gnd
topic_facet Cristallographie
Rayons X - Diffraction
Crystallography
X-ray crystallography
X-rays Diffraction
Röntgenkristallographie
Aufsatzsammlung
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