1,3-dihydroxybenzene-2-13C: Its preparation and reaction with chlorine and bromine in aqueous solution

1,3‐cyclohexanedione‐2‐13C was prepared by intramolecular Claisen condensation of methyl 5‐oxohexanote‐6‐13C with sodium methoxide. Formation of the ketoester starting material involved treatment of a mixed dicarboxylic anhydride with an isotopicallylabelled Grignard reagent, methyl‐13C magnesium io...

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Veröffentlicht in:	Journal of labelled compounds & radiopharmaceuticals 1983-02, Vol.20 (2), p.243-256
Hauptverfasser:	Boyce, Scott D., Barefoot, Aldos C., Hornig, James F.
Format:	Artikel
Sprache:	eng
Schlagworte:	Catalytic Dehydrogenation Claisen Condensation Grignard Reaction Halogenation Resorcinol Trihalomethanes
Online-Zugang:	Volltext
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