Fast and mild alkaline solvothermal synthesis of nanostructured flower-like Na2Ti3O7 and its methylene blue adsorption capacity

•Hierarchical flower-like particles are synthesized by the solvothermal method.•The sodium titanates are obtained under mildly alkaline conditions (2 M NaOH).•A Short time of solvothermal reaction (8 h) is enough to obtain the sodium titanates.•The adsorption equilibrium was achieved in a short time...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Materials letters 2021-06, Vol.292, p.129589, Article 129589
Hauptverfasser: Reyes-Miranda, J., Garcia-Murillo, A., Garrido-Hernández, A., Carrillo-Romo, F. de J.
Format: Artikel
Sprache:eng
Schlagworte:
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:•Hierarchical flower-like particles are synthesized by the solvothermal method.•The sodium titanates are obtained under mildly alkaline conditions (2 M NaOH).•A Short time of solvothermal reaction (8 h) is enough to obtain the sodium titanates.•The adsorption equilibrium was achieved in a short time of 10 min. This work reports a facile solvothermal synthesis of hierarchical flower-like Na2Ti3O7 structures with fast and high methylene blue adsorption capacity. A mesoporous architecture of Na2Ti3O7 with a surface area of 159.63 m2-g-1 was produced under mild alkaline conditions (2 M NaOH) and a short reaction time (8 h). Interestingly, methylene blue adsorption equilibrium on the Na2Ti3O7 powders was achieved in a short time of 10 min. The pseudo-second-order kinetic model and the Langmuir isotherm model described the adsorption mechanism. The synthesized Na2Ti3O7 powders have interesting features that highlight their suitability for environmental applications.
ISSN:0167-577X
1873-4979
DOI:10.1016/j.matlet.2021.129589