Continuous microwave synthesis of Bi2O3 rods coated with a temperature-sensitive polymer
Poly( N -isopropylacrylamide) (PNIPAM) is an organic environment-sensitive material, which can be combined with photocatalysts to control the photocatalytic process. Herein, rodlike environment-sensitive Bi 2 O 3 (PNIPAM/Bi 2 O 3 ) was prepared by a novel one-step continuous microwave method. This n...
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| Veröffentlicht in: | Journal of materials science 2020-09, Vol.55 (25), p.11213-11225 |
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| container_title | Journal of materials science |
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| creator | Zhu, Xiaodie Lu, Ziyang Liu, Xinlin Song, Minshan Zhou, Guosheng Yu, Zehui Xu, Lingyan Liu, Qian Han, Song Chu, Jinyu |
| description | Poly(
N
-isopropylacrylamide) (PNIPAM) is an organic environment-sensitive material, which can be combined with photocatalysts to control the photocatalytic process. Herein, rodlike environment-sensitive Bi
2
O
3
(PNIPAM/Bi
2
O
3
) was prepared by a novel one-step continuous microwave method. This new method is efficient and convenient. The as-prepared PNIPAM/Bi
2
O
3
was very sensitive to temperature and pH, and the degradation rate in the environment of 25 °C and pH = 9 was 3.87 times than that in the environment of 45 °C and pH = 5. While Bi
2
O
3
is under the above various environmental conditions, its degradation rate did not change obviously. More interestingly, the introduction of PNIPAM and one-step continuous microwave method was beneficial to the transformation of Bi
2
O
3
from no specific shape to rodlike morphology without changing its crystal structure. This work not only developed a new one-step continuous microwave synthesis method, but also opened up new ideas for the controllability requirements of materials in special environment. |
| doi_str_mv | 10.1007/s10853-020-04799-w |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_webof</sourceid><recordid>TN_cdi_webofscience_primary_000532894000003</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>2411432414</sourcerecordid><originalsourceid>FETCH-LOGICAL-c356t-6cd5087727986233d40a45060d610dd05140df2f49b1e573d27bf5665978a6bb3</originalsourceid><addsrcrecordid>eNqNkE1vFSEUhkljE6_VP-CKxKWhHr5nljpRa9Kkm5q4I8zAWJpeuALj5P77cjtGd6YsYPM85_C-CL2lcEkB9IdCoZOcAAMCQvc9Wc_QjkrNieiAv0A7AMYIE4q-RK9KuQcAqRndoR9DijXEJS0F78OU02p_e1yOsd75EgpOM_4U2A3HObmCp2Srd3gN9Q5bXP3-4LOtS_ak-FhCDc09pIfj3ufX6Hy2D8W_-fNeoO9fPt8OV-T65uu34eM1mbhUlajJSei0ZrrvFOPcCbBCggKnKDgHkgpwM5tFP1Lf8jimx1kqJXvdWTWO_AK92-Yecvq1-FLNfVpybCsNE5QK3m7RKLZRLWEp2c_mkMPe5qOhYE4Nmq1B0xo0Tw2atUndJq1-THOZgo-T_yueKuSs6wWcDh9CtTWkOKQl1qa-f77aaL7RpRHxp8__Mvzne48PApSO</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2411432414</pqid></control><display><type>article</type><title>Continuous microwave synthesis of Bi2O3 rods coated with a temperature-sensitive polymer</title><source>Springer Nature - Complete Springer Journals</source><creator>Zhu, Xiaodie ; Lu, Ziyang ; Liu, Xinlin ; Song, Minshan ; Zhou, Guosheng ; Yu, Zehui ; Xu, Lingyan ; Liu, Qian ; Han, Song ; Chu, Jinyu</creator><creatorcontrib>Zhu, Xiaodie ; Lu, Ziyang ; Liu, Xinlin ; Song, Minshan ; Zhou, Guosheng ; Yu, Zehui ; Xu, Lingyan ; Liu, Qian ; Han, Song ; Chu, Jinyu</creatorcontrib><description>Poly(
N
-isopropylacrylamide) (PNIPAM) is an organic environment-sensitive material, which can be combined with photocatalysts to control the photocatalytic process. Herein, rodlike environment-sensitive Bi
2
O
3
(PNIPAM/Bi
2
O
3
) was prepared by a novel one-step continuous microwave method. This new method is efficient and convenient. The as-prepared PNIPAM/Bi
2
O
3
was very sensitive to temperature and pH, and the degradation rate in the environment of 25 °C and pH = 9 was 3.87 times than that in the environment of 45 °C and pH = 5. While Bi
2
O
3
is under the above various environmental conditions, its degradation rate did not change obviously. More interestingly, the introduction of PNIPAM and one-step continuous microwave method was beneficial to the transformation of Bi
2
O
3
from no specific shape to rodlike morphology without changing its crystal structure. This work not only developed a new one-step continuous microwave synthesis method, but also opened up new ideas for the controllability requirements of materials in special environment.</description><identifier>ISSN: 0022-2461</identifier><identifier>EISSN: 1573-4803</identifier><identifier>DOI: 10.1007/s10853-020-04799-w</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Bismuth oxides ; Bismuth trioxide ; Characterization and Evaluation of Materials ; Chemical Routes to Materials ; Chemistry and Materials Science ; Classical Mechanics ; Controllability ; Crystal structure ; Crystallography and Scattering Methods ; Degradation ; Materials Science ; Materials Science, Multidisciplinary ; Morphology ; Photocatalysis ; Polyisopropyl acrylamide ; Polymer Sciences ; Science & Technology ; Solid Mechanics ; Stability ; Technology</subject><ispartof>Journal of materials science, 2020-09, Vol.55 (25), p.11213-11225</ispartof><rights>Springer Science+Business Media, LLC, part of Springer Nature 2020</rights><rights>Springer Science+Business Media, LLC, part of Springer Nature 2020.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>true</woscitedreferencessubscribed><woscitedreferencescount>11</woscitedreferencescount><woscitedreferencesoriginalsourcerecordid>wos000532894000003</woscitedreferencesoriginalsourcerecordid><citedby>FETCH-LOGICAL-c356t-6cd5087727986233d40a45060d610dd05140df2f49b1e573d27bf5665978a6bb3</citedby><cites>FETCH-LOGICAL-c356t-6cd5087727986233d40a45060d610dd05140df2f49b1e573d27bf5665978a6bb3</cites><orcidid>0000-0001-8873-3695</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10853-020-04799-w$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10853-020-04799-w$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,778,782,27911,27912,41475,42544,51306</link.rule.ids></links><search><creatorcontrib>Zhu, Xiaodie</creatorcontrib><creatorcontrib>Lu, Ziyang</creatorcontrib><creatorcontrib>Liu, Xinlin</creatorcontrib><creatorcontrib>Song, Minshan</creatorcontrib><creatorcontrib>Zhou, Guosheng</creatorcontrib><creatorcontrib>Yu, Zehui</creatorcontrib><creatorcontrib>Xu, Lingyan</creatorcontrib><creatorcontrib>Liu, Qian</creatorcontrib><creatorcontrib>Han, Song</creatorcontrib><creatorcontrib>Chu, Jinyu</creatorcontrib><title>Continuous microwave synthesis of Bi2O3 rods coated with a temperature-sensitive polymer</title><title>Journal of materials science</title><addtitle>J Mater Sci</addtitle><addtitle>J MATER SCI</addtitle><description>Poly(
N
-isopropylacrylamide) (PNIPAM) is an organic environment-sensitive material, which can be combined with photocatalysts to control the photocatalytic process. Herein, rodlike environment-sensitive Bi
2
O
3
(PNIPAM/Bi
2
O
3
) was prepared by a novel one-step continuous microwave method. This new method is efficient and convenient. The as-prepared PNIPAM/Bi
2
O
3
was very sensitive to temperature and pH, and the degradation rate in the environment of 25 °C and pH = 9 was 3.87 times than that in the environment of 45 °C and pH = 5. While Bi
2
O
3
is under the above various environmental conditions, its degradation rate did not change obviously. More interestingly, the introduction of PNIPAM and one-step continuous microwave method was beneficial to the transformation of Bi
2
O
3
from no specific shape to rodlike morphology without changing its crystal structure. This work not only developed a new one-step continuous microwave synthesis method, but also opened up new ideas for the controllability requirements of materials in special environment.</description><subject>Bismuth oxides</subject><subject>Bismuth trioxide</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemical Routes to Materials</subject><subject>Chemistry and Materials Science</subject><subject>Classical Mechanics</subject><subject>Controllability</subject><subject>Crystal structure</subject><subject>Crystallography and Scattering Methods</subject><subject>Degradation</subject><subject>Materials Science</subject><subject>Materials Science, Multidisciplinary</subject><subject>Morphology</subject><subject>Photocatalysis</subject><subject>Polyisopropyl acrylamide</subject><subject>Polymer Sciences</subject><subject>Science & Technology</subject><subject>Solid Mechanics</subject><subject>Stability</subject><subject>Technology</subject><issn>0022-2461</issn><issn>1573-4803</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><sourceid>AOWDO</sourceid><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNqNkE1vFSEUhkljE6_VP-CKxKWhHr5nljpRa9Kkm5q4I8zAWJpeuALj5P77cjtGd6YsYPM85_C-CL2lcEkB9IdCoZOcAAMCQvc9Wc_QjkrNieiAv0A7AMYIE4q-RK9KuQcAqRndoR9DijXEJS0F78OU02p_e1yOsd75EgpOM_4U2A3HObmCp2Srd3gN9Q5bXP3-4LOtS_ak-FhCDc09pIfj3ufX6Hy2D8W_-fNeoO9fPt8OV-T65uu34eM1mbhUlajJSei0ZrrvFOPcCbBCggKnKDgHkgpwM5tFP1Lf8jimx1kqJXvdWTWO_AK92-Yecvq1-FLNfVpybCsNE5QK3m7RKLZRLWEp2c_mkMPe5qOhYE4Nmq1B0xo0Tw2atUndJq1-THOZgo-T_yueKuSs6wWcDh9CtTWkOKQl1qa-f77aaL7RpRHxp8__Mvzne48PApSO</recordid><startdate>20200901</startdate><enddate>20200901</enddate><creator>Zhu, Xiaodie</creator><creator>Lu, Ziyang</creator><creator>Liu, Xinlin</creator><creator>Song, Minshan</creator><creator>Zhou, Guosheng</creator><creator>Yu, Zehui</creator><creator>Xu, Lingyan</creator><creator>Liu, Qian</creator><creator>Han, Song</creator><creator>Chu, Jinyu</creator><general>Springer US</general><general>Springer Nature</general><general>Springer Nature B.V</general><scope>AOWDO</scope><scope>BLEPL</scope><scope>DTL</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>L6V</scope><scope>M7S</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>PTHSS</scope><orcidid>https://orcid.org/0000-0001-8873-3695</orcidid></search><sort><creationdate>20200901</creationdate><title>Continuous microwave synthesis of Bi2O3 rods coated with a temperature-sensitive polymer</title><author>Zhu, Xiaodie ; Lu, Ziyang ; Liu, Xinlin ; Song, Minshan ; Zhou, Guosheng ; Yu, Zehui ; Xu, Lingyan ; Liu, Qian ; Han, Song ; Chu, Jinyu</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c356t-6cd5087727986233d40a45060d610dd05140df2f49b1e573d27bf5665978a6bb3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Bismuth oxides</topic><topic>Bismuth trioxide</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemical Routes to Materials</topic><topic>Chemistry and Materials Science</topic><topic>Classical Mechanics</topic><topic>Controllability</topic><topic>Crystal structure</topic><topic>Crystallography and Scattering Methods</topic><topic>Degradation</topic><topic>Materials Science</topic><topic>Materials Science, Multidisciplinary</topic><topic>Morphology</topic><topic>Photocatalysis</topic><topic>Polyisopropyl acrylamide</topic><topic>Polymer Sciences</topic><topic>Science & Technology</topic><topic>Solid Mechanics</topic><topic>Stability</topic><topic>Technology</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Zhu, Xiaodie</creatorcontrib><creatorcontrib>Lu, Ziyang</creatorcontrib><creatorcontrib>Liu, Xinlin</creatorcontrib><creatorcontrib>Song, Minshan</creatorcontrib><creatorcontrib>Zhou, Guosheng</creatorcontrib><creatorcontrib>Yu, Zehui</creatorcontrib><creatorcontrib>Xu, Lingyan</creatorcontrib><creatorcontrib>Liu, Qian</creatorcontrib><creatorcontrib>Han, Song</creatorcontrib><creatorcontrib>Chu, Jinyu</creatorcontrib><collection>Web of Science - Science Citation Index Expanded - 2020</collection><collection>Web of Science Core Collection</collection><collection>Science Citation Index Expanded</collection><collection>CrossRef</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Science Database</collection><collection>ProQuest Engineering Collection</collection><collection>Engineering Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>Engineering Collection</collection><jtitle>Journal of materials science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Zhu, Xiaodie</au><au>Lu, Ziyang</au><au>Liu, Xinlin</au><au>Song, Minshan</au><au>Zhou, Guosheng</au><au>Yu, Zehui</au><au>Xu, Lingyan</au><au>Liu, Qian</au><au>Han, Song</au><au>Chu, Jinyu</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Continuous microwave synthesis of Bi2O3 rods coated with a temperature-sensitive polymer</atitle><jtitle>Journal of materials science</jtitle><stitle>J Mater Sci</stitle><stitle>J MATER SCI</stitle><date>2020-09-01</date><risdate>2020</risdate><volume>55</volume><issue>25</issue><spage>11213</spage><epage>11225</epage><pages>11213-11225</pages><issn>0022-2461</issn><eissn>1573-4803</eissn><abstract>Poly(
N
-isopropylacrylamide) (PNIPAM) is an organic environment-sensitive material, which can be combined with photocatalysts to control the photocatalytic process. Herein, rodlike environment-sensitive Bi
2
O
3
(PNIPAM/Bi
2
O
3
) was prepared by a novel one-step continuous microwave method. This new method is efficient and convenient. The as-prepared PNIPAM/Bi
2
O
3
was very sensitive to temperature and pH, and the degradation rate in the environment of 25 °C and pH = 9 was 3.87 times than that in the environment of 45 °C and pH = 5. While Bi
2
O
3
is under the above various environmental conditions, its degradation rate did not change obviously. More interestingly, the introduction of PNIPAM and one-step continuous microwave method was beneficial to the transformation of Bi
2
O
3
from no specific shape to rodlike morphology without changing its crystal structure. This work not only developed a new one-step continuous microwave synthesis method, but also opened up new ideas for the controllability requirements of materials in special environment.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10853-020-04799-w</doi><tpages>13</tpages><orcidid>https://orcid.org/0000-0001-8873-3695</orcidid></addata></record> |
| fulltext | fulltext |
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| ispartof | Journal of materials science, 2020-09, Vol.55 (25), p.11213-11225 |
| issn | 0022-2461 1573-4803 |
| language | eng |
| recordid | cdi_webofscience_primary_000532894000003 |
| source | Springer Nature - Complete Springer Journals |
| subjects | Bismuth oxides Bismuth trioxide Characterization and Evaluation of Materials Chemical Routes to Materials Chemistry and Materials Science Classical Mechanics Controllability Crystal structure Crystallography and Scattering Methods Degradation Materials Science Materials Science, Multidisciplinary Morphology Photocatalysis Polyisopropyl acrylamide Polymer Sciences Science & Technology Solid Mechanics Stability Technology |
| title | Continuous microwave synthesis of Bi2O3 rods coated with a temperature-sensitive polymer |
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