Preparation of copper nanoparticles by chemical reduction method using potassium borohydride
High dispersive copper nanoparticles were prepared by chemical reduction method using potassium borohydride as reducing agent. The effects of reactant ratio, concentration of CuSO 4, reaction temperature, and dispersant on the size of product and conversion rate were studied. The morphologies of cop...
Gespeichert in:
| Veröffentlicht in: | Transactions of Nonferrous Metals Society of China 2010-05, Vol.20 (z1), p.s240-s244 |
|---|---|
| Hauptverfasser: | , , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | s244 |
|---|---|
| container_issue | z1 |
| container_start_page | s240 |
| container_title | Transactions of Nonferrous Metals Society of China |
| container_volume | 20 |
| creator | ZHANG, Qiu-li YANG, Zhi-mao DING, Bing-jun LAN, Xin-zhe GUO, Ying-juan |
| description | High dispersive copper nanoparticles were prepared by chemical reduction method using potassium borohydride as reducing agent. The effects of reactant ratio, concentration of CuSO
4, reaction temperature, and dispersant on the size of product and conversion rate were studied. The morphologies of copper nanoparticles were characterized by scanning electron microscopy. The results show that the optimum process conditions are as follows: the molar ratio of KBH
4 to CuSO
4 is 0.75 (3:4), concentration of CuSO
4 is 0.4 mol/L, reaction temperature is 30 °C, and dispersant is
n-butyl alcohol. The average particles size of copper powders with spherical shape gained is about 100 nm. |
| doi_str_mv | 10.1016/S1003-6326(10)60047-7 |
| format | Article |
| fullrecord | <record><control><sourceid>wanfang_jour_proqu</sourceid><recordid>TN_cdi_wanfang_journals_zgysjsxb_e2010z1047</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><wanfj_id>zgysjsxb_e2010z1047</wanfj_id><els_id>S1003632610600477</els_id><sourcerecordid>zgysjsxb_e2010z1047</sourcerecordid><originalsourceid>FETCH-LOGICAL-c444t-1f9b25726dec63f045d29ea4f388a8c198d58050cc3d63cf1e31d8644f2d990a3</originalsourceid><addsrcrecordid>eNqFkF1LwzAUhnuh4Jz-BCGXE6kmTZq2VyLDLxgoqHdCyJKTLaNNatKq26-328Rbrw68POc9nCdJzgi-JJjwqxeCMU05zfiE4HOOMSvS4iAZ_cVHyXGMqyFnnJNR8v4coJVBdtY75A1Svm0hICedH-LOqhoimq-RWkJjlaxRAN2rHd1At_Qa9dG6BWp9J2O0fYPmPvjlWger4SQ5NLKOcPo7x8nb3e3r9CGdPd0_Tm9mqWKMdSkx1TzLi4xrUJwazHKdVSCZoWUpS0WqUuclzrFSVHOqDAFKdMkZM5muKizpOLnY935JZ6RbiJXvgxsuis1iHVfxey4gwwRvyKBjoCd7ug3-o4fYicZGBXUtHfg-CsILkjFKaTag-R5VwccYwIg22EaGtSBYbH2LnW-xFbuNdr7F9sT1fg-Grz8tBBGVBadA2wCqE9rbfxp-AMWEiyI</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1671243332</pqid></control><display><type>article</type><title>Preparation of copper nanoparticles by chemical reduction method using potassium borohydride</title><source>Elsevier ScienceDirect Journals</source><source>Alma/SFX Local Collection</source><creator>ZHANG, Qiu-li ; YANG, Zhi-mao ; DING, Bing-jun ; LAN, Xin-zhe ; GUO, Ying-juan</creator><creatorcontrib>ZHANG, Qiu-li ; YANG, Zhi-mao ; DING, Bing-jun ; LAN, Xin-zhe ; GUO, Ying-juan</creatorcontrib><description>High dispersive copper nanoparticles were prepared by chemical reduction method using potassium borohydride as reducing agent. The effects of reactant ratio, concentration of CuSO
4, reaction temperature, and dispersant on the size of product and conversion rate were studied. The morphologies of copper nanoparticles were characterized by scanning electron microscopy. The results show that the optimum process conditions are as follows: the molar ratio of KBH
4 to CuSO
4 is 0.75 (3:4), concentration of CuSO
4 is 0.4 mol/L, reaction temperature is 30 °C, and dispersant is
n-butyl alcohol. The average particles size of copper powders with spherical shape gained is about 100 nm.</description><identifier>ISSN: 1003-6326</identifier><identifier>DOI: 10.1016/S1003-6326(10)60047-7</identifier><language>eng</language><publisher>Elsevier Ltd</publisher><subject>Borohydrides ; chemical reduction ; Conversion ; Copper ; COPPER SULFATE ; Dispersants ; HYDRIDES ; MICA ; Nanoparticles ; Optimization ; PARTICLES ; Potassium ; potassium borohydride ; Reduction (chemical)</subject><ispartof>Transactions of Nonferrous Metals Society of China, 2010-05, Vol.20 (z1), p.s240-s244</ispartof><rights>2010 The Nonferrous Metals Society of China</rights><rights>Copyright © Wanfang Data Co. Ltd. All Rights Reserved.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c444t-1f9b25726dec63f045d29ea4f388a8c198d58050cc3d63cf1e31d8644f2d990a3</citedby></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Uhttp://www.wanfangdata.com.cn/images/PeriodicalImages/zgysjsxb-e/zgysjsxb-e.jpg</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/S1003-6326(10)60047-7$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3536,27903,27904,45974</link.rule.ids></links><search><creatorcontrib>ZHANG, Qiu-li</creatorcontrib><creatorcontrib>YANG, Zhi-mao</creatorcontrib><creatorcontrib>DING, Bing-jun</creatorcontrib><creatorcontrib>LAN, Xin-zhe</creatorcontrib><creatorcontrib>GUO, Ying-juan</creatorcontrib><title>Preparation of copper nanoparticles by chemical reduction method using potassium borohydride</title><title>Transactions of Nonferrous Metals Society of China</title><description>High dispersive copper nanoparticles were prepared by chemical reduction method using potassium borohydride as reducing agent. The effects of reactant ratio, concentration of CuSO
4, reaction temperature, and dispersant on the size of product and conversion rate were studied. The morphologies of copper nanoparticles were characterized by scanning electron microscopy. The results show that the optimum process conditions are as follows: the molar ratio of KBH
4 to CuSO
4 is 0.75 (3:4), concentration of CuSO
4 is 0.4 mol/L, reaction temperature is 30 °C, and dispersant is
n-butyl alcohol. The average particles size of copper powders with spherical shape gained is about 100 nm.</description><subject>Borohydrides</subject><subject>chemical reduction</subject><subject>Conversion</subject><subject>Copper</subject><subject>COPPER SULFATE</subject><subject>Dispersants</subject><subject>HYDRIDES</subject><subject>MICA</subject><subject>Nanoparticles</subject><subject>Optimization</subject><subject>PARTICLES</subject><subject>Potassium</subject><subject>potassium borohydride</subject><subject>Reduction (chemical)</subject><issn>1003-6326</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2010</creationdate><recordtype>article</recordtype><recordid>eNqFkF1LwzAUhnuh4Jz-BCGXE6kmTZq2VyLDLxgoqHdCyJKTLaNNatKq26-328Rbrw68POc9nCdJzgi-JJjwqxeCMU05zfiE4HOOMSvS4iAZ_cVHyXGMqyFnnJNR8v4coJVBdtY75A1Svm0hICedH-LOqhoimq-RWkJjlaxRAN2rHd1At_Qa9dG6BWp9J2O0fYPmPvjlWger4SQ5NLKOcPo7x8nb3e3r9CGdPd0_Tm9mqWKMdSkx1TzLi4xrUJwazHKdVSCZoWUpS0WqUuclzrFSVHOqDAFKdMkZM5muKizpOLnY935JZ6RbiJXvgxsuis1iHVfxey4gwwRvyKBjoCd7ug3-o4fYicZGBXUtHfg-CsILkjFKaTag-R5VwccYwIg22EaGtSBYbH2LnW-xFbuNdr7F9sT1fg-Grz8tBBGVBadA2wCqE9rbfxp-AMWEiyI</recordid><startdate>20100501</startdate><enddate>20100501</enddate><creator>ZHANG, Qiu-li</creator><creator>YANG, Zhi-mao</creator><creator>DING, Bing-jun</creator><creator>LAN, Xin-zhe</creator><creator>GUO, Ying-juan</creator><general>Elsevier Ltd</general><general>School of Metallurgical Engineering,Xi'an University of Architecture and Technology,Xi'an 710055,China%School of Science,Xi'an Jiaotong University,Xi'an 710049,China</general><scope>AAYXX</scope><scope>CITATION</scope><scope>8BQ</scope><scope>8FD</scope><scope>H8G</scope><scope>JG9</scope><scope>2B.</scope><scope>4A8</scope><scope>92I</scope><scope>93N</scope><scope>PSX</scope><scope>TCJ</scope></search><sort><creationdate>20100501</creationdate><title>Preparation of copper nanoparticles by chemical reduction method using potassium borohydride</title><author>ZHANG, Qiu-li ; YANG, Zhi-mao ; DING, Bing-jun ; LAN, Xin-zhe ; GUO, Ying-juan</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c444t-1f9b25726dec63f045d29ea4f388a8c198d58050cc3d63cf1e31d8644f2d990a3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2010</creationdate><topic>Borohydrides</topic><topic>chemical reduction</topic><topic>Conversion</topic><topic>Copper</topic><topic>COPPER SULFATE</topic><topic>Dispersants</topic><topic>HYDRIDES</topic><topic>MICA</topic><topic>Nanoparticles</topic><topic>Optimization</topic><topic>PARTICLES</topic><topic>Potassium</topic><topic>potassium borohydride</topic><topic>Reduction (chemical)</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>ZHANG, Qiu-li</creatorcontrib><creatorcontrib>YANG, Zhi-mao</creatorcontrib><creatorcontrib>DING, Bing-jun</creatorcontrib><creatorcontrib>LAN, Xin-zhe</creatorcontrib><creatorcontrib>GUO, Ying-juan</creatorcontrib><collection>CrossRef</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Copper Technical Reference Library</collection><collection>Materials Research Database</collection><collection>Wanfang Data Journals - Hong Kong</collection><collection>WANFANG Data Centre</collection><collection>Wanfang Data Journals</collection><collection>万方数据期刊 - 香港版</collection><collection>China Online Journals (COJ)</collection><collection>China Online Journals (COJ)</collection><jtitle>Transactions of Nonferrous Metals Society of China</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>ZHANG, Qiu-li</au><au>YANG, Zhi-mao</au><au>DING, Bing-jun</au><au>LAN, Xin-zhe</au><au>GUO, Ying-juan</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Preparation of copper nanoparticles by chemical reduction method using potassium borohydride</atitle><jtitle>Transactions of Nonferrous Metals Society of China</jtitle><date>2010-05-01</date><risdate>2010</risdate><volume>20</volume><issue>z1</issue><spage>s240</spage><epage>s244</epage><pages>s240-s244</pages><issn>1003-6326</issn><abstract>High dispersive copper nanoparticles were prepared by chemical reduction method using potassium borohydride as reducing agent. The effects of reactant ratio, concentration of CuSO
4, reaction temperature, and dispersant on the size of product and conversion rate were studied. The morphologies of copper nanoparticles were characterized by scanning electron microscopy. The results show that the optimum process conditions are as follows: the molar ratio of KBH
4 to CuSO
4 is 0.75 (3:4), concentration of CuSO
4 is 0.4 mol/L, reaction temperature is 30 °C, and dispersant is
n-butyl alcohol. The average particles size of copper powders with spherical shape gained is about 100 nm.</abstract><pub>Elsevier Ltd</pub><doi>10.1016/S1003-6326(10)60047-7</doi><tpages>5</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1003-6326 |
| ispartof | Transactions of Nonferrous Metals Society of China, 2010-05, Vol.20 (z1), p.s240-s244 |
| issn | 1003-6326 |
| language | eng |
| recordid | cdi_wanfang_journals_zgysjsxb_e2010z1047 |
| source | Elsevier ScienceDirect Journals; Alma/SFX Local Collection |
| subjects | Borohydrides chemical reduction Conversion Copper COPPER SULFATE Dispersants HYDRIDES MICA Nanoparticles Optimization PARTICLES Potassium potassium borohydride Reduction (chemical) |
| title | Preparation of copper nanoparticles by chemical reduction method using potassium borohydride |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-23T08%3A25%3A07IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-wanfang_jour_proqu&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Preparation%20of%20copper%20nanoparticles%20by%20chemical%20reduction%20method%20using%20potassium%20borohydride&rft.jtitle=Transactions%20of%20Nonferrous%20Metals%20Society%20of%20China&rft.au=ZHANG,%20Qiu-li&rft.date=2010-05-01&rft.volume=20&rft.issue=z1&rft.spage=s240&rft.epage=s244&rft.pages=s240-s244&rft.issn=1003-6326&rft_id=info:doi/10.1016/S1003-6326(10)60047-7&rft_dat=%3Cwanfang_jour_proqu%3Ezgysjsxb_e2010z1047%3C/wanfang_jour_proqu%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=1671243332&rft_id=info:pmid/&rft_wanfj_id=zgysjsxb_e2010z1047&rft_els_id=S1003632610600477&rfr_iscdi=true |