Synthesis and crystal structure of sodium praseodymium polyphosphate, NaPr(PO 3) 4
Reaction of Na 2CO 3, Pr 6O 11 and H 3PO 4 gave the sodium praseodymium polyphosphate NaPr(PO 3) 4. The title compound crystallized in the monoclinic P2 1/ n space group with a=0.9965(4) nm, b=1.31437(4) nm, c=0.72271(3) nm, β=90.429(3)°, V=0.9465(4) nm 3, Z=4, R=0.0493 and wR=0.1266 for 1855 indepe...
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| Veröffentlicht in: | Journal of rare earths 2009-02, Vol.27 (1), p.1-3 |
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| container_title | Journal of rare earths |
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| creator | Horchani-Naifer, K. Amami, J. Férid, M. |
| description | Reaction of Na
2CO
3, Pr
6O
11 and H
3PO
4 gave the sodium praseodymium polyphosphate NaPr(PO
3)
4. The title compound crystallized in the monoclinic
P2
1/
n space group with
a=0.9965(4) nm,
b=1.31437(4) nm,
c=0.72271(3) nm, β=90.429(3)°,
V=0.9465(4) nm
3,
Z=4,
R=0.0493 and
wR=0.1266 for 1855 independent reflections. The structure of NaPr(PO
3)
4 consisted of PrO
8 polyhedra sharing oxygen atoms with phosphoric group PO
4 to form a three-dimensional framework, delimiting intersecting tunnels in which the sodium ion was located. Each Na
+ ion was bonded to seven oxygen atoms. |
| doi_str_mv | 10.1016/S1002-0721(08)60179-9 |
| format | Article |
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2CO
3, Pr
6O
11 and H
3PO
4 gave the sodium praseodymium polyphosphate NaPr(PO
3)
4. The title compound crystallized in the monoclinic
P2
1/
n space group with
a=0.9965(4) nm,
b=1.31437(4) nm,
c=0.72271(3) nm, β=90.429(3)°,
V=0.9465(4) nm
3,
Z=4,
R=0.0493 and
wR=0.1266 for 1855 independent reflections. The structure of NaPr(PO
3)
4 consisted of PrO
8 polyhedra sharing oxygen atoms with phosphoric group PO
4 to form a three-dimensional framework, delimiting intersecting tunnels in which the sodium ion was located. Each Na
+ ion was bonded to seven oxygen atoms.</description><identifier>ISSN: 1002-0721</identifier><identifier>EISSN: 2509-4963</identifier><identifier>DOI: 10.1016/S1002-0721(08)60179-9</identifier><language>eng</language><publisher>Elsevier B.V</publisher><subject>crystal structure ; infrared spectroscopy ; polyphosphate ; praseodymium ; rare earths</subject><ispartof>Journal of rare earths, 2009-02, Vol.27 (1), p.1-3</ispartof><rights>2009 The Chinese Society of Rare Earths</rights><rights>Copyright © Wanfang Data Co. Ltd. All Rights Reserved.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c2891-8913d948b9f6dcc177378dbbde7688934ce4ecfabe7e61d643fdd2ef544253bc3</citedby><cites>FETCH-LOGICAL-c2891-8913d948b9f6dcc177378dbbde7688934ce4ecfabe7e61d643fdd2ef544253bc3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Uhttp://www.wanfangdata.com.cn/images/PeriodicalImages/zgxtxb-e/zgxtxb-e.jpg</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/S1002-0721(08)60179-9$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,777,781,3537,27905,27906,45976</link.rule.ids></links><search><creatorcontrib>Horchani-Naifer, K.</creatorcontrib><creatorcontrib>Amami, J.</creatorcontrib><creatorcontrib>Férid, M.</creatorcontrib><title>Synthesis and crystal structure of sodium praseodymium polyphosphate, NaPr(PO 3) 4</title><title>Journal of rare earths</title><description>Reaction of Na
2CO
3, Pr
6O
11 and H
3PO
4 gave the sodium praseodymium polyphosphate NaPr(PO
3)
4. The title compound crystallized in the monoclinic
P2
1/
n space group with
a=0.9965(4) nm,
b=1.31437(4) nm,
c=0.72271(3) nm, β=90.429(3)°,
V=0.9465(4) nm
3,
Z=4,
R=0.0493 and
wR=0.1266 for 1855 independent reflections. The structure of NaPr(PO
3)
4 consisted of PrO
8 polyhedra sharing oxygen atoms with phosphoric group PO
4 to form a three-dimensional framework, delimiting intersecting tunnels in which the sodium ion was located. Each Na
+ ion was bonded to seven oxygen atoms.</description><subject>crystal structure</subject><subject>infrared spectroscopy</subject><subject>polyphosphate</subject><subject>praseodymium</subject><subject>rare earths</subject><issn>1002-0721</issn><issn>2509-4963</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2009</creationdate><recordtype>article</recordtype><recordid>eNqFkF9LwzAUxYMoOKcfQciTbGA1adKmeRIZ_gPR4fQ5pMmt6-iamrRq_fTWTXz14XK58Dvncg5Cx5ScUULT8wUlJI6IiOmEZNOUUCEjuYNGcUJkxGXKdtHoD9lHByGsCGEikWSEnhZ93S4hlAHr2mLj-9DqCofWd6btPGBX4OBs2a1x43UAZ_v15nBV3yxdaJa6hVP8oOd-Mn_EbIr5IdordBXg6HeP0cv11fPsNrp_vLmbXd5HJs4kjYZhVvIsl0VqjaFCMJHZPLcg0iyTjBvgYAqdg4CU2pSzwtoYioTzOGG5YWM03fp-6LrQ9atauc7Xw0f19frZfuYKYkIkGZLTgT3Zso13bx2EVq3LYKCqdA2uC4pxJjiL2QAmW9B4F4KHQjW-XGvfK0rUT9tq07b6qVKRTG3aVnLQXWx1MCR-L8GrYEqoDdjSg2mVdeU_Dt8anYbf</recordid><startdate>20090201</startdate><enddate>20090201</enddate><creator>Horchani-Naifer, K.</creator><creator>Amami, J.</creator><creator>Férid, M.</creator><general>Elsevier B.V</general><general>Research Unit of Rare Earth Materials,National Research Center in Sciences of Materials,B,P,95 Hammam-Lif,2050,Tunisia</general><scope>AAYXX</scope><scope>CITATION</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>2B.</scope><scope>4A8</scope><scope>92I</scope><scope>93N</scope><scope>PSX</scope><scope>TCJ</scope></search><sort><creationdate>20090201</creationdate><title>Synthesis and crystal structure of sodium praseodymium polyphosphate, NaPr(PO 3) 4</title><author>Horchani-Naifer, K. ; Amami, J. ; Férid, M.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c2891-8913d948b9f6dcc177378dbbde7688934ce4ecfabe7e61d643fdd2ef544253bc3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2009</creationdate><topic>crystal structure</topic><topic>infrared spectroscopy</topic><topic>polyphosphate</topic><topic>praseodymium</topic><topic>rare earths</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Horchani-Naifer, K.</creatorcontrib><creatorcontrib>Amami, J.</creatorcontrib><creatorcontrib>Férid, M.</creatorcontrib><collection>CrossRef</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Wanfang Data Journals - Hong Kong</collection><collection>WANFANG Data Centre</collection><collection>Wanfang Data Journals</collection><collection>万方数据期刊 - 香港版</collection><collection>China Online Journals (COJ)</collection><collection>China Online Journals (COJ)</collection><jtitle>Journal of rare earths</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Horchani-Naifer, K.</au><au>Amami, J.</au><au>Férid, M.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and crystal structure of sodium praseodymium polyphosphate, NaPr(PO 3) 4</atitle><jtitle>Journal of rare earths</jtitle><date>2009-02-01</date><risdate>2009</risdate><volume>27</volume><issue>1</issue><spage>1</spage><epage>3</epage><pages>1-3</pages><issn>1002-0721</issn><eissn>2509-4963</eissn><abstract>Reaction of Na
2CO
3, Pr
6O
11 and H
3PO
4 gave the sodium praseodymium polyphosphate NaPr(PO
3)
4. The title compound crystallized in the monoclinic
P2
1/
n space group with
a=0.9965(4) nm,
b=1.31437(4) nm,
c=0.72271(3) nm, β=90.429(3)°,
V=0.9465(4) nm
3,
Z=4,
R=0.0493 and
wR=0.1266 for 1855 independent reflections. The structure of NaPr(PO
3)
4 consisted of PrO
8 polyhedra sharing oxygen atoms with phosphoric group PO
4 to form a three-dimensional framework, delimiting intersecting tunnels in which the sodium ion was located. Each Na
+ ion was bonded to seven oxygen atoms.</abstract><pub>Elsevier B.V</pub><doi>10.1016/S1002-0721(08)60179-9</doi><tpages>3</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1002-0721 |
| ispartof | Journal of rare earths, 2009-02, Vol.27 (1), p.1-3 |
| issn | 1002-0721 2509-4963 |
| language | eng |
| recordid | cdi_wanfang_journals_zgxtxb_e200901001 |
| source | Elsevier ScienceDirect Journals; Alma/SFX Local Collection |
| subjects | crystal structure infrared spectroscopy polyphosphate praseodymium rare earths |
| title | Synthesis and crystal structure of sodium praseodymium polyphosphate, NaPr(PO 3) 4 |
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