Synthesis and Characterization of Rare Earth Solid Complexes with Sodium 5-Aminosalicylate
Ten new rare earth solid complexes were synthesized by the reaction of sodium 5-aminosalicyliate with rare earth chloride. The structure character, physical and chemical properties of these complexes were studied by IR, UV,^1H NMR spectra, TG-DTA, fluorescence, elemental analyses, molar conductance...
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Veröffentlicht in: | Journal of rare earths 2005-04, Vol.23 (2), p.143-147 |
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description | Ten new rare earth solid complexes were synthesized by the reaction of sodium 5-aminosalicyliate with rare earth chloride. The structure character, physical and chemical properties of these complexes were studied by IR, UV,^1H NMR spectra, TG-DTA, fluorescence, elemental analyses, molar conductance and magnetic susceptibility. The ten rare earth complexes exist in dimeric form probably and the coordination number is seven. The antibacterial activity of the ligand and six complexes was also tested against Staphylococcus aureus, Escherichia coli and Bacillus subtilis, and the effect of Yb complex at 20mg·ml^-1 against Staphylococcus aureus is most significant. |
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The structure character, physical and chemical properties of these complexes were studied by IR, UV,^1H NMR spectra, TG-DTA, fluorescence, elemental analyses, molar conductance and magnetic susceptibility. The ten rare earth complexes exist in dimeric form probably and the coordination number is seven. The antibacterial activity of the ligand and six complexes was also tested against Staphylococcus aureus, Escherichia coli and Bacillus subtilis, and the effect of Yb complex at 20mg·ml^-1 against Staphylococcus aureus is most significant.</description><identifier>ISSN: 1002-0721</identifier><identifier>EISSN: 2509-4963</identifier><language>eng</language><publisher>Department of Chemistry, Zhoukou Normal University, Zhoukou 466000, China%Hubei Institute of Aerospace Chemotechnology, Xiangfan 441003, China</publisher><subject>AIDS ; 抗细菌活性 ; 氨基水杨酸 ; 稀土元素复合物 ; 预防方法</subject><ispartof>Journal of rare earths, 2005-04, Vol.23 (2), p.143-147</ispartof><rights>Copyright © Wanfang Data Co. Ltd. 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The antibacterial activity of the ligand and six complexes was also tested against Staphylococcus aureus, Escherichia coli and Bacillus subtilis, and the effect of Yb complex at 20mg·ml^-1 against Staphylococcus aureus is most significant.</description><subject>AIDS</subject><subject>抗细菌活性</subject><subject>氨基水杨酸</subject><subject>稀土元素复合物</subject><subject>预防方法</subject><issn>1002-0721</issn><issn>2509-4963</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2005</creationdate><recordtype>article</recordtype><recordid>eNotj01Lw0AQhoMoWKv_YfEgeAhM9iPJHkupH1AQrF68hEmyabZudtvshn78eqP1MgPvPDwvcxFNqAAZc5myy2iSANAYMppcRzfebwBYJiRMoq_V0YZWee0J2prMW-yxCqrXJwzaWeIa8o69IgvsQ0tWzugRct3WqIPyZK__wloPHRHxrNPWeTS6OhoM6ja6atB4dfe_p9Hn0-Jj_hIv355f57NlXFGehRhFAllaMqCiqYGVeQolh6wSqaQcxwuqPFGshPETKVWW11jymle8TEWaUs6m0ePZu0fboF0XGzf0dmwsTutDOJSFogACxsFG9uHMbnu3G5QPRad9pYxBq9zgCyopSMF-pfdnsGqdXe_0qC2x-m60UUUiMi7zJGU_H_pqBw</recordid><startdate>20050401</startdate><enddate>20050401</enddate><creator>张秀英 李书静</creator><general>Department of Chemistry, Zhoukou Normal University, Zhoukou 466000, China%Hubei Institute of Aerospace Chemotechnology, Xiangfan 441003, China</general><general>Henan Key Laboratory for Environmental Pollution Control, College of Chemistry and Environmental Science, Henan Normal University, Xinxiang 453007, China%Henan Key Laboratory for Environmental Pollution Control, College of Chemistry and Environmental Science, Henan Normal University, Xinxiang 453007, China</general><scope>2RA</scope><scope>92L</scope><scope>CQIGP</scope><scope>W94</scope><scope>~WA</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope><scope>2B.</scope><scope>4A8</scope><scope>92I</scope><scope>93N</scope><scope>PSX</scope><scope>TCJ</scope></search><sort><creationdate>20050401</creationdate><title>Synthesis and Characterization of Rare Earth Solid Complexes with Sodium 5-Aminosalicylate</title><author>张秀英 李书静</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c247t-a51076b3025fd03b860b407c56924a76bae81e3b049699e78dab4d4c4b6566243</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2005</creationdate><topic>AIDS</topic><topic>抗细菌活性</topic><topic>氨基水杨酸</topic><topic>稀土元素复合物</topic><topic>预防方法</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>张秀英 李书静</creatorcontrib><collection>中文科技期刊数据库</collection><collection>中文科技期刊数据库-CALIS站点</collection><collection>中文科技期刊数据库-7.0平台</collection><collection>中文科技期刊数据库-自然科学</collection><collection>中文科技期刊数据库- 镜像站点</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Wanfang Data Journals - Hong Kong</collection><collection>WANFANG Data Centre</collection><collection>Wanfang Data Journals</collection><collection>万方数据期刊 - 香港版</collection><collection>China Online Journals (COJ)</collection><collection>China Online Journals (COJ)</collection><jtitle>Journal of rare earths</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>张秀英 李书静</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and Characterization of Rare Earth Solid Complexes with Sodium 5-Aminosalicylate</atitle><jtitle>Journal of rare earths</jtitle><addtitle>Journal of Rare Earths</addtitle><date>2005-04-01</date><risdate>2005</risdate><volume>23</volume><issue>2</issue><spage>143</spage><epage>147</epage><pages>143-147</pages><issn>1002-0721</issn><eissn>2509-4963</eissn><abstract>Ten new rare earth solid complexes were synthesized by the reaction of sodium 5-aminosalicyliate with rare earth chloride. The structure character, physical and chemical properties of these complexes were studied by IR, UV,^1H NMR spectra, TG-DTA, fluorescence, elemental analyses, molar conductance and magnetic susceptibility. The ten rare earth complexes exist in dimeric form probably and the coordination number is seven. The antibacterial activity of the ligand and six complexes was also tested against Staphylococcus aureus, Escherichia coli and Bacillus subtilis, and the effect of Yb complex at 20mg·ml^-1 against Staphylococcus aureus is most significant.</abstract><pub>Department of Chemistry, Zhoukou Normal University, Zhoukou 466000, China%Hubei Institute of Aerospace Chemotechnology, Xiangfan 441003, China</pub><tpages>5</tpages></addata></record> |
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subjects | AIDS 抗细菌活性 氨基水杨酸 稀土元素复合物 预防方法 |
title | Synthesis and Characterization of Rare Earth Solid Complexes with Sodium 5-Aminosalicylate |
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