Synthesis of powdered silver nanoparticles using hydrogen in aqueous medium
Environmentally benign one-pot protocol is used in the synthesis of silver nanoparticles （AgNPs） in powder form, involving the reduction of silver nitrate in the presence of fully hydrolyzed polyvinyl alcohol （PVA） as stabilizer by hydrogen （H2） as reducing agent in aqueous medium. Fully hydrolyzed...
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| Veröffentlicht in: | Particuology 2012-02, Vol.10 (1), p.140-143 |
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| container_title | Particuology |
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| creator | Bhatte, Kushal D. Deshmukh, Krishna M. Patil, Yogesh P. Sawant, Dinesh N. Fujita, Shin-Ichiro Arai, Masahiko Bhanage, Bhalchandra M. |
| description | Environmentally benign one-pot protocol is used in the synthesis of silver nanoparticles （AgNPs） in powder form, involving the reduction of silver nitrate in the presence of fully hydrolyzed polyvinyl alcohol （PVA） as stabilizer by hydrogen （H2） as reducing agent in aqueous medium. Fully hydrolyzed biodegradable PVA has extremely low cytotoxicity, making it a favorable stabilizer from green perspective. In the present methodology, essentially naked silver nanoparticles are obtained in good yield. The prepared sil- ver nanoparticles were characterized by TEM, XRD, EDAX, UV-Vis spectroscopy and DLS histogram, and studied for its activity as a recyclable catalyst for synthesis of different enaminones. |
| doi_str_mv | 10.1016/j.partic.2011.05.005 |
| format | Article |
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Fully hydrolyzed biodegradable PVA has extremely low cytotoxicity, making it a favorable stabilizer from green perspective. In the present methodology, essentially naked silver nanoparticles are obtained in good yield. 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Fully hydrolyzed biodegradable PVA has extremely low cytotoxicity, making it a favorable stabilizer from green perspective. In the present methodology, essentially naked silver nanoparticles are obtained in good yield. The prepared sil- ver nanoparticles were characterized by TEM, XRD, EDAX, UV-Vis spectroscopy and DLS histogram, and studied for its activity as a recyclable catalyst for synthesis of different enaminones.</abstract><pub>Elsevier B.V</pub><doi>10.1016/j.partic.2011.05.005</doi><tpages>4</tpages></addata></record> |
| fulltext | fulltext |
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| ispartof | Particuology, 2012-02, Vol.10 (1), p.140-143 |
| issn | 1674-2001 2210-4291 |
| language | eng |
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| source | Elsevier ScienceDirect Journals; Alma/SFX Local Collection |
| subjects | AGNPS Aqueous media Biodegradability Catalysis Enaminones synthesis Hydrogen Nanoparticles Polyvinyl alcohols Silver Silver nanoparticles Silver nitrates Spectroscopy Synthesis Transmission electron microscopy 可生物降解 合成 氢 水溶液 粉末状 聚乙烯醇 银纳米粒子 |
| title | Synthesis of powdered silver nanoparticles using hydrogen in aqueous medium |
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