C60-TEGs/PdCl2催化Suzuki反应绿色合成联苯乙酸
采用水溶性富勒烯负载PdCl2纳米催化剂[C60-TEGs/PdCl2]催化对溴苯乙酸和苯硼酸在纯水中绿色合成联苯乙酸。分别考察催化剂用量、反应温度、反应时间、碱的种类以及用量对联苯乙酸产率的影响,摸索出环保、经济、简便高效的联苯乙酸合成工艺条件。优化后的合成工艺条件为:催化剂量0.01mol%,2mmol K2CO3作为碱,室温纯水中反应4h,其产率能够达到94.7%。...
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| Veröffentlicht in: | 宜春学院学报 2018-12, Vol.40 (12), p.12-14 |
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| container_title | 宜春学院学报 |
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| creator | 周秀明 李景波 刘万云 |
| description | 采用水溶性富勒烯负载PdCl2纳米催化剂[C60-TEGs/PdCl2]催化对溴苯乙酸和苯硼酸在纯水中绿色合成联苯乙酸。分别考察催化剂用量、反应温度、反应时间、碱的种类以及用量对联苯乙酸产率的影响,摸索出环保、经济、简便高效的联苯乙酸合成工艺条件。优化后的合成工艺条件为:催化剂量0.01mol%,2mmol K2CO3作为碱,室温纯水中反应4h,其产率能够达到94.7%。 |
| doi_str_mv | 10.3969/j.issn.1671-380X.2018.12.004 |
| format | Article |
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| source | 国家哲学社会科学学术期刊数据库 (National Social Sciences Database) |
| title | C60-TEGs/PdCl2催化Suzuki反应绿色合成联苯乙酸 |
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