新型去氢枞基1,3,4-(噁)二唑的合成与表征
TQ225.24; 以去氢枞酸为原料,经酰化得到酰氯,酰氯与85%(质量分数)水合肼反应制备出去氢枞酰肼,去氢枞酰肼再与5种芳香酰氯反应得N,N'-二酰基肼,其再经POCl3脱水闭环反应,合成了5种新的2-去氢枞基-5-芳基-1,3,4-(噁)二唑.研究了合成反应条件;每步收率均在75%以上....
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| Veröffentlicht in: | 现代化工 2007, Vol.27 (8), p.42-44 |
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| container_title | 现代化工 |
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| creator | 韩春蕊 宋湛谦 商士斌 高宏 |
| description | TQ225.24; 以去氢枞酸为原料,经酰化得到酰氯,酰氯与85%(质量分数)水合肼反应制备出去氢枞酰肼,去氢枞酰肼再与5种芳香酰氯反应得N,N'-二酰基肼,其再经POCl3脱水闭环反应,合成了5种新的2-去氢枞基-5-芳基-1,3,4-(噁)二唑.研究了合成反应条件;每步收率均在75%以上. |
| doi_str_mv | 10.3321/j.issn:0253-4320.2007.08.009 |
| format | Article |
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| source | Alma/SFX Local Collection |
| title | 新型去氢枞基1,3,4-(噁)二唑的合成与表征 |
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