Synthesis of Spin-ladder Sr14Cu24O41 Material by Citrates Sol-gel Method

Synthesis of Spin-ladder Sr14Cu24O41 Material by Citrates Sol-gel Method

A new process to synthesize polycrystalline samples of Sr14Cu24O41 was presented. Firstly, dry gel powder of Sr14Cu24O41 was synthesized by the citrates sol-gel method, using Sr（NO3）2, Cu（NO3）2, ethylene glycol and citrate acid as raw materials. Then, polycrystalline samples of Sr14Cu24O41 were prep...

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Veröffentlicht in:Journal of Wuhan University of Technology. Materials science edition 2008-04, Vol.23 (2), p.173-176
Hauptverfasser: Wang, Lili, Wei, Hui, Hu, Ni, Xiong, Rui, Yu, Zuxing, Tang, Wufeng, Shi, Jing
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Chemistry and Materials Science
Materials Science
Scanning electron microscopy
Sr14Cu24O41
制备方法
固态反应
柠檬酸盐溶胶-凝胶法
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container_start_page 173
container_title Journal of Wuhan University of Technology. Materials science edition
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creator Wang, Lili
Wei, Hui
Hu, Ni
Xiong, Rui
Yu, Zuxing
Tang, Wufeng
Shi, Jing
description A new process to synthesize polycrystalline samples of Sr14Cu24O41 was presented. Firstly, dry gel powder of Sr14Cu24O41 was synthesized by the citrates sol-gel method, using Sr（NO3）2, Cu（NO3）2, ethylene glycol and citrate acid as raw materials. Then, polycrystalline samples of Sr14Cu24O41 were prepared by solid-state reaction. Thermal Gravimetric and Differential Thermal Analysis（TG-DTA） showed that the temperature for solid-state reaction is at 942 ℃. The samples are identified to be single phase by X-ray Diffraction（XRD） and Scanning Electron Microscopy（SEM）. The SEM pictures showed that the first-step particles were at even size of about 100 nm by this technique. The electronic transport measurements showed that the doping compound were semiconductor with a crossover temperature T in the Arrhenius plot of the resistivity versus temprature.
doi_str_mv 10.1007/s11595-006-2173-8
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Firstly, dry gel powder of Sr14Cu24O41 was synthesized by the citrates sol-gel method, using Sr（NO3）2, Cu（NO3）2, ethylene glycol and citrate acid as raw materials. Then, polycrystalline samples of Sr14Cu24O41 were prepared by solid-state reaction. Thermal Gravimetric and Differential Thermal Analysis（TG-DTA） showed that the temperature for solid-state reaction is at 942 ℃. The samples are identified to be single phase by X-ray Diffraction（XRD） and Scanning Electron Microscopy（SEM）. The SEM pictures showed that the first-step particles were at even size of about 100 nm by this technique. 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subjects Chemistry and Materials Science
Materials Science
Scanning electron microscopy
Sr14Cu24O41
制备方法
固态反应
柠檬酸盐溶胶-凝胶法
title Synthesis of Spin-ladder Sr14Cu24O41 Material by Citrates Sol-gel Method
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