Preparation and thermal treatment of Pd/Ag composite membrane on a porous α-alumina tube by sequential electroless plating technique for H2 separation
TE3; Pd/Ag/α-Al2O3 composite membranes were prepared by sequential electroless plating technique. The prepared membranes were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive spec-troscopy, and inductively coupled plasma atomic emission spectroscopy tec...
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| Veröffentlicht in: | Journal of natural gas chemistry 2008, Vol.17 (4), p.321-326 |
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| container_title | Journal of natural gas chemistry |
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| creator | NAVAEI ALVAR, E REZA GOLMOHAMMADI, M REZAEI, M NAVAEI ALVAR, H MARDANLOO, A HABIBZAD NOUHIAN, S DIDARI, M |
| description | TE3; Pd/Ag/α-Al2O3 composite membranes were prepared by sequential electroless plating technique. The prepared membranes were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive spec-troscopy, and inductively coupled plasma atomic emission spectroscopy techniques (ICP-AES). Effects of annealing time, Ag content, and air treatment on the hydrogen permeation flux and morphology of the alloys were investigated. The results of the investigation showed that the prepared type of tube had a good potential as substrate for membrane preparation. In addition, a uniform defect-free alloy was prepared by annealing at 550 ℃ in H2 atmosphere. The permeation results showed an increase in H2 permeation flux by increasing the Ag content and the annealing time. In addition, the air treatment of the prepared membranes at 400 ℃ for 1 h changed the morphology of the alloy and substantially enhanced the hydrogen flux. |
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The prepared membranes were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive spec-troscopy, and inductively coupled plasma atomic emission spectroscopy techniques (ICP-AES). Effects of annealing time, Ag content, and air treatment on the hydrogen permeation flux and morphology of the alloys were investigated. The results of the investigation showed that the prepared type of tube had a good potential as substrate for membrane preparation. In addition, a uniform defect-free alloy was prepared by annealing at 550 ℃ in H2 atmosphere. The permeation results showed an increase in H2 permeation flux by increasing the Ag content and the annealing time. In addition, the air treatment of the prepared membranes at 400 ℃ for 1 h changed the morphology of the alloy and substantially enhanced the hydrogen flux.</description><identifier>ISSN: 1003-9953</identifier><language>eng</language><publisher>Chengdu: Dalian Institute of Chemical Physics</publisher><subject>Alternative fuels. Production and utilization ; Applied sciences ; Energy ; Exact sciences and technology ; Fuels ; Hydrogen</subject><ispartof>Journal of natural gas chemistry, 2008, Vol.17 (4), p.321-326</ispartof><rights>2009 INIST-CNRS</rights><rights>Copyright © Wanfang Data Co. Ltd. All Rights Reserved.</rights><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Uhttp://www.wanfangdata.com.cn/images/PeriodicalImages/trqhxzz-e/trqhxzz-e.jpg</thumbnail><link.rule.ids>314,780,784,4023</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=21012341$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>NAVAEI ALVAR, E</creatorcontrib><creatorcontrib>REZA GOLMOHAMMADI, M</creatorcontrib><creatorcontrib>REZAEI, M</creatorcontrib><creatorcontrib>NAVAEI ALVAR, H</creatorcontrib><creatorcontrib>MARDANLOO, A</creatorcontrib><creatorcontrib>HABIBZAD NOUHIAN, S</creatorcontrib><creatorcontrib>DIDARI, M</creatorcontrib><title>Preparation and thermal treatment of Pd/Ag composite membrane on a porous α-alumina tube by sequential electroless plating technique for H2 separation</title><title>Journal of natural gas chemistry</title><description>TE3; Pd/Ag/α-Al2O3 composite membranes were prepared by sequential electroless plating technique. The prepared membranes were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive spec-troscopy, and inductively coupled plasma atomic emission spectroscopy techniques (ICP-AES). Effects of annealing time, Ag content, and air treatment on the hydrogen permeation flux and morphology of the alloys were investigated. The results of the investigation showed that the prepared type of tube had a good potential as substrate for membrane preparation. In addition, a uniform defect-free alloy was prepared by annealing at 550 ℃ in H2 atmosphere. The permeation results showed an increase in H2 permeation flux by increasing the Ag content and the annealing time. In addition, the air treatment of the prepared membranes at 400 ℃ for 1 h changed the morphology of the alloy and substantially enhanced the hydrogen flux.</description><subject>Alternative fuels. Production and utilization</subject><subject>Applied sciences</subject><subject>Energy</subject><subject>Exact sciences and technology</subject><subject>Fuels</subject><subject>Hydrogen</subject><issn>1003-9953</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2008</creationdate><recordtype>article</recordtype><recordid>eNo1kE1OwzAQhbMAifJzh9mwQYrwT5I2y6oCilSJLrqPJvakTZXYqe0I2otwDi7CmTAqrGbzzfee3kUy4YzJtCxzeZVce79nLGNSlJPkc-1oQIehtQbQaAg7cj12EBxh6MkEsA2s9eN8C8r2g_VtIOiprx0agt8nGKyzo4fvrxS7sW8NQhhrgvoIng5jVLTRRx2p4GxH3sPQxTyzhUBqZ9qIQGMdLEXk_7vcJpcNdp7u_u5Nsnl-2iyW6ert5XUxX6VDkYuUSj0tc8aKTBeZmHKVU0Y1SSGUUkw3mCFKqVUjs5JNNau5rnmNSvKCZnk-lTfJw1n7jqZBs632dnQmBlbBHXYfp1NFgrFZXIuJCN-f4QG9wq6JC6jWV4Nre3THSnDGhcy4_AFJNXVh</recordid><startdate>2008</startdate><enddate>2008</enddate><creator>NAVAEI ALVAR, E</creator><creator>REZA GOLMOHAMMADI, M</creator><creator>REZAEI, M</creator><creator>NAVAEI ALVAR, H</creator><creator>MARDANLOO, A</creator><creator>HABIBZAD NOUHIAN, S</creator><creator>DIDARI, M</creator><general>Dalian Institute of Chemical Physics</general><general>Department of Mining & Metallurgy Engineering, Amirkabir University of Technology, Tehran, Iran%Sarv Oil & Gas Industries Development Co, Tehran, Iran%Department of Chemical Engineering, Faculty of Engineering, University of Kashan, Kashan, Iran</general><scope>IQODW</scope><scope>2B.</scope><scope>4A8</scope><scope>92I</scope><scope>93N</scope><scope>PSX</scope><scope>TCJ</scope></search><sort><creationdate>2008</creationdate><title>Preparation and thermal treatment of Pd/Ag composite membrane on a porous α-alumina tube by sequential electroless plating technique for H2 separation</title><author>NAVAEI ALVAR, E ; REZA GOLMOHAMMADI, M ; REZAEI, M ; NAVAEI ALVAR, H ; MARDANLOO, A ; HABIBZAD NOUHIAN, S ; DIDARI, M</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-p652-e9d7950064d64271c5e4ebe322ccc0dfa4aa33dcf34907d0b1db1bac316e85573</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2008</creationdate><topic>Alternative fuels. Production and utilization</topic><topic>Applied sciences</topic><topic>Energy</topic><topic>Exact sciences and technology</topic><topic>Fuels</topic><topic>Hydrogen</topic><toplevel>online_resources</toplevel><creatorcontrib>NAVAEI ALVAR, E</creatorcontrib><creatorcontrib>REZA GOLMOHAMMADI, M</creatorcontrib><creatorcontrib>REZAEI, M</creatorcontrib><creatorcontrib>NAVAEI ALVAR, H</creatorcontrib><creatorcontrib>MARDANLOO, A</creatorcontrib><creatorcontrib>HABIBZAD NOUHIAN, S</creatorcontrib><creatorcontrib>DIDARI, M</creatorcontrib><collection>Pascal-Francis</collection><collection>Wanfang Data Journals - Hong Kong</collection><collection>WANFANG Data Centre</collection><collection>Wanfang Data Journals</collection><collection>万方数据期刊 - 香港版</collection><collection>China Online Journals (COJ)</collection><collection>China Online Journals (COJ)</collection><jtitle>Journal of natural gas chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>NAVAEI ALVAR, E</au><au>REZA GOLMOHAMMADI, M</au><au>REZAEI, M</au><au>NAVAEI ALVAR, H</au><au>MARDANLOO, A</au><au>HABIBZAD NOUHIAN, S</au><au>DIDARI, M</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Preparation and thermal treatment of Pd/Ag composite membrane on a porous α-alumina tube by sequential electroless plating technique for H2 separation</atitle><jtitle>Journal of natural gas chemistry</jtitle><date>2008</date><risdate>2008</risdate><volume>17</volume><issue>4</issue><spage>321</spage><epage>326</epage><pages>321-326</pages><issn>1003-9953</issn><abstract>TE3; Pd/Ag/α-Al2O3 composite membranes were prepared by sequential electroless plating technique. The prepared membranes were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive spec-troscopy, and inductively coupled plasma atomic emission spectroscopy techniques (ICP-AES). Effects of annealing time, Ag content, and air treatment on the hydrogen permeation flux and morphology of the alloys were investigated. The results of the investigation showed that the prepared type of tube had a good potential as substrate for membrane preparation. In addition, a uniform defect-free alloy was prepared by annealing at 550 ℃ in H2 atmosphere. The permeation results showed an increase in H2 permeation flux by increasing the Ag content and the annealing time. In addition, the air treatment of the prepared membranes at 400 ℃ for 1 h changed the morphology of the alloy and substantially enhanced the hydrogen flux.</abstract><cop>Chengdu</cop><pub>Dalian Institute of Chemical Physics</pub><tpages>6</tpages></addata></record> |
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| ispartof | Journal of natural gas chemistry, 2008, Vol.17 (4), p.321-326 |
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| language | eng |
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| source | ScienceDirect Journals (5 years ago - present) |
| subjects | Alternative fuels. Production and utilization Applied sciences Energy Exact sciences and technology Fuels Hydrogen |
| title | Preparation and thermal treatment of Pd/Ag composite membrane on a porous α-alumina tube by sequential electroless plating technique for H2 separation |
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