由对苯二甲酸和1,3-双(咪唑基-1-甲基)苯构筑的锌配合物的水热合成及晶体结构
O631; 以Zn(NO3)2·6H2O、对苯二甲酸(H2BDC)和1,3-双(咪唑基-1-甲基)苯(mbix)为原料,采用水热法合成了二维网状配位聚合物[Zn(BDC) (mbix)]n(1),并对其进行了元素分析、红外光谱、荧光光谱和X-射线单晶衍射测定.该配合物属于三斜晶系,P-1空间群,a=9.6216(18),b=9.7009(18),c=11.855(2)A,α=108.286(3),β=103.830(3),γ=91.922(3)°,V=1013.1(3)A3,Z=2,Dc=1.533g/cm3,μ=1.250mm-1,F(000)=480,R1=0.0294,wR2=0.070...
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| Veröffentlicht in: | 通化师范学院学报 2015, Vol.36 (2), p.37-84 |
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| container_title | 通化师范学院学报 |
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| creator | 战佩英 李秀梅 潘亚茹 黄艳菊 王志涛 |
| description | O631; 以Zn(NO3)2·6H2O、对苯二甲酸(H2BDC)和1,3-双(咪唑基-1-甲基)苯(mbix)为原料,采用水热法合成了二维网状配位聚合物[Zn(BDC) (mbix)]n(1),并对其进行了元素分析、红外光谱、荧光光谱和X-射线单晶衍射测定.该配合物属于三斜晶系,P-1空间群,a=9.6216(18),b=9.7009(18),c=11.855(2)A,α=108.286(3),β=103.830(3),γ=91.922(3)°,V=1013.1(3)A3,Z=2,Dc=1.533g/cm3,μ=1.250mm-1,F(000)=480,R1=0.0294,wR2=0.0704. |
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| issn | 1008-7974 |
| language | chi |
| recordid | cdi_wanfang_journals_thsfxyxb201502012 |
| source | 国家哲学社会科学学术期刊数据库 (National Social Sciences Database) |
| title | 由对苯二甲酸和1,3-双(咪唑基-1-甲基)苯构筑的锌配合物的水热合成及晶体结构 |
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