1,10-邻菲咯啉取代苷脲与Co(Ⅱ)一维配位聚合物的合成及晶体结构
O625.15; 以1,10-邻菲咯啉取代苷脲为原料,与CoCl2· 6H2O在乙醇溶液中反应,生成了标题化合物井得到其单晶.单晶经X-射线单晶衍射实验表征,化合物单晶为正交晶系,P212121空间群,晶胞参数为:a=11.2115(4)A,b=12.9155(5) A,c=14.2723(6)A,α=β=γ=90°,V=2067.4A3,Z=4,Dc=1.321g·cm-3,μ=0.856mm-1,F(000) =852,R1=0.0443,ωR2=0.0980.配合物分子间通过多种相互作用,形成一维链状结构....
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| Veröffentlicht in: | 兴义民族师范学院学报 2013 (6), p.111-113 |
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| container_title | 兴义民族师范学院学报 |
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| creator | 陈明华 蔡元志 易君明 郑玉国 马培华 |
| description | O625.15; 以1,10-邻菲咯啉取代苷脲为原料,与CoCl2· 6H2O在乙醇溶液中反应,生成了标题化合物井得到其单晶.单晶经X-射线单晶衍射实验表征,化合物单晶为正交晶系,P212121空间群,晶胞参数为:a=11.2115(4)A,b=12.9155(5) A,c=14.2723(6)A,α=β=γ=90°,V=2067.4A3,Z=4,Dc=1.321g·cm-3,μ=0.856mm-1,F(000) =852,R1=0.0443,ωR2=0.0980.配合物分子间通过多种相互作用,形成一维链状结构. |
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| source | 国家哲学社会科学学术期刊数据库 (National Social Sciences Database) |
| title | 1,10-邻菲咯啉取代苷脲与Co(Ⅱ)一维配位聚合物的合成及晶体结构 |
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