Preparation of copper nanoparticles by radiation

Preparation of copper nanoparticles by radiation

Copper nanoparticles were successfully synthesized by 60Co-γ radiation with aqueous solution of cupric sulfate under inert nitrogen-purged conditions. Cu nanoparticles were characterized by using X-ray diffraction （XRD）, transmission electron microscopy （TEM）, laser particle size distribution analyz...

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Veröffentlicht in:核技术（英文版） 2013-12, Vol.24 (6), p.29-35
1. Verfasser: LIU Yajian GUO Xiongbin FU Junj ie TAN Yuanyuan LI Zhaolong ZHOU Xinyao XU Furong
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Sprache:eng
Schlagworte:
储存稳定性
制备
合成条件
差示扫描量热计
辐射
透射电子显微镜
铜纳米粒子
铜纳米颗粒
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creator LIU Yajian GUO Xiongbin FU Junj ie TAN Yuanyuan LI Zhaolong ZHOU Xinyao XU Furong
description Copper nanoparticles were successfully synthesized by 60Co-γ radiation with aqueous solution of cupric sulfate under inert nitrogen-purged conditions. Cu nanoparticles were characterized by using X-ray diffraction （XRD）, transmission electron microscopy （TEM）, laser particle size distribution analyzer （LSPSDA） and differential scanning calorimeter （DSC） techniques, respectively. The effects of solution system, pH, additive of surfactant and absorbed doses on the particle size and its distribution as well as stored stability of Cu naoparticles were investigated. High resolution TEM pictures showed the formation of homogeneous cubic-structured copper nanoparticles with different sizes depends on the synthetic conditions. This new kind of synthesis method shows the excellent stability, which may provide an efficient way to improve the fine tuning of the structure and size of copper nanoparticles.
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subjects 储存稳定性
制备
合成条件
差示扫描量热计
辐射
透射电子显微镜
铜纳米粒子
铜纳米颗粒
title Preparation of copper nanoparticles by radiation
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