co-Condensation Synthesis of Salicylaldimine Calcium Complex Containing Mesoporous Silica Nanoparticles as Carriers for Drug Release
A series of functional mesoporous silica nanoparticles（MSNs） was synthesized by a one-step simple synthesis approach involving co-condensation of tetraethoxysilane（TEOS） and salicylaldimine ligand（Sal-Si） in the presence of cetyltrimethylammonium chloride（CTAC） under basic conditions.The target MSNs...
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| Veröffentlicht in: | Chemical research in Chinese universities 2014-08, Vol.30 (4), p.531-537 |
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| creator | Tang, Duihai Zhang, Weiran Wang, Yifan Miao, Jing Qiao, Zhen’an Huo, Qisheng Zhang, Lirong |
| description | A series of functional mesoporous silica nanoparticles（MSNs） was synthesized by a one-step simple synthesis approach involving co-condensation of tetraethoxysilane（TEOS） and salicylaldimine ligand（Sal-Si） in the presence of cetyltrimethylammonium chloride（CTAC） under basic conditions.The target MSNs with different sizes （50,100 and 200 nm,respectively） were obtained.Furthermore,the Ca^2＋ cations were also introduced into MSNs.The prepared nanoparticles were characterized by means of infrared（IR） spectra,thermogravimetric analysis（TGA）,inductively coupled plasma（ICP）,CHN elemental analysis,nitrogen adsorption-desorption,scanning electron microscope（SEM） and transmission electron microscope（TEM）.Ibuprofen（IBU） which contains carboxyl groups was selected as a model drug.The results of drug loading and release reveal that the loading capacities and release behaviors of the model drug are highly dependent on the Ca^2＋ cations in MSNs.The release of IBU from the MSNs functionalized by Ca^2＋ cations is found to be effectively controlled when compared to the release from the MSNs without the functionalization of Ca^2＋ cations,which is due to the ionic interaction between carboxyl groups in IBU and Ca^2＋ cations in MSNs. |
| doi_str_mv | 10.1007/s40242-014-4097-8 |
| format | Article |
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All Rights Reserved.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c349t-53444fe861f72c73ad8a6348373db82dc2b5abbd698324751bc682d0dd18cc283</citedby><cites>FETCH-LOGICAL-c349t-53444fe861f72c73ad8a6348373db82dc2b5abbd698324751bc682d0dd18cc283</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Uhttp://image.cqvip.com/vip1000/qk/86071X/86071X.jpg</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s40242-014-4097-8$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s40242-014-4097-8$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Tang, Duihai</creatorcontrib><creatorcontrib>Zhang, Weiran</creatorcontrib><creatorcontrib>Wang, Yifan</creatorcontrib><creatorcontrib>Miao, Jing</creatorcontrib><creatorcontrib>Qiao, Zhen’an</creatorcontrib><creatorcontrib>Huo, Qisheng</creatorcontrib><creatorcontrib>Zhang, Lirong</creatorcontrib><title>co-Condensation Synthesis of Salicylaldimine Calcium Complex Containing Mesoporous Silica Nanoparticles as Carriers for Drug Release</title><title>Chemical research in Chinese universities</title><addtitle>Chem. Res. Chin. Univ</addtitle><addtitle>Chemical Research in Chinese University</addtitle><description>A series of functional mesoporous silica nanoparticles（MSNs） was synthesized by a one-step simple synthesis approach involving co-condensation of tetraethoxysilane（TEOS） and salicylaldimine ligand（Sal-Si） in the presence of cetyltrimethylammonium chloride（CTAC） under basic conditions.The target MSNs with different sizes （50,100 and 200 nm,respectively） were obtained.Furthermore,the Ca^2＋ cations were also introduced into MSNs.The prepared nanoparticles were characterized by means of infrared（IR） spectra,thermogravimetric analysis（TGA）,inductively coupled plasma（ICP）,CHN elemental analysis,nitrogen adsorption-desorption,scanning electron microscope（SEM） and transmission electron microscope（TEM）.Ibuprofen（IBU） which contains carboxyl groups was selected as a model drug.The results of drug loading and release reveal that the loading capacities and release behaviors of the model drug are highly dependent on the Ca^2＋ cations in MSNs.The release of IBU from the MSNs functionalized by Ca^2＋ cations is found to be effectively controlled when compared to the release from the MSNs without the functionalization of Ca^2＋ cations,which is due to the ionic interaction between carboxyl groups in IBU and Ca^2＋ cations in MSNs.</description><subject>Analytical Chemistry</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Chemistry/Food Science</subject><subject>Inorganic Chemistry</subject><subject>Organic Chemistry</subject><subject>Physical Chemistry</subject><subject>二氧化</subject><subject>亚胺基</subject><subject>共缩聚</subject><subject>十六烷基三甲基氯化铵</subject><subject>合成方法</subject><subject>水杨醛亚胺</subject><subject>硅纳米颗粒</subject><subject>药物释放</subject><issn>1005-9040</issn><issn>2210-3171</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><recordid>eNp9kU1rGzEQhkVpoU7aH9CbyC0HpfraXe0xbNOmkLRQJ2cxK2nXMmvJkdbUvueHR8ahufU0MLzPvPAMQl8YvWKUNl-zpFxyQpkkkrYNUe_QgnNGiWANe48WJVSRlkr6EZ3lvKZUtHUtF-jZRNLFYF3IMPsY8PIQ5pXLPuM44CVM3hwmmKzf-OBwB5Pxuw3u4mY7uX2ZYQYffBjxvctxG1PcZbz0hQL8C0LcQpq9mVzGkAudkncp4yEm_C3tRvzHTQ6y-4Q-DDBl9_l1nqPH7zcP3S25-_3jZ3d9R4yQ7UwqIaUcnKrZ0HDTCLAKaiGVaITtFbeG9xX0va1bJbhsKtabuqyptUwZw5U4R5enu38hDBBGvY67FEqjHu1-v9of1rwILJIoK1l2ypoUc05u0NvkN5AOmlF9VK5PynUh9FG5Pt7nJyaXbBhdeiv4H3TxWrSKYXwq3L-muua0_FBV4gU7H5G0</recordid><startdate>20140801</startdate><enddate>20140801</enddate><creator>Tang, Duihai</creator><creator>Zhang, Weiran</creator><creator>Wang, Yifan</creator><creator>Miao, Jing</creator><creator>Qiao, Zhen’an</creator><creator>Huo, Qisheng</creator><creator>Zhang, Lirong</creator><general>Jilin University and The Editorial Department of Chemical Research in Chinese Universities</general><general>State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, College of Chemistry,Jilin University, Changchun 130012, P.R.China</general><scope>2RA</scope><scope>92L</scope><scope>CQIGP</scope><scope>~WA</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>2B.</scope><scope>4A8</scope><scope>92I</scope><scope>93N</scope><scope>PSX</scope><scope>TCJ</scope></search><sort><creationdate>20140801</creationdate><title>co-Condensation Synthesis of Salicylaldimine Calcium Complex Containing Mesoporous Silica Nanoparticles as Carriers for Drug Release</title><author>Tang, Duihai ; 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| subjects | Analytical Chemistry Chemistry Chemistry and Materials Science Chemistry/Food Science Inorganic Chemistry Organic Chemistry Physical Chemistry 二氧化 亚胺基 共缩聚 十六烷基三甲基氯化铵 合成方法 水杨醛亚胺 硅纳米颗粒 药物释放 |
| title | co-Condensation Synthesis of Salicylaldimine Calcium Complex Containing Mesoporous Silica Nanoparticles as Carriers for Drug Release |
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