Ionic Liquid-based Microwave-assisted Liquid-liquid Microextraction and High Performance Liquid Chromatography Determination of Sulfonamides from Animal Oils
The authors performed ionic liquid-based microwave-assisted liquid-liquid microextraction（IL-based MALLME） coupled with high performance liquid chromatographic separation for the determination of 6 sulfonamides （SAs） from animal oils. The target analytes were extracted from animal oil samples with s...
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| Veröffentlicht in: | Chemical research in Chinese universities 2013-08, Vol.29 (4), p.647-652 |
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| creator | Feng, Xu-dong Liang, Fang-hui Su, Rui Wu, Li-jie Li, Xue-yuan Wang, Xing-hua Zhang, Han-qi Yu, Ai-min |
| description | The authors performed ionic liquid-based microwave-assisted liquid-liquid microextraction（IL-based MALLME） coupled with high performance liquid chromatographic separation for the determination of 6 sulfonamides （SAs） from animal oils. The target analytes were extracted from animal oil samples with sodium hydroxide solution containing 1-butyl-3-methylimidazolium tetrafluoroborateand as the extraction solvent under microwave irradiation. The experimental parameters of the IL-based MALLME, including types of ILs, volume of IL, amount of ion-pairing agent（NHaPF6）, pH value of sample solution, and extraction temperature and time were evaluated. The limits of detection and quantification obtained were in a range of 0.4--0.5μg/kg and a range of 1.2--1.8μg/kg, respectively. The accuracy of the method was evaluated by analyzing five spiked animal oil samples at two fortified levels（5 and 50μg/kg）, and the recoveries of SAs varied from 81.4% to 114.5% with relative standard deviations ranging from 0.8% to 9.0%. |
| doi_str_mv | 10.1007/s40242-013-2516-x |
| format | Article |
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The target analytes were extracted from animal oil samples with sodium hydroxide solution containing 1-butyl-3-methylimidazolium tetrafluoroborateand as the extraction solvent under microwave irradiation. The experimental parameters of the IL-based MALLME, including types of ILs, volume of IL, amount of ion-pairing agent（NHaPF6）, pH value of sample solution, and extraction temperature and time were evaluated. The limits of detection and quantification obtained were in a range of 0.4--0.5μg/kg and a range of 1.2--1.8μg/kg, respectively. The accuracy of the method was evaluated by analyzing five spiked animal oil samples at two fortified levels（5 and 50μg/kg）, and the recoveries of SAs varied from 81.4% to 114.5% with relative standard deviations ranging from 0.8% to 9.0%.</description><identifier>ISSN: 1005-9040</identifier><identifier>EISSN: 2210-3171</identifier><identifier>DOI: 10.1007/s40242-013-2516-x</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer Berlin Heidelberg</publisher><subject>Analytical Chemistry ; Chemistry ; Chemistry and Materials Science ; Chemistry/Food Science ; Inorganic Chemistry ; Organic Chemistry ; Physical Chemistry ; 分离测定 ; 动物油 ; 微波辅助 ; 氢氧化钠溶液 ; 液相微萃取 ; 磺胺类 ; 离子液体 ; 高效液相色谱法</subject><ispartof>Chemical research in Chinese universities, 2013-08, Vol.29 (4), p.647-652</ispartof><rights>Jilin University, The Editorial Department of Chemical Research in Chinese Universities and Springer-Verlag GmbH 2013</rights><rights>Copyright © Wanfang Data Co. Ltd. All Rights Reserved.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c348t-5543a5d1702e52a9bba0c241e11b9945af896d75b8d452d757bfb769b4880af53</citedby><cites>FETCH-LOGICAL-c348t-5543a5d1702e52a9bba0c241e11b9945af896d75b8d452d757bfb769b4880af53</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Uhttp://image.cqvip.com/vip1000/qk/86071X/86071X.jpg</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s40242-013-2516-x$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s40242-013-2516-x$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Feng, Xu-dong</creatorcontrib><creatorcontrib>Liang, Fang-hui</creatorcontrib><creatorcontrib>Su, Rui</creatorcontrib><creatorcontrib>Wu, Li-jie</creatorcontrib><creatorcontrib>Li, Xue-yuan</creatorcontrib><creatorcontrib>Wang, Xing-hua</creatorcontrib><creatorcontrib>Zhang, Han-qi</creatorcontrib><creatorcontrib>Yu, Ai-min</creatorcontrib><title>Ionic Liquid-based Microwave-assisted Liquid-liquid Microextraction and High Performance Liquid Chromatography Determination of Sulfonamides from Animal Oils</title><title>Chemical research in Chinese universities</title><addtitle>Chem. Res. Chin. Univ</addtitle><addtitle>Chemical Research in Chinese University</addtitle><description>The authors performed ionic liquid-based microwave-assisted liquid-liquid microextraction（IL-based MALLME） coupled with high performance liquid chromatographic separation for the determination of 6 sulfonamides （SAs） from animal oils. The target analytes were extracted from animal oil samples with sodium hydroxide solution containing 1-butyl-3-methylimidazolium tetrafluoroborateand as the extraction solvent under microwave irradiation. The experimental parameters of the IL-based MALLME, including types of ILs, volume of IL, amount of ion-pairing agent（NHaPF6）, pH value of sample solution, and extraction temperature and time were evaluated. The limits of detection and quantification obtained were in a range of 0.4--0.5μg/kg and a range of 1.2--1.8μg/kg, respectively. The accuracy of the method was evaluated by analyzing five spiked animal oil samples at two fortified levels（5 and 50μg/kg）, and the recoveries of SAs varied from 81.4% to 114.5% with relative standard deviations ranging from 0.8% to 9.0%.</description><subject>Analytical Chemistry</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Chemistry/Food Science</subject><subject>Inorganic Chemistry</subject><subject>Organic Chemistry</subject><subject>Physical Chemistry</subject><subject>分离测定</subject><subject>动物油</subject><subject>微波辅助</subject><subject>氢氧化钠溶液</subject><subject>液相微萃取</subject><subject>磺胺类</subject><subject>离子液体</subject><subject>高效液相色谱法</subject><issn>1005-9040</issn><issn>2210-3171</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><recordid>eNp9kc1u3CAUhVHVSJ0mfYDu6LILWsBgm2U0bX6kqVKp7Rpd22AzsiEBT-J5mL5rSTxqd11dBOfjXJ2D0HtGPzFKq89JUC44oawgXLKSLK_QhnNGScEq9hptskgSRQV9g96mtKe0UGUpNuj3bfCuxTv3cHAdaSCZDn9zbQxP8GgIpOTSnK9O7-PLWAVmmSO0swseg-_wjesH_N1EG-IEvjUnBG-HGCaYQx_hfjjiL2Y2cXIeXsBg8Y_DaIOHyXUmYZu1-NK7CUZ858Z0gc4sjMm8O81z9Ovq68_tDdndXd9uL3ekLUQ9EylFAbJjFeVGclBNA7TlghnGGqWEBFursqtkU3dC8nyoGttUpWpEXVOwsjhHH9d_n8Bb8L3eh0P02VH33bIMy3HPc7I5PVpnLVu1OYOUorH6PuaF41Ezqp-70GsXOhP6uQu9ZIavTMpa35v4z-B_0IeT0RB8_5C5v06iVKqUucQ_Wi-boQ</recordid><startdate>20130801</startdate><enddate>20130801</enddate><creator>Feng, Xu-dong</creator><creator>Liang, Fang-hui</creator><creator>Su, Rui</creator><creator>Wu, Li-jie</creator><creator>Li, Xue-yuan</creator><creator>Wang, Xing-hua</creator><creator>Zhang, Han-qi</creator><creator>Yu, Ai-min</creator><general>Springer Berlin Heidelberg</general><general>College of Chemistry, Jilin University, Changchun 130012, P.R.China%Department of Pharmacy, Changchun Medical College, Changchun 130117, P.R.China</general><scope>2RA</scope><scope>92L</scope><scope>CQIGP</scope><scope>~WA</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>2B.</scope><scope>4A8</scope><scope>92I</scope><scope>93N</scope><scope>PSX</scope><scope>TCJ</scope></search><sort><creationdate>20130801</creationdate><title>Ionic Liquid-based Microwave-assisted Liquid-liquid Microextraction and High Performance Liquid Chromatography Determination of Sulfonamides from Animal Oils</title><author>Feng, Xu-dong ; Liang, Fang-hui ; Su, Rui ; Wu, Li-jie ; Li, Xue-yuan ; Wang, Xing-hua ; Zhang, Han-qi ; Yu, Ai-min</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c348t-5543a5d1702e52a9bba0c241e11b9945af896d75b8d452d757bfb769b4880af53</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2013</creationdate><topic>Analytical Chemistry</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Chemistry/Food Science</topic><topic>Inorganic Chemistry</topic><topic>Organic Chemistry</topic><topic>Physical Chemistry</topic><topic>分离测定</topic><topic>动物油</topic><topic>微波辅助</topic><topic>氢氧化钠溶液</topic><topic>液相微萃取</topic><topic>磺胺类</topic><topic>离子液体</topic><topic>高效液相色谱法</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Feng, Xu-dong</creatorcontrib><creatorcontrib>Liang, Fang-hui</creatorcontrib><creatorcontrib>Su, Rui</creatorcontrib><creatorcontrib>Wu, Li-jie</creatorcontrib><creatorcontrib>Li, Xue-yuan</creatorcontrib><creatorcontrib>Wang, Xing-hua</creatorcontrib><creatorcontrib>Zhang, Han-qi</creatorcontrib><creatorcontrib>Yu, Ai-min</creatorcontrib><collection>中文科技期刊数据库</collection><collection>中文科技期刊数据库-CALIS站点</collection><collection>中文科技期刊数据库-7.0平台</collection><collection>中文科技期刊数据库- 镜像站点</collection><collection>CrossRef</collection><collection>Wanfang Data Journals - Hong Kong</collection><collection>WANFANG Data Centre</collection><collection>Wanfang Data Journals</collection><collection>万方数据期刊 - 香港版</collection><collection>China Online Journals (COJ)</collection><collection>China Online Journals (COJ)</collection><jtitle>Chemical research in Chinese universities</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Feng, Xu-dong</au><au>Liang, Fang-hui</au><au>Su, Rui</au><au>Wu, Li-jie</au><au>Li, Xue-yuan</au><au>Wang, Xing-hua</au><au>Zhang, Han-qi</au><au>Yu, Ai-min</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Ionic Liquid-based Microwave-assisted Liquid-liquid Microextraction and High Performance Liquid Chromatography Determination of Sulfonamides from Animal Oils</atitle><jtitle>Chemical research in Chinese universities</jtitle><stitle>Chem. 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The limits of detection and quantification obtained were in a range of 0.4--0.5μg/kg and a range of 1.2--1.8μg/kg, respectively. The accuracy of the method was evaluated by analyzing five spiked animal oil samples at two fortified levels（5 and 50μg/kg）, and the recoveries of SAs varied from 81.4% to 114.5% with relative standard deviations ranging from 0.8% to 9.0%.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><doi>10.1007/s40242-013-2516-x</doi><tpages>6</tpages></addata></record> |
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| subjects | Analytical Chemistry Chemistry Chemistry and Materials Science Chemistry/Food Science Inorganic Chemistry Organic Chemistry Physical Chemistry 分离测定 动物油 微波辅助 氢氧化钠溶液 液相微萃取 磺胺类 离子液体 高效液相色谱法 |
| title | Ionic Liquid-based Microwave-assisted Liquid-liquid Microextraction and High Performance Liquid Chromatography Determination of Sulfonamides from Animal Oils |
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