Innovative method for boron extraction from iron ore containing boron

A novel process for boron enrichment and extraction from ludwigite based on iron nugget technology was proposed. The key steps of this novel process, which include boron and iron separation, crystallization of boron-rich slag, and elucidation of the boron extraction be- havior of boron-rich slag by...

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Veröffentlicht in:International journal of minerals, metallurgy and materials metallurgy and materials, 2016-03, Vol.23 (3), p.247-256
Hauptverfasser: Wang, Guang, Wang, Jing-song, Yu, Xin-yun, Shen, Ying-feng, Zuo, Hai-bin, Xue, Qing-guo
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container_title International journal of minerals, metallurgy and materials
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creator Wang, Guang
Wang, Jing-song
Yu, Xin-yun
Shen, Ying-feng
Zuo, Hai-bin
Xue, Qing-guo
description A novel process for boron enrichment and extraction from ludwigite based on iron nugget technology was proposed. The key steps of this novel process, which include boron and iron separation, crystallization of boron-rich slag, and elucidation of the boron extraction be- havior of boron-rich slag by acid leaching, were performed at the laboratory. The results indicated that 95.7% of the total boron could be en- riched into the slag phase, thereby forming a boron-rich slag during the iron and slag melting separation process. Suanite and kotoite were observed to be the boron-containing crystalline phases, and the boron extraction properties of the boron-rich slag depended on the amounts and grain sizes of these minerals. When the boron-rich slag was slowly cooled to 1100℃, the slag crystallized well and the efficiency of ex- traction of boron (EEB) of the slag was the highest observed in the present study. The boron extraction property of the slow-cooled bo- ron-rich slag obtained in this study was much better than that of szaibelyite ore under the conditions of 80% of theoretical sulfuric acid amount, leaching time of 30 min, leaching temperature of 40℃ ,and liquid-to-solid ratio of 8 mL/g.
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The key steps of this novel process, which include boron and iron separation, crystallization of boron-rich slag, and elucidation of the boron extraction be- havior of boron-rich slag by acid leaching, were performed at the laboratory. The results indicated that 95.7% of the total boron could be en- riched into the slag phase, thereby forming a boron-rich slag during the iron and slag melting separation process. Suanite and kotoite were observed to be the boron-containing crystalline phases, and the boron extraction properties of the boron-rich slag depended on the amounts and grain sizes of these minerals. When the boron-rich slag was slowly cooled to 1100℃, the slag crystallized well and the efficiency of ex- traction of boron (EEB) of the slag was the highest observed in the present study. The boron extraction property of the slow-cooled bo- ron-rich slag obtained in this study was much better than that of szaibelyite ore under the conditions of 80% of theoretical sulfuric acid amount, leaching time of 30 min, leaching temperature of 40℃ ,and liquid-to-solid ratio of 8 mL/g.</description><identifier>ISSN: 1674-4799</identifier><identifier>EISSN: 1869-103X</identifier><identifier>DOI: 10.1007/s12613-016-1233-0</identifier><language>eng</language><publisher>Beijing: University of Science and Technology Beijing</publisher><subject>Boron ; Ceramics ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Composites ; Corrosion and Coatings ; Crystallization ; Glass ; Grain size ; Iron ; Iron ores ; Leaching ; Ludwigite ; Materials Science ; Metallic Materials ; Natural Materials ; Separation ; Slag ; Sulfuric acid ; Surfaces and Interfaces ; Thin Films ; Tribology ; 分离过程 ; 创新方法 ; 富硼渣 ; 提取 ; 浸出行为 ; 硼铁矿 ; 结晶相 ; 萃取性能</subject><ispartof>International journal of minerals, metallurgy and materials, 2016-03, Vol.23 (3), p.247-256</ispartof><rights>University of Science and Technology Beijing and Springer-Verlag Berlin Heidelberg 2016</rights><rights>University of Science and Technology Beijing and Springer-Verlag Berlin Heidelberg 2016.</rights><rights>Copyright © Wanfang Data Co. 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The key steps of this novel process, which include boron and iron separation, crystallization of boron-rich slag, and elucidation of the boron extraction be- havior of boron-rich slag by acid leaching, were performed at the laboratory. The results indicated that 95.7% of the total boron could be en- riched into the slag phase, thereby forming a boron-rich slag during the iron and slag melting separation process. Suanite and kotoite were observed to be the boron-containing crystalline phases, and the boron extraction properties of the boron-rich slag depended on the amounts and grain sizes of these minerals. When the boron-rich slag was slowly cooled to 1100℃, the slag crystallized well and the efficiency of ex- traction of boron (EEB) of the slag was the highest observed in the present study. 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The key steps of this novel process, which include boron and iron separation, crystallization of boron-rich slag, and elucidation of the boron extraction be- havior of boron-rich slag by acid leaching, were performed at the laboratory. The results indicated that 95.7% of the total boron could be en- riched into the slag phase, thereby forming a boron-rich slag during the iron and slag melting separation process. Suanite and kotoite were observed to be the boron-containing crystalline phases, and the boron extraction properties of the boron-rich slag depended on the amounts and grain sizes of these minerals. When the boron-rich slag was slowly cooled to 1100℃, the slag crystallized well and the efficiency of ex- traction of boron (EEB) of the slag was the highest observed in the present study. The boron extraction property of the slow-cooled bo- ron-rich slag obtained in this study was much better than that of szaibelyite ore under the conditions of 80% of theoretical sulfuric acid amount, leaching time of 30 min, leaching temperature of 40℃ ,and liquid-to-solid ratio of 8 mL/g.</abstract><cop>Beijing</cop><pub>University of Science and Technology Beijing</pub><doi>10.1007/s12613-016-1233-0</doi><tpages>10</tpages></addata></record>
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identifier ISSN: 1674-4799
ispartof International journal of minerals, metallurgy and materials, 2016-03, Vol.23 (3), p.247-256
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language eng
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source ProQuest Central UK/Ireland; Alma/SFX Local Collection; SpringerLink Journals - AutoHoldings; ProQuest Central
subjects Boron
Ceramics
Characterization and Evaluation of Materials
Chemistry and Materials Science
Composites
Corrosion and Coatings
Crystallization
Glass
Grain size
Iron
Iron ores
Leaching
Ludwigite
Materials Science
Metallic Materials
Natural Materials
Separation
Slag
Sulfuric acid
Surfaces and Interfaces
Thin Films
Tribology
分离过程
创新方法
富硼渣
提取
浸出行为
硼铁矿
结晶相
萃取性能
title Innovative method for boron extraction from iron ore containing boron
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