In situ synthesis of Fe-based alloy clad coatings containing TiB2–TiN–(h-BN)

Fe-based alloy coatings containing TiB 2 –TiN–(h-BN) were synthesized in situ on Q235 steel substrates by a plasma cladding process using the powders of Fe901 alloy, Ti, and h-BN as raw materials. The effects of Ti/h-BN mass ratio on interfacial bonds between the coating and substrate along with the...

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Veröffentlicht in:International journal of minerals, metallurgy and materials metallurgy and materials, 2015-06, Vol.22 (6), p.613-619
Hauptverfasser: Jiang, Shao-qun, Wang, Gang, Ren, Qing-wen, Yang, Chuan-duo, Wang, Ze-hua, Zhou, Ze-hua
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container_issue 6
container_start_page 613
container_title International journal of minerals, metallurgy and materials
container_volume 22
creator Jiang, Shao-qun
Wang, Gang
Ren, Qing-wen
Yang, Chuan-duo
Wang, Ze-hua
Zhou, Ze-hua
description Fe-based alloy coatings containing TiB 2 –TiN–(h-BN) were synthesized in situ on Q235 steel substrates by a plasma cladding process using the powders of Fe901 alloy, Ti, and h-BN as raw materials. The effects of Ti/h-BN mass ratio on interfacial bonds between the coating and substrate along with the microstructures and microhardnesses of the coatings were investigated. The results show that the Ti/h-BN mass ratio is a vital factor in the formation of the coatings. Free h-BN can be introduced into the coatings by adding an excess amount of h-BN into the precursor. Decreases in the Ti/h-BN mass ratio improve the microstructural uniformity and compactness and enhance the interfacial bonds of the coatings. At a Ti/h-BN mass ratio of 10/20, the coating is free of cracks and micropores, and mainly consists of Fe-Cr, Fe 3 B, TiB 2 , TiN, Ti 2 N, TiB, FeN, FeB, Fe 2 B, and h-BN phases. Its average microhardness in the zone between 0.1–2.8 mm from the coating surface is about Hv 0.2 551.5.
doi_str_mv 10.1007/s12613-015-1114-y
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The effects of Ti/h-BN mass ratio on interfacial bonds between the coating and substrate along with the microstructures and microhardnesses of the coatings were investigated. The results show that the Ti/h-BN mass ratio is a vital factor in the formation of the coatings. Free h-BN can be introduced into the coatings by adding an excess amount of h-BN into the precursor. Decreases in the Ti/h-BN mass ratio improve the microstructural uniformity and compactness and enhance the interfacial bonds of the coatings. At a Ti/h-BN mass ratio of 10/20, the coating is free of cracks and micropores, and mainly consists of Fe-Cr, Fe 3 B, TiB 2 , TiN, Ti 2 N, TiB, FeN, FeB, Fe 2 B, and h-BN phases. 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The effects of Ti/h-BN mass ratio on interfacial bonds between the coating and substrate along with the microstructures and microhardnesses of the coatings were investigated. The results show that the Ti/h-BN mass ratio is a vital factor in the formation of the coatings. Free h-BN can be introduced into the coatings by adding an excess amount of h-BN into the precursor. Decreases in the Ti/h-BN mass ratio improve the microstructural uniformity and compactness and enhance the interfacial bonds of the coatings. At a Ti/h-BN mass ratio of 10/20, the coating is free of cracks and micropores, and mainly consists of Fe-Cr, Fe 3 B, TiB 2 , TiN, Ti 2 N, TiB, FeN, FeB, Fe 2 B, and h-BN phases. 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The effects of Ti/h-BN mass ratio on interfacial bonds between the coating and substrate along with the microstructures and microhardnesses of the coatings were investigated. The results show that the Ti/h-BN mass ratio is a vital factor in the formation of the coatings. Free h-BN can be introduced into the coatings by adding an excess amount of h-BN into the precursor. Decreases in the Ti/h-BN mass ratio improve the microstructural uniformity and compactness and enhance the interfacial bonds of the coatings. At a Ti/h-BN mass ratio of 10/20, the coating is free of cracks and micropores, and mainly consists of Fe-Cr, Fe 3 B, TiB 2 , TiN, Ti 2 N, TiB, FeN, FeB, Fe 2 B, and h-BN phases. Its average microhardness in the zone between 0.1–2.8 mm from the coating surface is about Hv 0.2 551.5.</abstract><cop>Beijing</cop><pub>University of Science and Technology Beijing</pub><doi>10.1007/s12613-015-1114-y</doi><tpages>7</tpages></addata></record>
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subjects Ceramics
Characterization and Evaluation of Materials
Chemistry and Materials Science
Coatings
Composites
Corrosion and Coatings
Ferrous alloys
Glass
Iron alloys
Killed steels
Materials Science
Metallic Materials
Microhardness
Microstructure
Natural Materials
Raw materials
Structural steels
Substrates
Surfaces and Interfaces
Thin Films
Titanium diboride
Titanium nitride
Tribology
title In situ synthesis of Fe-based alloy clad coatings containing TiB2–TiN–(h-BN)
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