Additive effects on tin electrodepositing in acid sulfate electrolytes
The effects of additives on the stannous reduction of an acid sulfate bath were investigated using cyclic and linear sweep voltammetry, electrochemical impedance spectroscopy （EIS）, and microstructure analysis. In the absence of additives, tin coatings are rough, and the tin electrodepositing is a s...
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| Veröffentlicht in: | International journal of minerals, metallurgy and materials metallurgy and materials, 2013-05, Vol.20 (5), p.472-478 |
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| container_title | International journal of minerals, metallurgy and materials |
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| creator | Xiao, Fa-xin Shen, Xiao-ni Ren, Feng-zhang Volinsky, Alex A. |
| description | The effects of additives on the stannous reduction of an acid sulfate bath were investigated using cyclic and linear sweep voltammetry, electrochemical impedance spectroscopy （EIS）, and microstructure analysis. In the absence of additives, tin coatings are rough, and the tin electrodepositing is a single-step reduction process accompanied by hydrogen gas evolution. The addition of tartaric acid produces a slight reduction in the peak current of stannous reduction and has an appreciably positive effect on the stability of the acidic tin bath. Both benzylidene acetone and polyoxyethylene octylphenol ether hinder the stannous reduction and greatly suppress the hydrogen gas evolution. Formaldehyde slightly decreases the peak current density of stannous reduction and serves as an auxiliary brightener in the acid sulfate bath. The presence of mixed additives greatly suppresses the stannous reduction and hydrogen gas evolution and consequently produces a significantly smoother and denser tin coating. The （112） crystal face is found to be the dominant and preferred orientation of tin deposits. |
| doi_str_mv | 10.1007/s12613-013-0753-0 |
| format | Article |
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In the absence of additives, tin coatings are rough, and the tin electrodepositing is a single-step reduction process accompanied by hydrogen gas evolution. The addition of tartaric acid produces a slight reduction in the peak current of stannous reduction and has an appreciably positive effect on the stability of the acidic tin bath. Both benzylidene acetone and polyoxyethylene octylphenol ether hinder the stannous reduction and greatly suppress the hydrogen gas evolution. Formaldehyde slightly decreases the peak current density of stannous reduction and serves as an auxiliary brightener in the acid sulfate bath. The presence of mixed additives greatly suppresses the stannous reduction and hydrogen gas evolution and consequently produces a significantly smoother and denser tin coating. The （112） crystal face is found to be the dominant and preferred orientation of tin deposits.</description><identifier>ISSN: 1674-4799</identifier><identifier>EISSN: 1869-103X</identifier><identifier>DOI: 10.1007/s12613-013-0753-0</identifier><language>eng</language><publisher>Beijing: University of Science and Technology Beijing</publisher><subject>Acids ; Additives ; Ceramics ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Coatings ; Composites ; Corrosion and Coatings ; Current density ; Electrochemical impedance spectroscopy ; Electrochemistry ; Electrolytes ; Gas evolution ; Glass ; Hydrogen ; Materials Science ; Metallic Materials ; Natural Materials ; Polyoxyethylene ; Preferred orientation ; Reduction ; Sulfates ; Surfaces and Interfaces ; Tartaric acid ; Thin Films ; Tin ; Tribology ; 加性效应 ; 峰电流密度 ; 混合添加剂 ; 电解质 ; 硫酸亚锡 ; 线性扫描伏安法 ; 辛基酚聚氧乙烯醚 ; 酸性硫酸盐</subject><ispartof>International journal of minerals, metallurgy and materials, 2013-05, Vol.20 (5), p.472-478</ispartof><rights>University of Science and Technology Beijing and Springer-Verlag Berlin Heidelberg 2013</rights><rights>University of Science and Technology Beijing and Springer-Verlag Berlin Heidelberg 2013.</rights><rights>Copyright © Wanfang Data Co. 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All Rights Reserved.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c477t-8fcea41ad1adc4c11131de765760d139e2a1fe354c73e41ce0acc9ee708218283</citedby><cites>FETCH-LOGICAL-c477t-8fcea41ad1adc4c11131de765760d139e2a1fe354c73e41ce0acc9ee708218283</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Uhttp://image.cqvip.com/vip1000/qk/85313A/85313A.jpg</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s12613-013-0753-0$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://www.proquest.com/docview/2919491647?pq-origsite=primo$$EHTML$$P50$$Gproquest$$H</linktohtml><link.rule.ids>314,780,784,21388,27924,27925,33744,33745,41488,42557,43805,51319,64385,64387,64389,72469</link.rule.ids></links><search><creatorcontrib>Xiao, Fa-xin</creatorcontrib><creatorcontrib>Shen, Xiao-ni</creatorcontrib><creatorcontrib>Ren, Feng-zhang</creatorcontrib><creatorcontrib>Volinsky, Alex A.</creatorcontrib><title>Additive effects on tin electrodepositing in acid sulfate electrolytes</title><title>International journal of minerals, metallurgy and materials</title><addtitle>Int J Miner Metall Mater</addtitle><addtitle>International Journal of Minerals,Metallurgy and Materials</addtitle><description>The effects of additives on the stannous reduction of an acid sulfate bath were investigated using cyclic and linear sweep voltammetry, electrochemical impedance spectroscopy （EIS）, and microstructure analysis. In the absence of additives, tin coatings are rough, and the tin electrodepositing is a single-step reduction process accompanied by hydrogen gas evolution. The addition of tartaric acid produces a slight reduction in the peak current of stannous reduction and has an appreciably positive effect on the stability of the acidic tin bath. Both benzylidene acetone and polyoxyethylene octylphenol ether hinder the stannous reduction and greatly suppress the hydrogen gas evolution. Formaldehyde slightly decreases the peak current density of stannous reduction and serves as an auxiliary brightener in the acid sulfate bath. The presence of mixed additives greatly suppresses the stannous reduction and hydrogen gas evolution and consequently produces a significantly smoother and denser tin coating. The （112） crystal face is found to be the dominant and preferred orientation of tin deposits.</description><subject>Acids</subject><subject>Additives</subject><subject>Ceramics</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Coatings</subject><subject>Composites</subject><subject>Corrosion and Coatings</subject><subject>Current density</subject><subject>Electrochemical impedance spectroscopy</subject><subject>Electrochemistry</subject><subject>Electrolytes</subject><subject>Gas evolution</subject><subject>Glass</subject><subject>Hydrogen</subject><subject>Materials Science</subject><subject>Metallic Materials</subject><subject>Natural Materials</subject><subject>Polyoxyethylene</subject><subject>Preferred orientation</subject><subject>Reduction</subject><subject>Sulfates</subject><subject>Surfaces and Interfaces</subject><subject>Tartaric acid</subject><subject>Thin Films</subject><subject>Tin</subject><subject>Tribology</subject><subject>加性效应</subject><subject>峰电流密度</subject><subject>混合添加剂</subject><subject>电解质</subject><subject>硫酸亚锡</subject><subject>线性扫描伏安法</subject><subject>辛基酚聚氧乙烯醚</subject><subject>酸性硫酸盐</subject><issn>1674-4799</issn><issn>1869-103X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNp9kV1LwzAUhoMoOKc_wLuKN4JUc9o0aS6HOBUG3ih4F7L0tLZ26dZ0uv17UzoneCHk5Os85yN5CTkHegOUilsHEYc4pL2JxE8HZAQplyHQ-O3Q77lgIRNSHpMT5ypKuRBUjMh0kmVlV35igHmOpnNBY4OutAHW_tQ2GS4b5wFbBP5SmzIL3LrOdYc_RL3t0J2So1zXDs9265i8Tu9f7h7D2fPD091kFhomRBemuUHNQGd-GGYAIIYMBU8EpxnEEiMNOcYJMyJGBgapNkYiCppGkEZpPCbXQ94vbXNtC1U169b6impefVTZZjNXGPlPoAn1Dx-Tq4Fets1qja5Ti9IZrGttsVk7BSySqeQSpEcv_6D7zJH3MwmcCU_BQJm2ca7FXC3bcqHbrQKqeh3UoIOivXkdVN9ENMQ4z9oC29_M_wVd7Aq9N7ZY-bh9JZakHHzX8TdoxZVm</recordid><startdate>20130501</startdate><enddate>20130501</enddate><creator>Xiao, Fa-xin</creator><creator>Shen, Xiao-ni</creator><creator>Ren, Feng-zhang</creator><creator>Volinsky, Alex A.</creator><general>University of Science and Technology Beijing</general><general>Springer Nature B.V</general><general>School of Materials Science and Engineering, Henan University of Science and Technology, Luoyang 471003, China%Department of Mechanical Engineering, University of South Florida, Tampa FL 33620, USA</general><scope>2RA</scope><scope>92L</scope><scope>CQIGP</scope><scope>W92</scope><scope>~WA</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>BHPHI</scope><scope>BKSAR</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>PCBAR</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>2B.</scope><scope>4A8</scope><scope>92I</scope><scope>93N</scope><scope>PSX</scope><scope>TCJ</scope></search><sort><creationdate>20130501</creationdate><title>Additive effects on tin electrodepositing in acid sulfate electrolytes</title><author>Xiao, Fa-xin ; Shen, Xiao-ni ; Ren, Feng-zhang ; Volinsky, Alex A.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c477t-8fcea41ad1adc4c11131de765760d139e2a1fe354c73e41ce0acc9ee708218283</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2013</creationdate><topic>Acids</topic><topic>Additives</topic><topic>Ceramics</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Coatings</topic><topic>Composites</topic><topic>Corrosion and Coatings</topic><topic>Current density</topic><topic>Electrochemical impedance spectroscopy</topic><topic>Electrochemistry</topic><topic>Electrolytes</topic><topic>Gas evolution</topic><topic>Glass</topic><topic>Hydrogen</topic><topic>Materials Science</topic><topic>Metallic Materials</topic><topic>Natural Materials</topic><topic>Polyoxyethylene</topic><topic>Preferred orientation</topic><topic>Reduction</topic><topic>Sulfates</topic><topic>Surfaces and Interfaces</topic><topic>Tartaric acid</topic><topic>Thin Films</topic><topic>Tin</topic><topic>Tribology</topic><topic>加性效应</topic><topic>峰电流密度</topic><topic>混合添加剂</topic><topic>电解质</topic><topic>硫酸亚锡</topic><topic>线性扫描伏安法</topic><topic>辛基酚聚氧乙烯醚</topic><topic>酸性硫酸盐</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Xiao, Fa-xin</creatorcontrib><creatorcontrib>Shen, Xiao-ni</creatorcontrib><creatorcontrib>Ren, Feng-zhang</creatorcontrib><creatorcontrib>Volinsky, Alex A.</creatorcontrib><collection>中文科技期刊数据库</collection><collection>中文科技期刊数据库-CALIS站点</collection><collection>中文科技期刊数据库-7.0平台</collection><collection>中文科技期刊数据库-工程技术</collection><collection>中文科技期刊数据库- 镜像站点</collection><collection>CrossRef</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>Natural Science Collection</collection><collection>Earth, Atmospheric & Aquatic Science Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Science Database</collection><collection>Earth, Atmospheric & Aquatic Science Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Wanfang Data Journals - Hong Kong</collection><collection>WANFANG Data Centre</collection><collection>Wanfang Data Journals</collection><collection>万方数据期刊 - 香港版</collection><collection>China Online Journals (COJ)</collection><collection>China Online Journals (COJ)</collection><jtitle>International journal of minerals, metallurgy and materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Xiao, Fa-xin</au><au>Shen, Xiao-ni</au><au>Ren, Feng-zhang</au><au>Volinsky, Alex A.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Additive effects on tin electrodepositing in acid sulfate electrolytes</atitle><jtitle>International journal of minerals, metallurgy and materials</jtitle><stitle>Int J Miner Metall Mater</stitle><addtitle>International Journal of Minerals,Metallurgy and Materials</addtitle><date>2013-05-01</date><risdate>2013</risdate><volume>20</volume><issue>5</issue><spage>472</spage><epage>478</epage><pages>472-478</pages><issn>1674-4799</issn><eissn>1869-103X</eissn><abstract>The effects of additives on the stannous reduction of an acid sulfate bath were investigated using cyclic and linear sweep voltammetry, electrochemical impedance spectroscopy （EIS）, and microstructure analysis. In the absence of additives, tin coatings are rough, and the tin electrodepositing is a single-step reduction process accompanied by hydrogen gas evolution. The addition of tartaric acid produces a slight reduction in the peak current of stannous reduction and has an appreciably positive effect on the stability of the acidic tin bath. Both benzylidene acetone and polyoxyethylene octylphenol ether hinder the stannous reduction and greatly suppress the hydrogen gas evolution. Formaldehyde slightly decreases the peak current density of stannous reduction and serves as an auxiliary brightener in the acid sulfate bath. The presence of mixed additives greatly suppresses the stannous reduction and hydrogen gas evolution and consequently produces a significantly smoother and denser tin coating. The （112） crystal face is found to be the dominant and preferred orientation of tin deposits.</abstract><cop>Beijing</cop><pub>University of Science and Technology Beijing</pub><doi>10.1007/s12613-013-0753-0</doi><tpages>7</tpages></addata></record> |
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| ispartof | International journal of minerals, metallurgy and materials, 2013-05, Vol.20 (5), p.472-478 |
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| subjects | Acids Additives Ceramics Characterization and Evaluation of Materials Chemistry and Materials Science Coatings Composites Corrosion and Coatings Current density Electrochemical impedance spectroscopy Electrochemistry Electrolytes Gas evolution Glass Hydrogen Materials Science Metallic Materials Natural Materials Polyoxyethylene Preferred orientation Reduction Sulfates Surfaces and Interfaces Tartaric acid Thin Films Tin Tribology 加性效应 峰电流密度 混合添加剂 电解质 硫酸亚锡 线性扫描伏安法 辛基酚聚氧乙烯醚 酸性硫酸盐 |
| title | Additive effects on tin electrodepositing in acid sulfate electrolytes |
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