Synthesis of LiNiO2 by two-step solid-state method
LiNiO2 was prepared through two-step solid-state reaction by mechanochemical method and heat treatment, using LiOH (Li2CO3) and Ni(OH)2 as starting materials. The influence of grinding speed and time, heat treatment time, and starting materials on the structure of LiNiO2 was studied. The as-milled s...
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| Veröffentlicht in: | Materials science--Poland 2018-03, Vol.36 (1), p.107-111 |
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| creator | Li, Shuiping Wu, Qisheng Zhang, Chun Zhu, Huajun Zhang, Changsen Wang, Xin Kong, Cancan |
| description | LiNiO2 was prepared through two-step solid-state reaction by mechanochemical method and heat treatment, using LiOH (Li2CO3) and Ni(OH)2 as starting materials. The influence of grinding speed and time, heat treatment time, and starting materials on the structure of LiNiO2 was studied. The as-milled samples and products were characterized by scanning electron microscope (SEM) and X-ray diffraction (XRD). The results show that uniform as-milled samples can be obtained at grinding speed of 580 rpm for 0.5 h, using LiOH and Ni(OH)2 as raw materials. Perfect crystal LiNiO2 has been prepared by calcining the as-milled samples at 700 °C for 15 h. Composite material powders consisting of Li2Ni8O10 and LiNiO2 have been obtained using Li2CO3 as lithium source. |
| doi_str_mv | 10.1515/msp-2018-0015 |
| format | Article |
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The influence of grinding speed and time, heat treatment time, and starting materials on the structure of LiNiO2 was studied. The as-milled samples and products were characterized by scanning electron microscope (SEM) and X-ray diffraction (XRD). The results show that uniform as-milled samples can be obtained at grinding speed of 580 rpm for 0.5 h, using LiOH and Ni(OH)2 as raw materials. Perfect crystal LiNiO2 has been prepared by calcining the as-milled samples at 700 °C for 15 h. Composite material powders consisting of Li2Ni8O10 and LiNiO2 have been obtained using Li2CO3 as lithium source.</description><identifier>EISSN: 2083-134X</identifier><identifier>DOI: 10.1515/msp-2018-0015</identifier><language>eng</language><publisher>De Gruyter Open</publisher><subject>grinding ; lithium ; mechanochemistry ; solid-state method</subject><ispartof>Materials science--Poland, 2018-03, Vol.36 (1), p.107-111</ispartof><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.degruyter.com/document/doi/10.1515/msp-2018-0015/pdf$$EPDF$$P50$$Gwalterdegruyter$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://www.degruyter.com/document/doi/10.1515/msp-2018-0015/html$$EHTML$$P50$$Gwalterdegruyter$$Hfree_for_read</linktohtml><link.rule.ids>314,780,784,27924,27925,67158,68942</link.rule.ids></links><search><creatorcontrib>Li, Shuiping</creatorcontrib><creatorcontrib>Wu, Qisheng</creatorcontrib><creatorcontrib>Zhang, Chun</creatorcontrib><creatorcontrib>Zhu, Huajun</creatorcontrib><creatorcontrib>Zhang, Changsen</creatorcontrib><creatorcontrib>Wang, Xin</creatorcontrib><creatorcontrib>Kong, Cancan</creatorcontrib><title>Synthesis of LiNiO2 by two-step solid-state method</title><title>Materials science--Poland</title><description>LiNiO2 was prepared through two-step solid-state reaction by mechanochemical method and heat treatment, using LiOH (Li2CO3) and Ni(OH)2 as starting materials. The influence of grinding speed and time, heat treatment time, and starting materials on the structure of LiNiO2 was studied. The as-milled samples and products were characterized by scanning electron microscope (SEM) and X-ray diffraction (XRD). The results show that uniform as-milled samples can be obtained at grinding speed of 580 rpm for 0.5 h, using LiOH and Ni(OH)2 as raw materials. Perfect crystal LiNiO2 has been prepared by calcining the as-milled samples at 700 °C for 15 h. Composite material powders consisting of Li2Ni8O10 and LiNiO2 have been obtained using Li2CO3 as lithium source.</description><subject>grinding</subject><subject>lithium</subject><subject>mechanochemistry</subject><subject>solid-state method</subject><issn>2083-134X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2018</creationdate><recordtype>article</recordtype><sourceid/><recordid>eNotj8tqwzAQRUWh0JBm2b1-QO2Mxq_QVQl9gWkWbaE7IUvjxsaJg6UQ_Pe1ae7mntW9HCHuEO4xxfRhH45KAxYKANMrsdBQkEJKfm7EKoQWpmRFCgkuhP4cD3HHoQmyr2XZfDRbLatRxnOvQuSjDH3X-AltZLnnuOv9rbiubRd4deml-H55_tq8qXL7-r55KlVLqKOq16xzdFChB-9q8OySzK8rJEjzjDHznOWp5oQKslC7yvuCanLkicE6S0vx-L97tl3kwfPvcBonMG1_Gg7Ts0Ews6-ZfM3sa2ZfyhAhpz_IvkzZ</recordid><startdate>20180301</startdate><enddate>20180301</enddate><creator>Li, Shuiping</creator><creator>Wu, Qisheng</creator><creator>Zhang, Chun</creator><creator>Zhu, Huajun</creator><creator>Zhang, Changsen</creator><creator>Wang, Xin</creator><creator>Kong, Cancan</creator><general>De Gruyter Open</general><scope/></search><sort><creationdate>20180301</creationdate><title>Synthesis of LiNiO2 by two-step solid-state method</title><author>Li, Shuiping ; Wu, Qisheng ; Zhang, Chun ; Zhu, Huajun ; Zhang, Changsen ; Wang, Xin ; Kong, Cancan</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-j312t-f9e271c0b1d0dcf0dec46d9b130576e16de6752e4383a0fcbdd83f3c3d3e0aca3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2018</creationdate><topic>grinding</topic><topic>lithium</topic><topic>mechanochemistry</topic><topic>solid-state method</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Li, Shuiping</creatorcontrib><creatorcontrib>Wu, Qisheng</creatorcontrib><creatorcontrib>Zhang, Chun</creatorcontrib><creatorcontrib>Zhu, Huajun</creatorcontrib><creatorcontrib>Zhang, Changsen</creatorcontrib><creatorcontrib>Wang, Xin</creatorcontrib><creatorcontrib>Kong, Cancan</creatorcontrib><jtitle>Materials science--Poland</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Li, Shuiping</au><au>Wu, Qisheng</au><au>Zhang, Chun</au><au>Zhu, Huajun</au><au>Zhang, Changsen</au><au>Wang, Xin</au><au>Kong, Cancan</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of LiNiO2 by two-step solid-state method</atitle><jtitle>Materials science--Poland</jtitle><date>2018-03-01</date><risdate>2018</risdate><volume>36</volume><issue>1</issue><spage>107</spage><epage>111</epage><pages>107-111</pages><eissn>2083-134X</eissn><abstract>LiNiO2 was prepared through two-step solid-state reaction by mechanochemical method and heat treatment, using LiOH (Li2CO3) and Ni(OH)2 as starting materials. The influence of grinding speed and time, heat treatment time, and starting materials on the structure of LiNiO2 was studied. The as-milled samples and products were characterized by scanning electron microscope (SEM) and X-ray diffraction (XRD). The results show that uniform as-milled samples can be obtained at grinding speed of 580 rpm for 0.5 h, using LiOH and Ni(OH)2 as raw materials. Perfect crystal LiNiO2 has been prepared by calcining the as-milled samples at 700 °C for 15 h. Composite material powders consisting of Li2Ni8O10 and LiNiO2 have been obtained using Li2CO3 as lithium source.</abstract><pub>De Gruyter Open</pub><doi>10.1515/msp-2018-0015</doi><tpages>5</tpages><oa>free_for_read</oa></addata></record> |
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| ispartof | Materials science--Poland, 2018-03, Vol.36 (1), p.107-111 |
| issn | 2083-134X |
| language | eng |
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| source | Walter De Gruyter: Open Access Journals; Free E-Journal (出版社公開部分のみ）; Free Full-Text Journals in Chemistry |
| subjects | grinding lithium mechanochemistry solid-state method |
| title | Synthesis of LiNiO2 by two-step solid-state method |
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