Effects of solvents and Sb sources on the morphologies of LaFe3CoSb12 nanopowders made by the hydro/solvo thermal method
The thermoelectric LaFe3CoSb12 nanopowders were synthesized by the hydro/solvo thermal method. The effects of different solvents were investigated by using only the potassium antimony tartrate as Sb source. Also, the effects of the different Sb sources were investigated by using only water as solven...
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| Veröffentlicht in: | Journal of materials research 2009-09, Vol.24 (9), p.2873-2879 |
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| container_title | Journal of materials research |
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| creator | Lu, Pengxian Shen, Zigang Hu, Xing |
| description | The thermoelectric LaFe3CoSb12 nanopowders were synthesized by the hydro/solvo thermal method. The effects of different solvents were investigated by using only the potassium antimony tartrate as Sb source. Also, the effects of the different Sb sources were investigated by using only water as solvent on the morphologies of the resulting nanopowders. The results show that a mixture of nanoparticles and nanorods can be obtained in aqueous solution of cetyltrimethylammonium bromide or ethylenediamine-tetra-acetic disodium salt. In ethylenediamine only nanorods can be obtained, and in ethylene glycol only nanoparticles can be obtained. The other morphologies of the LaFe3CoSb12, such as particle-like, nest-shaped, branch-shaped, or feather-like crystalline, can be synthesized in water by selecting a suitable Sb source. |
| doi_str_mv | 10.1557/jmr.2009.0363 |
| format | Article |
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The effects of different solvents were investigated by using only the potassium antimony tartrate as Sb source. Also, the effects of the different Sb sources were investigated by using only water as solvent on the morphologies of the resulting nanopowders. The results show that a mixture of nanoparticles and nanorods can be obtained in aqueous solution of cetyltrimethylammonium bromide or ethylenediamine-tetra-acetic disodium salt. In ethylenediamine only nanorods can be obtained, and in ethylene glycol only nanoparticles can be obtained. The other morphologies of the LaFe3CoSb12, such as particle-like, nest-shaped, branch-shaped, or feather-like crystalline, can be synthesized in water by selecting a suitable Sb source.</description><identifier>ISSN: 0884-2914</identifier><identifier>EISSN: 2044-5326</identifier><identifier>DOI: 10.1557/jmr.2009.0363</identifier><language>eng</language><publisher>New York, USA: Cambridge University Press</publisher><subject>Applied and Technical Physics ; Biomaterials ; Hydrothermal ; Inorganic Chemistry ; Materials Engineering ; Materials Science ; Nanostructure ; Nanotechnology ; Thermoelectric</subject><ispartof>Journal of materials research, 2009-09, Vol.24 (9), p.2873-2879</ispartof><rights>Copyright © Materials Research Society 2009</rights><rights>The Materials Research Society 2009</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c202t-93bccc26a9d1751154a110e2aa91794f098aa1957b5415d8b5749480db63fe5a3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1557/jmr.2009.0363$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1557/jmr.2009.0363$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Lu, Pengxian</creatorcontrib><creatorcontrib>Shen, Zigang</creatorcontrib><creatorcontrib>Hu, Xing</creatorcontrib><title>Effects of solvents and Sb sources on the morphologies of LaFe3CoSb12 nanopowders made by the hydro/solvo thermal method</title><title>Journal of materials research</title><addtitle>Journal of Materials Research</addtitle><addtitle>J. Mater. Res</addtitle><description>The thermoelectric LaFe3CoSb12 nanopowders were synthesized by the hydro/solvo thermal method. The effects of different solvents were investigated by using only the potassium antimony tartrate as Sb source. Also, the effects of the different Sb sources were investigated by using only water as solvent on the morphologies of the resulting nanopowders. The results show that a mixture of nanoparticles and nanorods can be obtained in aqueous solution of cetyltrimethylammonium bromide or ethylenediamine-tetra-acetic disodium salt. In ethylenediamine only nanorods can be obtained, and in ethylene glycol only nanoparticles can be obtained. 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Mater. Res</addtitle><date>2009-09-01</date><risdate>2009</risdate><volume>24</volume><issue>9</issue><spage>2873</spage><epage>2879</epage><pages>2873-2879</pages><issn>0884-2914</issn><eissn>2044-5326</eissn><abstract>The thermoelectric LaFe3CoSb12 nanopowders were synthesized by the hydro/solvo thermal method. The effects of different solvents were investigated by using only the potassium antimony tartrate as Sb source. Also, the effects of the different Sb sources were investigated by using only water as solvent on the morphologies of the resulting nanopowders. The results show that a mixture of nanoparticles and nanorods can be obtained in aqueous solution of cetyltrimethylammonium bromide or ethylenediamine-tetra-acetic disodium salt. In ethylenediamine only nanorods can be obtained, and in ethylene glycol only nanoparticles can be obtained. 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| subjects | Applied and Technical Physics Biomaterials Hydrothermal Inorganic Chemistry Materials Engineering Materials Science Nanostructure Nanotechnology Thermoelectric |
| title | Effects of solvents and Sb sources on the morphologies of LaFe3CoSb12 nanopowders made by the hydro/solvo thermal method |
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