Hydrothermal synthesis of carbon quantum dots from biowaste for bio-imaging
Carbon Quantum Dots (CQDs) is one of the new types of carbon-based nanomaterials which are rapidly gaining attention due to its excellent properties. In this study, a facile approach was used for synthesizing fluorescent carbon quantum dots using hydrothermal treatment of calamansi (Citrofortunella...
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description | Carbon Quantum Dots (CQDs) is one of the new types of carbon-based nanomaterials which are rapidly gaining attention due to its excellent properties. In this study, a facile approach was used for synthesizing fluorescent carbon quantum dots using hydrothermal treatment of calamansi (Citrofortunella microcarpa) and pineapples (Ananas comosus) wastes as a carbon source. The carbon quantum dots were synthesized using a 23 factorial design for the temperature, presence of TEPA, and acid type as the processing parameters to determine the best response. The composition and optical properties of the produced CQDs were characterized using a series of spectral analyses. The as-synthesized CQDs exhibited coagulation in aqueous solution and a strong blue fluorescence under UV light (λ= 365 nm). FTIR analysis confirmed the presence of functional group C-N on the surface of the CQDs which was more pronounced with the incorporation of TEPA. |
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In this study, a facile approach was used for synthesizing fluorescent carbon quantum dots using hydrothermal treatment of calamansi (Citrofortunella microcarpa) and pineapples (Ananas comosus) wastes as a carbon source. The carbon quantum dots were synthesized using a 23 factorial design for the temperature, presence of TEPA, and acid type as the processing parameters to determine the best response. The composition and optical properties of the produced CQDs were characterized using a series of spectral analyses. The as-synthesized CQDs exhibited coagulation in aqueous solution and a strong blue fluorescence under UV light (λ= 365 nm). FTIR analysis confirmed the presence of functional group C-N on the surface of the CQDs which was more pronounced with the incorporation of TEPA.</description><identifier>ISSN: 0094-243X</identifier><identifier>EISSN: 1551-7616</identifier><identifier>DOI: 10.1063/1.5094310</identifier><identifier>CODEN: APCPCS</identifier><language>eng</language><publisher>Melville: American Institute of Physics</publisher><subject>Aqueous solutions ; Carbon ; Coagulation ; Factorial design ; Fluorescence ; Functional groups ; Hydrothermal treatment ; Nanomaterials ; Optical properties ; Pineapples ; Process parameters ; Quantum dots ; Synthesis ; Ultraviolet radiation</subject><ispartof>AIP conference proceedings, 2019, Vol.2083 (1)</ispartof><rights>Author(s)</rights><rights>2019 Author(s). 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FTIR analysis confirmed the presence of functional group C-N on the surface of the CQDs which was more pronounced with the incorporation of TEPA.</description><subject>Aqueous solutions</subject><subject>Carbon</subject><subject>Coagulation</subject><subject>Factorial design</subject><subject>Fluorescence</subject><subject>Functional groups</subject><subject>Hydrothermal treatment</subject><subject>Nanomaterials</subject><subject>Optical properties</subject><subject>Pineapples</subject><subject>Process parameters</subject><subject>Quantum dots</subject><subject>Synthesis</subject><subject>Ultraviolet radiation</subject><issn>0094-243X</issn><issn>1551-7616</issn><fulltext>true</fulltext><rsrctype>conference_proceeding</rsrctype><creationdate>2019</creationdate><recordtype>conference_proceeding</recordtype><recordid>eNp9kEFLAzEQhYMoWKsH_0HAm7A12SS7yVGKWrHgRcFbmN0kdUt3s02ySv99t7TgzdPMGz7ePB5Ct5TMKCnYA50Jojij5AxNqBA0KwtanKMJGa9ZztnXJbqKcU1IrspSTtDbYmeCT982tLDBcdeNa2wi9g7XECrf4e0AXRpabHyK2AXf4qrxvxCTxc6Hg8iaFlZNt7pGFw420d6c5hR9Pj99zBfZ8v3ldf64zPpcypQZwSpXFrWlVQ2lrKwCyBkRkjFegxF8FLzi1giTO6OoFCCLihvgHDgQy6bo7ujbB78dbEx67YfQjS91ThWXKudKjNT9kYp1kyA1vtN9GJOGnaZEH8rSVJ_K-g_-8eEP1L1xbA-yvWtp</recordid><startdate>20190321</startdate><enddate>20190321</enddate><creator>de Yro, Persia Ada N.</creator><creator>Quaichon, Gerald Mari O.</creator><creator>Cruz, Roland Andrew T.</creator><creator>Emolaga, Carlo S.</creator><creator>Que, Mar Christian O.</creator><creator>Magdaluyo, Eduardo R.</creator><creator>Basilia, Blessie A.</creator><general>American Institute of Physics</general><scope>8FD</scope><scope>H8D</scope><scope>L7M</scope></search><sort><creationdate>20190321</creationdate><title>Hydrothermal synthesis of carbon quantum dots from biowaste for bio-imaging</title><author>de Yro, Persia Ada N. ; Quaichon, Gerald Mari O. ; Cruz, Roland Andrew T. ; Emolaga, Carlo S. ; Que, Mar Christian O. ; Magdaluyo, Eduardo R. ; Basilia, Blessie A.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-p288t-d53bf76ce1bca78be9aa23058334cad542304b4ed5d2fd9185a86b4da44a4a0e3</frbrgroupid><rsrctype>conference_proceedings</rsrctype><prefilter>conference_proceedings</prefilter><language>eng</language><creationdate>2019</creationdate><topic>Aqueous solutions</topic><topic>Carbon</topic><topic>Coagulation</topic><topic>Factorial design</topic><topic>Fluorescence</topic><topic>Functional groups</topic><topic>Hydrothermal treatment</topic><topic>Nanomaterials</topic><topic>Optical properties</topic><topic>Pineapples</topic><topic>Process parameters</topic><topic>Quantum dots</topic><topic>Synthesis</topic><topic>Ultraviolet radiation</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>de Yro, Persia Ada N.</creatorcontrib><creatorcontrib>Quaichon, Gerald Mari O.</creatorcontrib><creatorcontrib>Cruz, Roland Andrew T.</creatorcontrib><creatorcontrib>Emolaga, Carlo S.</creatorcontrib><creatorcontrib>Que, Mar Christian O.</creatorcontrib><creatorcontrib>Magdaluyo, Eduardo R.</creatorcontrib><creatorcontrib>Basilia, Blessie A.</creatorcontrib><collection>Technology Research Database</collection><collection>Aerospace Database</collection><collection>Advanced Technologies Database with Aerospace</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>de Yro, Persia Ada N.</au><au>Quaichon, Gerald Mari O.</au><au>Cruz, Roland Andrew T.</au><au>Emolaga, Carlo S.</au><au>Que, Mar Christian O.</au><au>Magdaluyo, Eduardo R.</au><au>Basilia, Blessie A.</au><au>Agarwal, Ramesh K.</au><format>book</format><genre>proceeding</genre><ristype>CONF</ristype><atitle>Hydrothermal synthesis of carbon quantum dots from biowaste for bio-imaging</atitle><btitle>AIP conference proceedings</btitle><date>2019-03-21</date><risdate>2019</risdate><volume>2083</volume><issue>1</issue><issn>0094-243X</issn><eissn>1551-7616</eissn><coden>APCPCS</coden><abstract>Carbon Quantum Dots (CQDs) is one of the new types of carbon-based nanomaterials which are rapidly gaining attention due to its excellent properties. In this study, a facile approach was used for synthesizing fluorescent carbon quantum dots using hydrothermal treatment of calamansi (Citrofortunella microcarpa) and pineapples (Ananas comosus) wastes as a carbon source. The carbon quantum dots were synthesized using a 23 factorial design for the temperature, presence of TEPA, and acid type as the processing parameters to determine the best response. The composition and optical properties of the produced CQDs were characterized using a series of spectral analyses. The as-synthesized CQDs exhibited coagulation in aqueous solution and a strong blue fluorescence under UV light (λ= 365 nm). FTIR analysis confirmed the presence of functional group C-N on the surface of the CQDs which was more pronounced with the incorporation of TEPA.</abstract><cop>Melville</cop><pub>American Institute of Physics</pub><doi>10.1063/1.5094310</doi><tpages>5</tpages><oa>free_for_read</oa></addata></record> |
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subjects | Aqueous solutions Carbon Coagulation Factorial design Fluorescence Functional groups Hydrothermal treatment Nanomaterials Optical properties Pineapples Process parameters Quantum dots Synthesis Ultraviolet radiation |
title | Hydrothermal synthesis of carbon quantum dots from biowaste for bio-imaging |
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