MgO NPs synthesis, capping and enhanced free radical effect on the bacteria and its cell morphology
Magnesium Oxide Nanoparticles (MgO NPs) commonly known as Magnesia is a white powder, hygroscopic material. MgO NPs were synthesized through four methods Co-precipitation method (Co-PM), Solution combustion (S-CoM) and Sol-gel method with starch (So-GSM) and CTAB (So-GCM), classified as template dep...
Gespeichert in:
Hauptverfasser: | , |
---|---|
Format: | Tagungsbericht |
Sprache: | eng |
Online-Zugang: | Volltext |
Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
container_end_page | |
---|---|
container_issue | 1 |
container_start_page | |
container_title | |
container_volume | 1961 |
creator | Kushwaha, Amisha Bagchi, T. |
description | Magnesium Oxide Nanoparticles (MgO NPs) commonly known as Magnesia is a white powder, hygroscopic material. MgO NPs were synthesized through four methods Co-precipitation method (Co-PM), Solution combustion (S-CoM) and Sol-gel method with starch (So-GSM) and CTAB (So-GCM), classified as template dependent and template independent method using magnesium nitrate hexahydrate (Mg(NO3).6H2O) as the precursor and comparative analysis was done through DLS. The order of hydrodynamic diameters of four different synthesis method of MgO NPs is Co-PM |
doi_str_mv | 10.1063/1.5035212 |
format | Conference Proceeding |
fullrecord | <record><control><sourceid>scitation</sourceid><recordid>TN_cdi_scitation_primary_10_1063_1_5035212</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>acp</sourcerecordid><originalsourceid>FETCH-LOGICAL-c230t-d63e776825bbec7d88140f729f33c77dd2a71b5c2cf20d2bb946520dc166fb673</originalsourceid><addsrcrecordid>eNotkL1OwzAYRS0EEqUw8AbfjEjxT2wnI6r4kwplAIktsj_brVHqRLGXvj0FOt27nDMcQq4ZXTCqxB1bSCokZ_yEzJiUrNKKqVMyo7StK16Lr3NykfM3pbzVupkRfN2s4e09Q96nsvU55ltAM44xbcAkBz5tTULvIEzew2RcRNODD8FjgSHBgQFrsPgpmj8glgzo-x52wzRuh37Y7C_JWTB99lfHnZPPx4eP5XO1Wj-9LO9XFXJBS-WU8FqrhktrPWrXNKymQfM2CIFaO8eNZlYix8Cp49a2tZKHh0ypYJUWc3Lz780YiylxSN04xZ2Z9h2j3W-ejnXHPOIHzd5XhQ</addsrcrecordid><sourcetype>Publisher</sourcetype><iscdi>true</iscdi><recordtype>conference_proceeding</recordtype></control><display><type>conference_proceeding</type><title>MgO NPs synthesis, capping and enhanced free radical effect on the bacteria and its cell morphology</title><source>AIP Journals Complete</source><creator>Kushwaha, Amisha ; Bagchi, T.</creator><contributor>Pati, Ranjan ; Mukhopadhyay, Indrajit ; Ray, Abhijit</contributor><creatorcontrib>Kushwaha, Amisha ; Bagchi, T. ; Pati, Ranjan ; Mukhopadhyay, Indrajit ; Ray, Abhijit</creatorcontrib><description>Magnesium Oxide Nanoparticles (MgO NPs) commonly known as Magnesia is a white powder, hygroscopic material. MgO NPs were synthesized through four methods Co-precipitation method (Co-PM), Solution combustion (S-CoM) and Sol-gel method with starch (So-GSM) and CTAB (So-GCM), classified as template dependent and template independent method using magnesium nitrate hexahydrate (Mg(NO3).6H2O) as the precursor and comparative analysis was done through DLS. The order of hydrodynamic diameters of four different synthesis method of MgO NPs is Co-PM<So-GSM<S-CoM<So-GCM. Co-PM getting lesser particle size of MgO NPs considered for the further studies and characterized through UV/Visible spectroscopy, DLS and FTIR spectroscopy and particle size was confirmed with transmission electron microscopy (TEM), crystal lattice was estimated by XRD spectroscopy, morphology was confirmed with SEM and surface absorbed free radicals were analysed with electron spin resonance (ESR). Subsequently, MgO NPs were capped with Lauric acid (LA). Further, antibacterial assay of MgO NPs, LA capped MgO NPs (LA-MgO) and LA studied against bacteria through Minimum Inhibitory Concentration (MIC). In the antibacterial test the Ascending order for bactericidal activity responding against Bacillus pumilus was resultant as LA> LA-MgO NPs> MgO NPs responding.</description><identifier>ISSN: 0094-243X</identifier><identifier>EISSN: 1551-7616</identifier><identifier>DOI: 10.1063/1.5035212</identifier><identifier>CODEN: APCPCS</identifier><language>eng</language><ispartof>AIP conference proceedings, 2018, Vol.1961 (1)</ispartof><rights>Author(s)</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c230t-d63e776825bbec7d88140f729f33c77dd2a71b5c2cf20d2bb946520dc166fb673</citedby></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://pubs.aip.org/acp/article-lookup/doi/10.1063/1.5035212$$EHTML$$P50$$Gscitation$$H</linktohtml><link.rule.ids>314,780,784,794,4512,27924,27925,76384</link.rule.ids></links><search><contributor>Pati, Ranjan</contributor><contributor>Mukhopadhyay, Indrajit</contributor><contributor>Ray, Abhijit</contributor><creatorcontrib>Kushwaha, Amisha</creatorcontrib><creatorcontrib>Bagchi, T.</creatorcontrib><title>MgO NPs synthesis, capping and enhanced free radical effect on the bacteria and its cell morphology</title><title>AIP conference proceedings</title><description>Magnesium Oxide Nanoparticles (MgO NPs) commonly known as Magnesia is a white powder, hygroscopic material. MgO NPs were synthesized through four methods Co-precipitation method (Co-PM), Solution combustion (S-CoM) and Sol-gel method with starch (So-GSM) and CTAB (So-GCM), classified as template dependent and template independent method using magnesium nitrate hexahydrate (Mg(NO3).6H2O) as the precursor and comparative analysis was done through DLS. The order of hydrodynamic diameters of four different synthesis method of MgO NPs is Co-PM<So-GSM<S-CoM<So-GCM. Co-PM getting lesser particle size of MgO NPs considered for the further studies and characterized through UV/Visible spectroscopy, DLS and FTIR spectroscopy and particle size was confirmed with transmission electron microscopy (TEM), crystal lattice was estimated by XRD spectroscopy, morphology was confirmed with SEM and surface absorbed free radicals were analysed with electron spin resonance (ESR). Subsequently, MgO NPs were capped with Lauric acid (LA). Further, antibacterial assay of MgO NPs, LA capped MgO NPs (LA-MgO) and LA studied against bacteria through Minimum Inhibitory Concentration (MIC). In the antibacterial test the Ascending order for bactericidal activity responding against Bacillus pumilus was resultant as LA> LA-MgO NPs> MgO NPs responding.</description><issn>0094-243X</issn><issn>1551-7616</issn><fulltext>true</fulltext><rsrctype>conference_proceeding</rsrctype><creationdate>2018</creationdate><recordtype>conference_proceeding</recordtype><sourceid/><recordid>eNotkL1OwzAYRS0EEqUw8AbfjEjxT2wnI6r4kwplAIktsj_brVHqRLGXvj0FOt27nDMcQq4ZXTCqxB1bSCokZ_yEzJiUrNKKqVMyo7StK16Lr3NykfM3pbzVupkRfN2s4e09Q96nsvU55ltAM44xbcAkBz5tTULvIEzew2RcRNODD8FjgSHBgQFrsPgpmj8glgzo-x52wzRuh37Y7C_JWTB99lfHnZPPx4eP5XO1Wj-9LO9XFXJBS-WU8FqrhktrPWrXNKymQfM2CIFaO8eNZlYix8Cp49a2tZKHh0ypYJUWc3Lz780YiylxSN04xZ2Z9h2j3W-ejnXHPOIHzd5XhQ</recordid><startdate>20180511</startdate><enddate>20180511</enddate><creator>Kushwaha, Amisha</creator><creator>Bagchi, T.</creator><scope/></search><sort><creationdate>20180511</creationdate><title>MgO NPs synthesis, capping and enhanced free radical effect on the bacteria and its cell morphology</title><author>Kushwaha, Amisha ; Bagchi, T.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c230t-d63e776825bbec7d88140f729f33c77dd2a71b5c2cf20d2bb946520dc166fb673</frbrgroupid><rsrctype>conference_proceedings</rsrctype><prefilter>conference_proceedings</prefilter><language>eng</language><creationdate>2018</creationdate><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Kushwaha, Amisha</creatorcontrib><creatorcontrib>Bagchi, T.</creatorcontrib></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Kushwaha, Amisha</au><au>Bagchi, T.</au><au>Pati, Ranjan</au><au>Mukhopadhyay, Indrajit</au><au>Ray, Abhijit</au><format>book</format><genre>proceeding</genre><ristype>CONF</ristype><atitle>MgO NPs synthesis, capping and enhanced free radical effect on the bacteria and its cell morphology</atitle><btitle>AIP conference proceedings</btitle><date>2018-05-11</date><risdate>2018</risdate><volume>1961</volume><issue>1</issue><issn>0094-243X</issn><eissn>1551-7616</eissn><coden>APCPCS</coden><abstract>Magnesium Oxide Nanoparticles (MgO NPs) commonly known as Magnesia is a white powder, hygroscopic material. MgO NPs were synthesized through four methods Co-precipitation method (Co-PM), Solution combustion (S-CoM) and Sol-gel method with starch (So-GSM) and CTAB (So-GCM), classified as template dependent and template independent method using magnesium nitrate hexahydrate (Mg(NO3).6H2O) as the precursor and comparative analysis was done through DLS. The order of hydrodynamic diameters of four different synthesis method of MgO NPs is Co-PM<So-GSM<S-CoM<So-GCM. Co-PM getting lesser particle size of MgO NPs considered for the further studies and characterized through UV/Visible spectroscopy, DLS and FTIR spectroscopy and particle size was confirmed with transmission electron microscopy (TEM), crystal lattice was estimated by XRD spectroscopy, morphology was confirmed with SEM and surface absorbed free radicals were analysed with electron spin resonance (ESR). Subsequently, MgO NPs were capped with Lauric acid (LA). Further, antibacterial assay of MgO NPs, LA capped MgO NPs (LA-MgO) and LA studied against bacteria through Minimum Inhibitory Concentration (MIC). In the antibacterial test the Ascending order for bactericidal activity responding against Bacillus pumilus was resultant as LA> LA-MgO NPs> MgO NPs responding.</abstract><doi>10.1063/1.5035212</doi><tpages>12</tpages></addata></record> |
fulltext | fulltext |
identifier | ISSN: 0094-243X |
ispartof | AIP conference proceedings, 2018, Vol.1961 (1) |
issn | 0094-243X 1551-7616 |
language | eng |
recordid | cdi_scitation_primary_10_1063_1_5035212 |
source | AIP Journals Complete |
title | MgO NPs synthesis, capping and enhanced free radical effect on the bacteria and its cell morphology |
url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2024-12-21T13%3A47%3A08IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-scitation&rft_val_fmt=info:ofi/fmt:kev:mtx:book&rft.genre=proceeding&rft.atitle=MgO%20NPs%20synthesis,%20capping%20and%20enhanced%20free%20radical%20effect%20on%20the%20bacteria%20and%20its%20cell%20morphology&rft.btitle=AIP%20conference%20proceedings&rft.au=Kushwaha,%20Amisha&rft.date=2018-05-11&rft.volume=1961&rft.issue=1&rft.issn=0094-243X&rft.eissn=1551-7616&rft.coden=APCPCS&rft_id=info:doi/10.1063/1.5035212&rft_dat=%3Cscitation%3Eacp%3C/scitation%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_id=info:pmid/&rfr_iscdi=true |