Effect of sintering treatment on structural and magnetic properties of Ni0.5Co0.5Fe2O4 ferrites
Two sets of Ni0.5Co0.5Fe2O4 ferrites were synthesized using sol-gel method. Both the samples were heat treated at different temperatures. The effect of sintering treatment analyzed on structural and magnetic properties. X-ray diffraction (XRD) and scanning electron microscope (SEM) were used for str...
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description | Two sets of Ni0.5Co0.5Fe2O4 ferrites were synthesized using sol-gel method. Both the samples were heat treated at different temperatures. The effect of sintering treatment analyzed on structural and magnetic properties. X-ray diffraction (XRD) and scanning electron microscope (SEM) were used for structural analysis. Alternating gradient magnetometer (AGM) is used for magnetic measurements. In structural analysis, grains size is calculated using Debye - Scherrer’s formula and Williamson-Hall (W-H) plot. From both the techniques, grain size is found nearly same and increased in size with increase sintering temperature. Increased particle size is confirmed from SEM micrographs. Strain value is calculated from intercept of W-H plot. In both the samples, compressive strain in nature is found. Magnetic properties were also varying under different heat treatment. The change in magnetic properties with change in structural change at different sintering treatment is discussed in this report. |
doi_str_mv | 10.1063/1.4946557 |
format | Conference Proceeding |
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C.</creator><contributor>Bhardwaj, Sudhir ; Shekhawat, Manoj Singh ; Suthar, Bhuvneshwer</contributor><creatorcontrib>Nandan, Brajesh ; Bhatnagar, M. C. ; Bhardwaj, Sudhir ; Shekhawat, Manoj Singh ; Suthar, Bhuvneshwer</creatorcontrib><description>Two sets of Ni0.5Co0.5Fe2O4 ferrites were synthesized using sol-gel method. Both the samples were heat treated at different temperatures. The effect of sintering treatment analyzed on structural and magnetic properties. X-ray diffraction (XRD) and scanning electron microscope (SEM) were used for structural analysis. Alternating gradient magnetometer (AGM) is used for magnetic measurements. In structural analysis, grains size is calculated using Debye - Scherrer’s formula and Williamson-Hall (W-H) plot. From both the techniques, grain size is found nearly same and increased in size with increase sintering temperature. Increased particle size is confirmed from SEM micrographs. Strain value is calculated from intercept of W-H plot. 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Both the samples were heat treated at different temperatures. The effect of sintering treatment analyzed on structural and magnetic properties. X-ray diffraction (XRD) and scanning electron microscope (SEM) were used for structural analysis. Alternating gradient magnetometer (AGM) is used for magnetic measurements. In structural analysis, grains size is calculated using Debye - Scherrer’s formula and Williamson-Hall (W-H) plot. From both the techniques, grain size is found nearly same and increased in size with increase sintering temperature. Increased particle size is confirmed from SEM micrographs. Strain value is calculated from intercept of W-H plot. In both the samples, compressive strain in nature is found. Magnetic properties were also varying under different heat treatment. The change in magnetic properties with change in structural change at different sintering treatment is discussed in this report.</description><subject>Compressive properties</subject><subject>Debye-Scherrer method</subject><subject>Ferrites</subject><subject>Heat treatment</subject><subject>Magnetic measurement</subject><subject>Magnetic properties</subject><subject>Magnetism</subject><subject>Mathematical analysis</subject><subject>Photomicrographs</subject><subject>Scanning electron microscopy</subject><subject>Sintering</subject><subject>Sol-gel processes</subject><subject>Structural analysis</subject><subject>X-ray diffraction</subject><issn>0094-243X</issn><issn>1551-7616</issn><fulltext>true</fulltext><rsrctype>conference_proceeding</rsrctype><creationdate>2016</creationdate><recordtype>conference_proceeding</recordtype><recordid>eNp9kE9LAzEQxYMoWKsHv0HAm7A1_7N7lNKqUOylB28hzU5KSptdk6zgt3dLBW9eZmD4vfeGh9A9JTNKFH-iM9EIJaW-QBMqJa20ouoSTQhpRMUE_7hGNznvCWGN1vUEmYX34AruPM4hFkgh7nBJYMsR4niOOJc0uDIke8A2tvhodxFKcLhPXQ-pBMgn8XsgMznvxrEEthbYQ0qhQL5FV94eMtz97inaLBeb-Wu1Wr-8zZ9XVc8kLxXbSqFdTX0tBDhOG6KV3nLWtlx6LQVpWe1aZhsKtaPOSSEdaKd8ozgbBVP0cLYdv_ocIBez74YUx0TDKKO6FkzLkXo8U9mFYkvooulTONr0bSgxp_4MNb_9_Qd_dekPNH3r-Q8nhnBB</recordid><startdate>20160506</startdate><enddate>20160506</enddate><creator>Nandan, Brajesh</creator><creator>Bhatnagar, M. C.</creator><general>American Institute of Physics</general><scope>8FD</scope><scope>H8D</scope><scope>L7M</scope></search><sort><creationdate>20160506</creationdate><title>Effect of sintering treatment on structural and magnetic properties of Ni0.5Co0.5Fe2O4 ferrites</title><author>Nandan, Brajesh ; Bhatnagar, M. C.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-p253t-2b547c81f844ec3190767b32dd35f7540d28cd2a91e8c1cc545ce7c6f9632ec3</frbrgroupid><rsrctype>conference_proceedings</rsrctype><prefilter>conference_proceedings</prefilter><language>eng</language><creationdate>2016</creationdate><topic>Compressive properties</topic><topic>Debye-Scherrer method</topic><topic>Ferrites</topic><topic>Heat treatment</topic><topic>Magnetic measurement</topic><topic>Magnetic properties</topic><topic>Magnetism</topic><topic>Mathematical analysis</topic><topic>Photomicrographs</topic><topic>Scanning electron microscopy</topic><topic>Sintering</topic><topic>Sol-gel processes</topic><topic>Structural analysis</topic><topic>X-ray diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Nandan, Brajesh</creatorcontrib><creatorcontrib>Bhatnagar, M. C.</creatorcontrib><collection>Technology Research Database</collection><collection>Aerospace Database</collection><collection>Advanced Technologies Database with Aerospace</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Nandan, Brajesh</au><au>Bhatnagar, M. C.</au><au>Bhardwaj, Sudhir</au><au>Shekhawat, Manoj Singh</au><au>Suthar, Bhuvneshwer</au><format>book</format><genre>proceeding</genre><ristype>CONF</ristype><atitle>Effect of sintering treatment on structural and magnetic properties of Ni0.5Co0.5Fe2O4 ferrites</atitle><btitle>AIP conference proceedings</btitle><date>2016-05-06</date><risdate>2016</risdate><volume>1728</volume><issue>1</issue><issn>0094-243X</issn><eissn>1551-7616</eissn><coden>APCPCS</coden><abstract>Two sets of Ni0.5Co0.5Fe2O4 ferrites were synthesized using sol-gel method. Both the samples were heat treated at different temperatures. The effect of sintering treatment analyzed on structural and magnetic properties. X-ray diffraction (XRD) and scanning electron microscope (SEM) were used for structural analysis. Alternating gradient magnetometer (AGM) is used for magnetic measurements. In structural analysis, grains size is calculated using Debye - Scherrer’s formula and Williamson-Hall (W-H) plot. From both the techniques, grain size is found nearly same and increased in size with increase sintering temperature. Increased particle size is confirmed from SEM micrographs. Strain value is calculated from intercept of W-H plot. In both the samples, compressive strain in nature is found. Magnetic properties were also varying under different heat treatment. The change in magnetic properties with change in structural change at different sintering treatment is discussed in this report.</abstract><cop>Melville</cop><pub>American Institute of Physics</pub><doi>10.1063/1.4946557</doi><tpages>4</tpages></addata></record> |
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subjects | Compressive properties Debye-Scherrer method Ferrites Heat treatment Magnetic measurement Magnetic properties Magnetism Mathematical analysis Photomicrographs Scanning electron microscopy Sintering Sol-gel processes Structural analysis X-ray diffraction |
title | Effect of sintering treatment on structural and magnetic properties of Ni0.5Co0.5Fe2O4 ferrites |
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